光谱学与光谱分析 |
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Speciation Analysis of Zinc in Bunge Pricklyash Seed by AAS |
TU Jian-bo1,WANG Si-wang1*,XIE Yan-hua1,LI Ding-chuan2,GAO Shuang-bin1,WANG Jian-bo1 |
1. Institute of Materia Medica of Pharmacy Department in Fourth Military Medical University,Xi’an 710032, China 2. The 305th Hospital of People’s Liberation Army, Beijing 100017, China |
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Abstract A method was developed for the investigation of the contents and the speciation of zinc in bunge pricklyash seed (BPS) in different habitats by atomic absorption spectrum (AAS). By using 0.45 μm filter membrane and chloroform,four different species of the decoction of BPS, named the suspended,the soluble,the inorganic and organic species, were obtained, and the segregation analysis methods for those species were developed. The octanol-water system was proposed to simulate the distribution of decocted zinc in the stomach and the intestine of the human body. The results showed that the decocted zinc was the main content of the total zinc, and the contents of zinc were different in different habitats, but the percentages of decocted zinc and the organism zinc were similar. The recovery for the method was 97.5%-104.0% and the relative standard deviation was less than 2.36%. The results showed that the sensitivity and reproducibility of this method were excellent.
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Received: 2006-08-08
Accepted: 2006-11-16
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Corresponding Authors:
WANG Si-wang
E-mail: wangsiw@fmmu.edu.cn
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Cite this article: |
TU Jian-bo,WANG Si-wang,XIE Yan-hua, et al. Speciation Analysis of Zinc in Bunge Pricklyash Seed by AAS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(11): 2357-2360.
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URL: |
https://www.gpxygpfx.com/EN/Y2007/V27/I11/2357 |
[1] LI Shi-zhen(李时珍). Compendium of Materia Medica(本草纲目). Beijing: People’s Medical Publishing House(北京: 人民卫生出版社), 1992. 1855. [2] DENG Zhen-yi, FAN Hong-zhang(邓振义, 樊鸿章). Shaanxi Journal of Agricultural Sciences(陕西农业科学), 2006, (2): 22. [3] SUN Rui-xia, SU Yong-xiang, SUN Jian-hui(孙瑞霞,苏永祥,孙剑辉). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2006, 26(4): 720. [4] DENG Nan-sheng, WU Feng(邓南圣, 吴 峰). Course of Environmental Chemistry(环境化学教程). Wuhan: Wuhan University Press(武汉: 武汉大学出版社), 2005. 6. [5] SUN Zhen-hua, WU Xi-hong, SUN Da-hai(孙振华, 吴熙红, 孙大海). Journal of Instrumental Analysis(分析测试学报), 2001, 20(2): 1. [6] ZHU Zhi-guo, HUA Rui-nian, LUO Wei-guo(朱志国,华瑞年,罗卫国). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2001,21(3):384. [7] Yüksel Ozdemir, Seref Gücer. Food Chemistry, 1998, 61(3): 313. [8] XIE Su-jing, XIE Shu-lian, XIE Bao-mei(谢苏婧,谢树莲,谢宝妹). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2003,23(3):615. [9] SHAWKET Abliz, WANG Ji-de,HU Xi-dan(肖开提·阿布力孜, 王吉德,胡西旦). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2005,25(12): 2082. [10] WU Yi-wei, ZHANG Han, HU Bin(吴一微,张 菡,胡 斌). Journal of Analytical Science(分析科学学报),2003,19(3):201. [11] LI Lei, XIE Ming-yong, WU Xi-hong(李 磊,谢明勇,吴熙鸿). Food Science(食品科学),2000,21(2):53. [12] GUO Chun-mei, WU Rong-lan, FENG Shun(郭春梅,武荣兰,封 顺). Journal of Instrumental Analysis(分析测试学报),2005,24(6):42. |
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