光谱学与光谱分析 |
|
|
|
|
|
Preparation Polyacrylonitrile/Ag Nanoparticle Composite Nanofibers Via an Elelctrospinning Technique and Their Surface Enhanced Raman Scattering Study |
SONG Wei, LI Ting-ting, WANG Xu, ZHAO Bing* |
State Key Laboratory of Supramolecular Structure and Materials, Jilin University, Changchun 130012, China |
|
|
Abstract In this paper, we have prepared polyacrylonitrile (PAN)/Ag nanoparticle composite nanofibers as a surface enhanced Raman scattering (SERS) substrate via an elelctrospinning technique. First, the PAN and AgNO3 were dissolved in N, N’-dimethylformamide solvent to get PAN/Ag seed solution; then the PAN/Ag seed solution was electrospun for the preparation of PAN/Ag seed composite nanofibers; Finally, the PAN/Ag seed composite nanofibers were treated by hydrazine hydrate to synthesize PAN/Ag nanoparticle composite nanofibers. The as-prepared PAN/Ag nanoparticle composite nanofibers were mixed with the probes for the SERS detection to get the SERS spectrum of the probes. The PAN/Ag nanoparticle composite nanofibers substate showed a good SERS signal when the concentration of PATP is as low as 10-6 mol·L-1. Furthermore, this kind of SERS substrate could be large-scale prepared, which showed a high commercial value.
|
Received: 2013-10-10
Accepted: 2014-05-08
|
|
Corresponding Authors:
ZHAO Bing
E-mail: zhaobing@jlu.edu.cn
|
|
[1] Han X X, Weidinger I M, Hildebrandt P, et al. ACS Nano, 2013, 7: 3212. [2] Song W, Mao Z, Liu X J, et al. Nanoscale, 2011, 4: 2333. [3] Mao Z, Song W, Chen L, et al. J. Phys. Chem. C, 2011, 115(37): 18378. [4] Xu H, Bjerneld E, Kall M, et al. Phys. Rev. Lett., 1999, 83: 4357. [5] Lierop D, Larmour L, Faulds K, et al. Anal. Chem., 2013, 85(3): 1408. [6] Xu H. Phys. Rev. B, 2005, 72: 073405. [7] Ji W, Xue X, Ruan W, et al. Chem. Commun., 2011,47: 2426. [8] Chen L, Yu Z, Lee Y, et al. Analyst, 2012, 137: 5834. [9] Lu X F, Wang C, Wei Y. Small, 2009, 5:2349. [10] Greiner A, Wendorff J H. Angew. Chem. Int. Ed., 2007, 46: 5670. [11] Huang Z M, Zhang Y Z, Kotaki M, et al. Composites Sci. Technol., 2003, 63: 2223. [12] Li D, Xia Y N. Adv. Mater., 2004, 16: 1151. [13] Osawa M, Matsuda N, Yoshii K, et al. J. Phys. Chem., 1994, 98: 12702. |
[1] |
YU Qing-bo1, HU Kun2*, WANG Cui-ping3, LI Xian-hua2. Ag NPS/g-C3N4 Nanosheets Nanocomposites Used for SERS Nanosensors[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(06): 1987-1992. |
[2] |
LUAN Xin-tong1, ZHOU Tie-li1,2, SUN Cheng-bin1, TAO Yan-chun1, ZHAO Bing1, WANG Xu1, RUAN Wei-dong1*. A SERS Study on Self-Assembly Process of 1-Hexanethiol on Ag Nanoparticles: Effects on Adsorption Time and Concentration[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(04): 1130-1133. |
[3] |
JIANG Jiao-lai1, ZHANG Jing2, JIA Jian-ping1, WANG Shao-fei1, WU Hao-xi1, YUN Wen1, WANG Xiao-lin2, LIAO Jun-sheng1*. Design and Fabrication of Silver Nanoparticles/Graphen Complex Substrate and Its Application for Detecting Uranium (Ⅵ)[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2016, 36(11): 3563-3567. |
[4] |
ZHANG Xiao-lei1, ZHANG Jie1*, REN Wen-jie1, LAI Chun-hong1, 2, ZHOU Hai-jun1 . SERS Enhancement Factor Analysis and Experiment of Carbon Nanotube Arrays Coated by Ag Nanoparticles [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(06): 1567-1571. |
[5] |
Medine Abduwayit, Ismayil Nurulla, Shawket Abliz* . Preparation of Polyacrylonitrile/Natural Sand Composite Materials and Analysis of Adsorption Properties of Pb(Ⅱ) on It by FAAS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(02): 539-542. |
[6] |
JIA Hui-min1, TANG Ji-long1*, FANG Xuan1*, WANG Shuang-peng2, ZHAO Hai-feng2, FANG Dan1, WANG Xiao-hua1, FANG Fang1, LI Jin-hua1, CHU Xue-ying1, WEI Zhi-peng1, MA Xiao-hui1, XU Li1 . Preparation of MgxZn1-xO Nanofibers Using PVP Nanofibers as Templates by Atom Layer Deposition and Their Optical Properties[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2014, 34(12): 3197-3200. |
[7] |
ZHANG Xiao-lei1, ZHANG Jie1*, FAN Tuo1, REN Wen-jie1, LAI Chun-hong1, 2 . Three-Dimensional Vertically Aligned CNTs Coated by Ag Nanoparticles for Surface-Enhanced Raman Scattering [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2014, 34(09): 2444-2448. |
[8] |
YANG Bi-wen, GUO Zhou-yi, LIU Zhi-ming, WAN Ming-ming, QIN Xiao-chu, ZHONG Hui-qing* . Green Synthesis of Silver Nanoparticles and Their Application in SERS [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2013, 33(07): 1816-1819. |
[9] |
LI Rui, YAN Hong-tao* . Photometric Determination of Captopril Usinglabel-Free Silver Nanoparticles [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2013, 33(04): 1104-1107. |
[10] |
CHEN Jia-long, GAO Guang-yu, CHU Sai-sai, WANG Shu-feng*, GONG Qi-huang* . All Wavelength Picosecond Fluorescent Anisotropy of Aligned MEH-PPV/PVP Electrospun Fibers[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2012, 32(10): 2593-2596. |
[11] |
LIU Yan-hong1, 2, LI Bin1*, CONG Yan1, 2 . Synthesis and Optical Property Studies of Long-Lasting Phosphor ZrO2∶Ti Electrospinning Fibers [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2010, 30(04): 887-891. |
[12] |
Shawket Abliz, PENG Yang, WANG Ji-de, Ismayil Nurulla* . Study on Adsorption Behavior of Crosslinked Polyarylonitrile for Copper, Lead, Cadmium and Zinc Ions by Atomic Absorption Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2010, 30(04): 1113-1116. |
[13] |
AI Shi-yun1,GAO Ji-gang1,ZHU Lu-sheng2*,MA Zhi-jun1,LI Xiao-chen1. Preparation and Spectroscopic Studies of Nanosilver/Silk-Fibroin Composite[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2008, 28(09): 2126-2129. |
[14] |
YANG Zhi-jie1,2,ZHAO Hui-chun1*,DING Fen1,LI Ai-yun1,WANG Xiao-li1. Nanosilver Sensitized Fluorescence and Second-Order Scattering of Tb(Ⅲ)-Norfloxacin and Its Application[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(12): 2534-2537. |
[15] |
SUN Ru, GU Ren-ao*. Electrochemical Character of Gold/Silver Nanoparticles and SERS Studies on Benzidine[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(12): 2240-2243. |
|
|
|
|