| 光谱学与光谱分析 |
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| Preparation Polyacrylonitrile/Ag Nanoparticle Composite Nanofibers Via an Elelctrospinning Technique and Their Surface Enhanced Raman Scattering Study |
| SONG Wei, LI Ting-ting, WANG Xu, ZHAO Bing* |
| State Key Laboratory of Supramolecular Structure and Materials, Jilin University, Changchun 130012, China |
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Abstract In this paper, we have prepared polyacrylonitrile (PAN)/Ag nanoparticle composite nanofibers as a surface enhanced Raman scattering (SERS) substrate via an elelctrospinning technique. First, the PAN and AgNO3 were dissolved in N, N’-dimethylformamide solvent to get PAN/Ag seed solution; then the PAN/Ag seed solution was electrospun for the preparation of PAN/Ag seed composite nanofibers; Finally, the PAN/Ag seed composite nanofibers were treated by hydrazine hydrate to synthesize PAN/Ag nanoparticle composite nanofibers. The as-prepared PAN/Ag nanoparticle composite nanofibers were mixed with the probes for the SERS detection to get the SERS spectrum of the probes. The PAN/Ag nanoparticle composite nanofibers substate showed a good SERS signal when the concentration of PATP is as low as 10-6 mol·L-1. Furthermore, this kind of SERS substrate could be large-scale prepared, which showed a high commercial value.
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Received: 2013-10-10
Accepted: 2014-05-08
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Corresponding Authors:
ZHAO Bing
E-mail: zhaobing@jlu.edu.cn
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[1] Han X X, Weidinger I M, Hildebrandt P, et al. ACS Nano, 2013, 7: 3212.
[2] Song W, Mao Z, Liu X J, et al. Nanoscale, 2011, 4: 2333.
[3] Mao Z, Song W, Chen L, et al. J. Phys. Chem. C, 2011, 115(37): 18378.
[4] Xu H, Bjerneld E, Kall M, et al. Phys. Rev. Lett., 1999, 83: 4357.
[5] Lierop D, Larmour L, Faulds K, et al. Anal. Chem., 2013, 85(3): 1408.
[6] Xu H. Phys. Rev. B, 2005, 72: 073405.
[7] Ji W, Xue X, Ruan W, et al. Chem. Commun., 2011,47: 2426.
[8] Chen L, Yu Z, Lee Y, et al. Analyst, 2012, 137: 5834.
[9] Lu X F, Wang C, Wei Y. Small, 2009, 5：2349.
[10] Greiner A, Wendorff J H. Angew. Chem. Int. Ed., 2007, 46: 5670.
[11] Huang Z M, Zhang Y Z, Kotaki M, et al. Composites Sci. Technol., 2003, 63: 2223.
[12] Li D, Xia Y N. Adv. Mater., 2004, 16: 1151.
[13] Osawa M, Matsuda N, Yoshii K, et al. J. Phys. Chem., 1994, 98: 12702. |
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