Abstract:The method for the determination of Pb, Cd, Cr and Co released from ceramic ware by ICP-AES has been presented. The factors such as the influence of power in 4% acetic acid,the selection of analytical wavelength,and the interference of coexistent element have been investigated. The detection limits were 6.8 μg·L-1 for Pb, 0.18 μg·L-1 for Cd, 0.61 μg·L-1 for Cr, 1.0 μg·L-1 for Co. The recovery rates of the procedure were between 98% and 104%. The RSDs were between 0.27% and 1.24%. The method was simple, rapid, precise,convenient and suitable for daily inspection of import and export ceramic ware.
吕水源, 李小晶, 刘 伟, 林 华. ICP-AES法同时测定陶瓷制品铅、镉、铬、钴的溶出量 [J]. 光谱学与光谱分析, 2004, 24(09): 1124-1126.
Lü Shui-yuan, LI Xiao-jing, LIU Wei, LIN Hua . Simultaneous Determination of Pb, Cd,Cr and Co Released from Ceramic Ware by ICP-AES . SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(09): 1124-1126.