|
|
|
|
|
|
A Review of the Development of Modern Laboratory X-Ray Fluorescence Element Distribution Imaging and Species Analysis Technology |
SHEN Ya-ting, LUO Li-qiang |
National Research Center of Geoanalysis, Beijing 100037, China |
|
|
Abstract In recent years, with the development of X-ray source, X-ray monochromatic-focusing and detector technology and calculation methods, X-ray fluorescence (XRF) and X-ray Absorption Spectroscopy (XAS) is used to obtain better two-dimensional/three-dimensional element spatial distribution characteristics and element morphology and coordination information in the lab and widely applied in geology, environment, biology, materials, medicine, art, cultural heritage and industry. However, more requirements are put forward to analyze spatial element distribution and species characteristics in the lab, such as analyzing unigue samples with complex matrices, obtaining better detection limits and shorter detection time, and higher spatial resolution, etc. Laboratory-type XRF element spatial distribution and imaging technology are divided into focus scanning type 2D/3D XRF element spatial distribution imaging technology (focus scanning 2D/3D XRF), full field-micro X-ray fluorescence (FF-MXRF) and XRF computer Tomography (XRF-CT). The advancement of 2D/3D XRF hardware technology includes: liquid metal jet source and pyroelectric X-ray generator and other new laboratory X-ray source have improved the excitation efficiency closed-loop feedback systems overcome problemes caused by rough sample surfaces. X-ray monochromatic and vacuum systems play an important role in reducing background and light elements interferences. Pn-charge coupled device and micro pore optic have promoted the progress of FF-MXRF; The development of monochromatic focusing systems such as toroidal curved crystal, spherical curved crystal and columnar curved crystal have enabled laboratory XAS technology development. The continuous improvement of calculation methods has greatly promoted laboratory XRF element spatial distribution imaging technology and laboratory XAS technology, especially the development of 2D/3D XRF and XRF-CT. Exploring laboratory X-ray source systems, efficient monochromatic and focusing optical systems, and promoting dynamic X-ray film shooting technology are essential in the future.
|
Received: 2020-09-29
Accepted: 2020-12-08
|
|
|
[1] Romano F P, Caliri C, Cosentino L, et al. Analytical Chemistry, 2016, 88(20): 9873.
[2] Hemberg O, Otendal M, Hertz H M. Applied Physics Letters, 2003, 83(7): 1483.
[3] Bauer L, Lindqvist M, Forste F, et al. Journal of Analytical Atomic Spectrometry, 2018, 33(9): 1552.
[4] Otendal M, Tuohimaa T, Vogt U, et al. Review of Scientific Instruments, 2008, 79(1): 016102.
[5] DONG Yi-fan, FAN Rui-rui, GUO Dong-ya, et al(董亦凡, 樊瑞睿, 郭东亚, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2016, 36(2): 550.
[6] Wilke M, Harnisch K, Knapp W, et al. Journal of Vacuum Science & Technology B, 2019, 37(1): 011203.
[7] Bonfigli F, Hampai D, Dabagov S B, et al. Optical Materials, 2016, 58: 398.
[8] Poths P, Chinea-Cano E, Dzigal N, et al. X-Ray Spectrometry, 2019, 48(5): 553.
[9] DUAN Ze-ming, LIU Jun, JIANG Qi-li, et al(段泽明,刘 俊,姜其立,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2019, 39(1): 303.
[10] Garrevoet J, Vekemans B, Bauters S, et al. Analytical Chemistry, 2015, 87(13): 6544.
[11] Yagi R, Tsuji K. X-Ray Spectrometry, 2015, 44(3): 186.
[12] Conti C, Botteon A, Colombo C, et al. Analytical Methods, 2018, 10(31): 3837.
[13] Hampai D, Cherepennikov Y M, Liedl A, et al. Journal of Instrumentation, 2018, 13:C04024.
[14] Dabagov S B, Hampai D, Guglielmotti V, et al. Rendiconti Lincei. Scienze Fisiche e Naturali, 2020, 31(2): 443.
[15] Shen Y T, Luo L Q, Song Y F, et al. X-Ray Spectrometry, 2019, 48(5): 536.
[16] Liu P, Ptacek C J, Blowes D W, et al. Journal of Analytical Atomic Spectrometry, 2017, 32(8): 1582.
[17] Mantouvalou I, Lachmann T, Singh S P, et al. Analytical Chemistry, 2017, 89(10): 5453.
[18] Smit Z, Prokes R. X-Ray Spectrometry, 2019, 48(6): 682.
[19] Aida S, Matsuno T, Hasegawa T, et al. Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, 2017, 402: 267.
[20] Yi L T, Qin M, Wang K, et al. Applied Physics A: Materials Science and Processing, 2016, 122(9):856.
[21] Wrobel P M, Fraczek P, Lankosz M. Analytical Chemistry, 2016, 88(3): 1661.
[22] Lachmann T, van der Snickt G, Haschke M, et al. Journal of Analytical Atomic Spectrometry, 2016, 31(10): 1989.
[23] Li F Z, Liu Z G, Sun T X, et al. Radiation Physics and Chemistry, 2015, 112: 163.
[24] Li F Z, Liu Z G, Sun T X. Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, 2016, 373: 91.
[25] O’Neil L P, Catling D C, Elam W T. Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, 2018, 436: 173.
[26] Li F Z, Liu Z G, Sun T X. Food Chemistry, 2016, 210: 435.
[27] De Pauw E, Tack P, Lindner M, et al. Analytical Chemistry, 2020, 92(1): 1106.
[28] Scharf O, Ihle S, Ordavo I, et al. Analytical Chemistry, 2011, 83(7): 2532.
[29] Romano F P, Altana C, Cosentino L, et al. Spectrochimica Acta Part B: Atomic Spectroscopy, 2013, 86: 60.
[30] Romano F P, Caliri C, Cosentino L, et al. Analytical Chemistry, 2014, 86(21): 10892.
[31] Walter P, Sarrazin P, Gailhanou M, et al. X-Ray Spectrometry, 2019, 48(4): 274.
[32] Zhao W Y, Sakurai K. Journal of Synchrotron Radiation, 2019, 26: 230.
[33] Buchriegler J, Klingner N, Hanf D, et al. X-Ray Spectrometry, 2018, 47(4): 327.
[34] Gailhanou M, Sarrazin P, Blake D. Applied Optics, 2018, 57(23): 6795.
[35] de Jonge M D, Vogt S. Current Opinion in Structural Biology, 2010, 20(5): 606.
[36] De Samber B, Vanblaere S, Evens R, et al. Powder Diffraction, 2010, 25(2): 169.
[37] Laforce B, Vermeulen B, Garrevoet J, et al. Analytical Chemistry, 2016, 88(6): 3386.
[38] Laforce B, Masschaele B, Boone M N, et al. Analytical Chemistry, 2017, 89(19): 10617.
[39] Zhang S Y, Li L, Chen Z Q. IEEE Access, 2019, 7: 113589.
[40] Ahmed M F, Yasar S, Cho S H. IEEE Transactions on Medical Imaging, 2018, 37(11): 2483.
[41] Shaker K, Larsson J C, Hertz H M. Biomedical Optics Express, 2019, 10(8): 3773.
[42] Wei F, Chen Z W, Gibson W M. X-Ray Spectrometry, 2009, 38(5): 382.
[43] Schlesiger C, Anklamm L, Stiel H, et al. Journal of Analytical Atomic Spectrometry, 2015, 30(5): 1080.
[44] Nemeth Z, Szlachetko J, Bajnoczi E G, et al. Review of Scientific Instruments, 2016, 87(10):103105.
[45] Seidler G T, Mortensen D R, Remesnik A J, et al. Review of Scientific Instruments, 2014, 85(11):113906.
[46] Szlachetko M, Berset M, Dousse J C, et al. Review of Scientific Instruments, 2013, 84(9):093104.
[47] Seely J F, Hudson L T, Henins A, et al. Review of Scientific Instruments, 2016, 87(11): 11E305. |
[1] |
HAN Xue1, 2, LIU Hai1, 2, LIU Jia-wei3, WU Ming-kai1, 2*. Rapid Identification of Inorganic Elements in Understory Soils in
Different Regions of Guizhou Province by X-Ray
Fluorescence Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 225-229. |
[2] |
CHENG Hui-zhu1, 2, YANG Wan-qi1, 2, LI Fu-sheng1, 2*, MA Qian1, 2, ZHAO Yan-chun1, 2. Genetic Algorithm Optimized BP Neural Network for Quantitative
Analysis of Soil Heavy Metals in XRF[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3742-3746. |
[3] |
LIU Wei1, 2, ZHANG Peng-yu1, 2, WU Na1, 2. The Spectroscopic Analysis of Corrosion Products on Gold-Painted Copper-Based Bodhisattva (Guanyin) in Half Lotus Position From National Museum of China[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3832-3839. |
[4] |
LIN Hong-jian1, ZHAI Juan1*, LAI Wan-chang1, ZENG Chen-hao1, 2, ZHAO Zi-qi1, SHI Jie1, ZHOU Jin-ge1. Determination of Mn, Co, Ni in Ternary Cathode Materials With
Homologous Correction EDXRF Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3436-3444. |
[5] |
LI Xiao-li1, WANG Yi-min2*, DENG Sai-wen2, WANG Yi-ya2, LI Song2, BAI Jin-feng1. Application of X-Ray Fluorescence Spectrometry in Geological and
Mineral Analysis for 60 Years[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 2989-2998. |
[6] |
CHENG Fang-beibei1, 2, GAN Ting-ting1, 3*, ZHAO Nan-jing1, 4*, YIN Gao-fang1, WANG Ying1, 3, FAN Meng-xi4. Rapid Detection of Heavy Metal Lead in Water Based on Enrichment by Chlorella Pyrenoidosa Combined With X-Ray Fluorescence Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2500-2506. |
[7] |
ZHOU Qing-qing1, LI Dong-ling1, 2, JIANG Li-wu1, 3*, WAN Wei-hao1, ZENG Qiang4, XUE Xin4, WANG Hai-zhou1, 2*. Quantitative Statistical Study on Dendritic Component Distribution of Single Crystal Blade Based on Microbeam X-Ray Fluorescence Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2112-2118. |
[8] |
DU Zhi-heng1, 2, 3, HE Jian-feng1, 2, 3*, LI Wei-dong1, 2, 3, WANG Xue-yuan1, 2, 3, YE Zhi-xiang1, 2, 3, WANG Wen1, 2, 3. A New EDXRF Spectral Decomposition Method for Sharpening Error Wavelets[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(06): 1719-1724. |
[9] |
LIN Jing-tao, XIN Chen-xing, LI Yan*. Spectral Characteristics of “Trapiche-Like Sapphire” From ChangLe, Shandong Province[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1199-1204. |
[10] |
WU Lei1, LI Ling-yun2, PENG Yong-zhen1*. Rapid Determination of Trace Elements in Water by Total Reflection
X-Ray Fluorescence Spectrometry Using Direct Sampling[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 990-996. |
[11] |
SHAO Jin-fa1, LI Rong-wu2, PAN Qiu-li1, CHENG Lin1*. The Study of Non-Destructive Analysis of Tang Sancai Firing Technology[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 781-787. |
[12] |
XU Wei-xuan1, CHEN Wen-bin2, 3*. Determination of Barium in Purple Clay Products for Food Contact by
Energy Dispersive X-Ray Fluorescence Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(02): 475-483. |
[13] |
CHEN Ji-wen, YANG Zhen, ZHANG Shuai, CUI En-di, LI Ming*. Fast Resolution Algorithm for Overlapping Peaks Based on Multi-Peak Synergy and Pure Element Characteristic Peak Area Normalization[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(01): 151-155. |
[14] |
JIA Wen-bao1, LI Jun1, ZHANG Xin-lei1, YANG Xiao-yan2, SHAO Jin-fa3, CHEN Qi-yan1, SHAN Qing1*LING Yong-sheng1, HEI Da-qian4. Study on Sample Preparation Method of Plant Powder Samples for Total Reflection X-Ray Fluorescence Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(01): 169-174. |
[15] |
TANG Ju1, 2, DAI Zi-yun2*, LI Xin-yu2, SUN Zheng-hai1*. Investigation and Research on the Characteristics of Heavy Metal Pollution in Children’s Sandpits Based on XRF Detection[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(12): 3879-3882. |
|
|
|
|