光谱学与光谱分析 |
|
|
|
|
|
Research on the Medicinal Effective Component and Characterization of Virus-Free Breeding and Sulfur Smoked Qi Chrysanthemum Based on FTIR and FT-Raman |
WANG Yu-tian, CAO Li-fang, YANG Zhe*, YAN Bing, ZHANG Li-juan |
Measurement Technology and Instrument Key Lab of Hebei Province, Yanshan University, Qinhuangdao 066004, China |
|
|
Abstract Based on Fourier transform infrared (FTIR) and Raman spectroscopy (FT - Raman), the effective medicinal composition and its content change of Qi chrysanthemum are directly and quickly determined among the virus-free breeding and sulfur smoked samples of three different groups. FTIR and FT-Raman spectra of three groups of Qi chrysanthemum sample are compared and analyzed. The results show that the intensities of multiple infrared absorption peaks are obvious different within the range of 1 800~500 cm-1 and the characteristic peak shapes are slightly different in the FTIR spectra of the three groups with obvious differences of characteristic peak shapes in FT - Raman spectrum have. FTIR and FT - Raman spectrum directly reflect that the stem tip virus-free breeding will make the volatile oil, flavonoids and other medicinal component content increase in Qi Chrysanthemum, but the sulfur smoked reduce. The FTIR, FT Raman spectroscopy for detection of effective medicinal composition changes in Qi Chrysanthemum caused by virus-free breeding or sulfur smoked establishes a scientific basis, also an effective method to test their component content.
|
Received: 2015-06-09
Accepted: 2015-10-24
|
|
Corresponding Authors:
YANG Zhe
E-mail: zheyang_her@163.com
|
|
[1] The Pharmacopoeia Committe of the People’s Republic of China(中华人民共和国药典委员会). Pharmacopeia of the People’s Republic of China(中华人民共和国药典). Beijing:Chemical Industry Press (北京: 化学工业出版社), 2005. 218. [2] FU Wei-lin, SUN Gui-ju(付为琳,孙桂菊). Science and Technology of Food Industry(食品工业科技), 2008, 29(3): 296. [3] WANG Ting-ting, WANG Shao-kang, HUANG Gui-ling, et al(王婷婷,王少康,黄桂玲, 等). Food Science(食品科学), 2013, 34(5): 95. [4] ZHANG Xiao-yuan, DUAN Li-hua, ZHAO Ding(张晓媛,段立华,赵 丁). Lishizhen Medicine and Materia Medica Research(时珍国医国药), 2008, 19(7): 1702. [5] LIU Wei-ping(刘卫平). Study on Development Present Status and Cuntermeasure of Virus Free Seed Potato in Heilongjiang Province(马铃薯脱毒种薯繁育发展现状与对策分析). Chinese Academy of Agricultural Sciences(中国农业科学院). Master Dissertation, 2013. [6] HAN Qiang, WANG Zong-hua, GUO Xin-mei, et al(韩 强,王宗花,郭新美,等). Chinese Journal of Analysis Laboratory(分析实验室), 2012, 31(3): 29. [7] ZHOU Xia, YAN Mao-wei, WAN Jun(周 霞,严茂伟,万 军). Lishizhen Medicine and Materia Medica Research(时珍国医国药), 2009, 20(l2): 3104. [8] LIU Sheng-jin, YANG Huan, WU De-kang et al(刘圣金,杨 欢,吴德康,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2015, 35(4): 909. [9] WANG Qing,BAI Xi,TANG Jun(王 青,白 希,唐 军). Chinese Journal of Spectroscopy Labaratory(光谱实验室), 2013, 30(5): 2084. [10] ZHAO Xian-de, DONG Da-ming, ZHENG Wen-gang(赵贤德,董大明,郑文刚). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2014, 34(10): 2667. [11] WU Juan-xia, XU Hua, ZHANG Jin(吴娟霞,徐 华,张 锦). Acta Chimica Sinica(化学学报), 2014, 72: 301. [12] XIE Jing-xi,CHANG Jun-biao,WANG Xu-ming(谢晶曦,常俊标,王绪明). The Application of Infrared Spectroscopy in Organic Chemistry and Medical Chemistry(红外光谱在有机化学和药物化学中的作用). Beijing:Science Press(北京:科学出版社),2001. 46. |
[1] |
XU Qi-lei, GUO Lu-yu, DU Kang, SHAN Bao-ming, ZHANG Fang-kun*. A Hybrid Shrinkage Strategy Based on Variable Stable Weighted for Solution Concentration Measurement in Crystallization Via ATR-FTIR Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(05): 1413-1418. |
[2] |
KAN Yu-na1, LÜ Si-qi1, SHEN Zhe1, ZHANG Yi-meng1, WU Qin-xian1, PAN Ming-zhu1, 2*, ZHAI Sheng-cheng1, 2*. Study on Polyols Liquefaction Process of Chinese Sweet Gum (Liquidambar formosana) Fruit by FTIR Spectra With Principal Component Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1212-1217. |
[3] |
YAN Li-dong1, ZHU Ya-ming1*, CHENG Jun-xia1, GAO Li-juan1, BAI Yong-hui2, ZHAO Xue-fei1*. Study on the Correlation Between Pyrolysis Characteristics and Molecular Structure of Lignite Thermal Extract[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 962-968. |
[4] |
LI Zong-xiang1, 2, ZHANG Ming-qian1*, YANG Zhi-bin1, DING Cong1, LIU Yu1, HUANG Ge1. Application of FTIR and XRD in Coal Structural Analysis of Fault
Tectonic[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(02): 657-664. |
[5] |
CHENG Xiao-xiao1, 2, LIU Jian-guo1, XU Liang1*, XU Han-yang1, JIN Ling1, SHEN Xian-chun1, SUN Yong-feng1. Quantitative Analysis and Source of Trans-Boundary Gas Pollution in Industrial Park[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(12): 3762-3769. |
[6] |
ZHANG Hao1, 2, HAN Wei-sheng1, CHENG Zheng-ming3, FAN Wei-wei1, LONG Hong-ming2, LIU Zi-min4, ZHANG Gui-wen5. Thermal Oxidative Aging Mechanism of Modified Steel Slag/Rubber Composites Based on SEM and FTIR[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(12): 3906-3912. |
[7] |
CHEN Jing-yi1, ZHU Nan2, ZAN Jia-nan3, XIAO Zi-kang1, ZHENG Jing1, LIU Chang1, SHEN Rui1, WANG Fang1, 3*, LIU Yun-fei3, JIANG Ling3. IR Characterizations of Ribavirin, Chloroquine Diphosphate and
Abidol Hydrochloride[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(07): 2047-2055. |
[8] |
MA Fang1, HUANG An-min2, ZHANG Qiu-hui1*. Discrimination of Four Black Heartwoods Using FTIR Spectroscopy and
Clustering Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1915-1921. |
[9] |
ZHANG Dian-kai1, LI Yan-hong1*, ZI Chang-yu1, ZHANG Yuan-qin1, YANG Rong1, TIAN Guo-cai2, ZHAO Wen-bo1. Molecular Structure and Molecular Simulation of Eshan Lignite[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1293-1298. |
[10] |
WANG Fang-fang1, ZHANG Xiao-dong1, 2*, PING Xiao-duo1, ZHANG Shuo1, LIU Xiao1, 2. Effect of Acidification Pretreatment on the Composition and Structure of Soluble Organic Matter in Coking Coal[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(03): 896-903. |
[11] |
HU Chao-shuai1, XU Yun-liang1, CHU Hong-yu1, CHENG Jun-xia1, GAO Li-juan1, ZHU Ya-ming1, 2*, ZHAO Xue-fei1, 2*. FTIR Analysis of the Correlation Between the Pyrolysis Characteristics and Molecular Structure of Ultrasonic Extraction Derived From Mid-Temperature Pitch[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(03): 889-895. |
[12] |
YANG Jiong1, 2, QIU Zhi-li1, 4*, SUN Bo3, GU Xian-zi5, ZHANG Yue-feng1, GAO Ming-kui3, BAI Dong-zhou1, CHEN Ming-jia1. Nondestructive Testing and Origin Traceability of Serpentine Jade From Dawenkou Culture Based on p-FTIR and p-XRF[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(02): 446-453. |
[13] |
HE Xiong-fei1, 2, HUANG Wei3, TANG Gang3, ZHANG Hao3*. Mechanism Investigation of Cement-Based Permeable Crystalline Waterproof Material Based on Spectral Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(12): 3909-3914. |
[14] |
ZHOU Jing1,2, ZHANG Qing-qing1,2, JIANG Jin-guo2, NIE Qian2, BAI Zhong-chen1, 2*. Study on the Rapid Identification of Flavonoids in Chestnut Rose (Rosa Roxburghii Tratt) by FTIR[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(10): 3045-3050. |
[15] |
Samy M. El-Megharbel*,Moamen S. Refat. In First Time: Synthesis and Spectroscopic Interpretations of Manganese(Ⅱ), Nickel(Ⅱ) and Mercury(Ⅱ) Clidinium Bromide Drug Complexes[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(10): 3316-3320. |
|
|
|
|