光谱学与光谱分析 |
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Simultaneous Analysis of Multi-Elements in Vegetation Oils by Inductively Coupled Plasma Atomic Emission Spectrometry |
GUO Lan1, 2,XIE Ming-yong1*,YAN Ai-ping2,XIAHOU Jian-yun2 |
1. Key Laboratory of Food Science of Ministry of Education, Nanchang University, Nanchang 330047, China 2. Center of Analysis and Testing of Nanchang University, Nanchang 330047, China |
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Abstract A simple, accurate and sensitive method for the simultaneous analysis of eleven trace elements (Fe, Cu, Co, Ni, Pb, Al, Zn, Cd, Cr, Mn and Mg) in vegetation oils by ICP-AES has been developed. The oils were digested by H2SO4 ashing method. The detection limits (MDLs) of the method for the eleven elements were in the range of 0.1-3.6 μg·kg-1. The average recoveries at three concentrations of 0.1, 0.5 mg·kg-1 were between 70.4% and 113% with the RSD in the range of 1.01%-10.6%. The proposed method has been applied to the determination of the above elements in soy, peanut, sesame, rape, tea and blended oils with satisfactory results.
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Received: 2006-08-02
Accepted: 2006-10-28
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Corresponding Authors:
XIE Ming-yong
E-mail: myxie@ncu.edu.cn
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Cite this article: |
GUO Lan,XIE Ming-yong,YAN Ai-ping, et al. Simultaneous Analysis of Multi-Elements in Vegetation Oils by Inductively Coupled Plasma Atomic Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(11): 2345-2348.
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URL: |
https://www.gpxygpfx.com/EN/Y2007/V27/I11/2345 |
[1] Anthemidis A N, Arvanitidis V, Stratis J A. Analytica Chimica Acta, 2005, 537: 271. [2] Hussain Reddy K, Prasad N B L, Sreenivasulu Reddy T. Talanta, 2003, 59: 425. [3] De Leonardis A, Macciola V, De Felice M. International Journal of Food Science and Technology, 2000, 35(4): 371. [4] CHEN Lan-ju, ZHENG Lian-yi, ZHAO Di-shun, et al(陈兰菊, 郑连义, 赵地顺, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2004, 24(8): 1013. [5] Canrio C M, Katskov D A. Journal of Analytical Atomic Spectrometry, 2005, 20: 1386. [6] CAI Qiu,LONG Mei-li(蔡 秋,龙梅立). Chinese Journal of Spectroscopy Laboratory(光谱实验室),2004,21(1):52. [7] SUN Jian-gang(孙建刚). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2003, 23(4): 793. [8] Zeiner M, Steffan I, Cindric I J. Microchemical Journal, 2005, 81: 171. [9] De Souza R M, Mathias B M, Da Silveira C L P, et al. Spectrochimica Acta Part B, 2005, 60: 711. [10] Murillo M, Benzo Z, Marcano E, et al. Journal of Analytical Atomic Spectrometry, 1999, 14(5): 815. [11] Castillo J R, Jiménez M S, Ebdon L. Journal of Analytical Atomic Spectrometry, 1999, 14(9): 1515. [12] Dugo G, La Pera L, La Torre G L, et al. Food Chemistry, 2004, 87: 639. [13] Lo Coco F, Ceccon L, Ciraolo L, et al. Food Control, 2003, 14(1): 55. [14] GB 2716—2005. Hygienic Standard for Edible Vegetable Oil(食用植物油卫生标准). |
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