| 光谱学与光谱分析 |
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| The New Applications of NMR Technology in the Field of Characterization of Surface Properties of the Material |
| LIANG Ni, ZHANG Di*, WEI Chao-xian |
| Faculty of Environmental Science and Engineering, Kunming University of Science and Technology, Kunming 650500, China |
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Abstract Nuclear magnetic resonance (NMR) technology has been developed continuely because of its rapid, accurate and high resolution advantages, The technology has become an important method to analyze the soil properties, and to identify the structure of matters, food analysis, medical imaging fields. This study summarized two aspects of the important applications of NMR in the characterization of the surface properties of materials. First, the use of NMR techniques for the adsorption, desorption and diffusion behaviors of polymer on solid particles (mainly SiO2 particles). Sencond, to investigate the wettability and water uptake progress of contaminated soils using NMR techniques. This study summarized the important applications of NMR techniques in the characterization of surface properties. It also showed the unique application in the field of polymer materials and environment. This study introduced the measured method for the relaxation time of substance using acorn surface area analyzer in the liquid environment. It reflect the surface properties and structural features of substance. It also provided data support for the explanation of environmental behaviors of contaminants and thus, it played an important role in the environmental field. Compared to the conventional BET method, acorn surface area analyzer showed the advantages in terms of conditions and time measurement. Especially, traditional BET method cannot get the information of the specific surface area of substances in the liquid directly, but acorn surface area analyzer solved the difficult problem. It is a new breakthrough in the field of characterization of the surface properties of materials by NMR in the liquid. We analyzed the application of acorn surface area analyzer in pharmaceuticals, cosmetic materials, electronic products because acorn surface area analyzer could reflects the important characteristics of the surface properties and structural features of substance. And we provide the prospective of the applications of NMR techniques in organic matter of soils, drug and natural products detecting.
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Received: 2014-06-11
Accepted: 2014-09-19
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Corresponding Authors:
ZHANG Di
E-mail: zhangdi2002113@sina.com
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[1] Yang X F, Furukawa T, Fujita T, et al. Hyperfine Interactions, 2014, 227(1-3): 147.
[2] Nokhrin S M, Weil J A, Howarth D F. Journal of Magnetic Resonance, 2005, 174: 209.
[3] Marie-France Dignac, Kgel-Knabner, Ingrid K gel-Knabner, et al. Journal of Plant Nutrition and Soil Science, 2002, 165(3): 281.
[4] ZANG Chong-zhi, PENG Pei-zhi, ZHANG Jie-tian, et al(臧充之, 彭培芝, 张洁天, 等). Physics Experimentation(物理实验), 2004, 24(8): 3.
[5] Krykin M A, Volkov V I, Volkov E V, et al. Applied Magnetic Resonance, 2005, 29(3): 459.
[6] Leblanc J L, Pilard J, Pianhanuruk E, et al. Journal of Applied Polymer Science, 2011, 119: 3058.
[7] BAI Huai-yong, ZHOU Ge, WANG Dian-sheng(白怀勇, 周 格, 王殿生). Physical Experiment of College(大学物理实验), 2013, 26(1): 7.
[8] Kemp W J M, Boer V O, Luijten P R, et al. NMR in Biomedicine, 2013, 26(10): 1299.
[9] Jiang J, Saito R, Grüneis A, et al. Chemical Physics Letters, 2004, 392: 383.
[10] QIAO Le, LI Yong, ZHOU Li-xia(乔 乐, 李 勇, 周丽霞). Physics Experimentation(物理实验), 2013, 33(8): 37.
[11] Barnett K G, Cosgrove T, Vincent B, et al. Macromolecules, 1981, 14(4): 1018.
[12] van Der Beek G P, Cohen Stuart M A, Cosgrove T. Langmuir, 1991, 7(2): 327.
[13] Beatrice Cattoz, Terence Cosgrove, Martin Crossman, et al. Langmuir, 2012, 28(5): 2485.
[14] Mears S J, Cosgrove T, Obey T, et al. Langmuir, 1998, 14(18): 4997.
[15] Mears S J, Cosgrove T, Thompson L, et al. Langmuir, 1998, 14(5): 997.
[16] Beatrice Cattoz, Wiebe M de Vos, Terence Cosgrove, et al. Langmuir, 2012, 28(15): 6282.
[17] Claire Roberts, Terence Cosgrove, Schmidt Randall G, et al. Macromolecules, 2001, 34(3): 538.
[18] Tatjana Garasanin, Terence Cosgrove, Leon Marteaux, et al. Langmuir, 2002, 18(26): 10298.
[19] Andrew Nelson, Jack Kevin S, Terence Cosgrove, et al. Langmuir, 2002, 18(7): 2750.
[20] Fleer G J. Colloids and Surfaces A: Physicochemical and Engineering Aspects, 1995, 104(2): 271.
[21] Catherine L Cooper, Terence Cosgrove, Jeroen S van Duijneveldt, et al. Langmuir, 2012, 28(48): 16588.
[22] James P Terry, Richard A Shakesby. Earth Surface Processes and Landforms, 1993, 18(6): 519.
[23] Louis W Dekker, Coen J Ritsema. Journal of Environmental Quality, 1995, 24(2): 324.
[24] Florence P Manalo, Apostolos Kantzas, Cooper H Langford. Environmental Science & Technology, 2003, 37(12): 2701.
[25] Tiona R Todoruk, Cooper H Langford, Apostolos Kantzas. Environmental Science & technology, 2003, 37(12): 2707.
[26] Tiona R Todoruk, Marina Litvina, Apostolos Kantzas, et al. Environmental Science & Technology, 2003, 37(13): 2878.
[27] GENG An-chao, ZHANG Shen(耿安朝, 章 申). Journal of Xiamen University(Natural Science)(厦门大学学报·自然科学版), 2006, 45(2).
[28] WU Jing-gui, WANG Ming-hui, JIANG Yi-mei, et al(吴景贵, 王明辉, 姜亦梅, 等). Acta Pedologica Sinica(土壤学报), 2006, 43(1).
[29] Kenneth S W Sing. Colloids and Surfaces, 1989, 38(1): 113.
[30] Giuffre A J, Oleson T A, Xu J, et al. American Geophysical Union, Fall Meeting Abstracts 1, 2008, 2156.
[31] Heister K. Geoderma, 2014, 216: 75.
[32] Streppel B, Hirscher M. Physical Chemistry Chemical Physics, 2010, 8: 3220.
[33] Jahanshahi M, Pacek A W, Nienow A W, et al. Journal of Chemical Technology and Biotechnology, 2003, 78: 1111.
[34] Pan Bo, Zhang Di, Li Hao, et al. Environmental Science & Technology, 2013, 47(14): 7722.
[35] Michael Hupfer, Stefanie Glss, Peter Schmieder, et al. International Review of Hydrobiology, 2008, 93(1): 1.
[36] Sren M Kristiansen, Wulf Amelung, Wolfgang Zech. Journal of Plant Nutrition and Soil Science, 2001, 164(1): 49.
[37] Cheng L L, Wen Q X, Chen B. Pedosphere, 2001, 11(2): 151.
[38] Wen Q X, Zhuo S N, Cheng L L. Pedoshpere, 2001, 11(1): 1.
[39] WANG Jun-mei, OUYANG Jie, SHANG-Qian, et al(王俊美, 欧阳捷, 尚 倩, 等). Chinese Journal of Magnetic Resonance(波谱学杂志), 2008, 25(2): 287.
[40] LIU Jiang-jiang, LIN Jin-ming(刘江疆, 林金明). Life Science Instruments(生命科学仪器), 2005, 3(3): 3.
[41] Ulrich Braumann, Heidrun Hndel, Sabine Strohschein, et al. Journal of Chromatography A, 1997, 761(1): 336.
[42] Dias D A, Urban S. Journal of Separation Science, 2009, 32: 542.
[43] Zhou G, Shi S, Zhang W, et al. Biomedical Chromatography, 2010, 24: 1130. |
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