光谱学与光谱分析 |
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Determination of Si and P in MnZn Ferrites by Inductively Coupled Plasma Mass Spectrometry |
ZHANG Ping1, FU Liang2*, NIE Xi-du1 |
1. College of Material and Chemical Engineering, Hunan Institute of Technology, Hengyang 421002, China 2. College of Chemistry and Chemical Engineering, Yangtze Normal University, Chongqing 408100, China |
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Abstract An inductively coupled plasma mass spectrometry (ICP-MS) was developed for the determination of Si and P in MnZn ferrites. The sample was digested by HNO3+HCl with microwave digestion followed by dilution with ultrapure water then the above two elements in the solution were analyzed directly by ICP-MS. The analytical elements were by introducing the helium gas into the octopole reaction system (ORS) to eliminate the polyatomic interferences caused by the high salty matrixes. The matrix effects and the instrument drift could be commendably calibrated with Y as internal standard element. The working parameters of the instrument were optimized. The NIST SRM 362 and NIST SRM 364 were used as standard reference materials. The results showed a good agreement between the certified values and the experimental results for three analytes. The detection limits for Si and P is 0.91 and 0.27 μg·L-1.
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Received: 2013-06-03
Accepted: 2013-10-12
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Corresponding Authors:
FU Liang
E-mail: zphy2008@163.com
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[1] DENG Hai-hong, JIN Feng-ying(邓海虹,金凤英). Mining&Metallurgy(矿冶), 2003, 12(3): 89. [2] Chen L, Shen Y, Bai J. Materials Letters, 2009, 63(12): 1099. [3] He J, Tang M, Zhou C, et al. Journal of Central South University of Technology, 2011, 18(4): 1074. [4] Kozono S, Takahashi S, Haraguchi H. Analytical and Bioanalytical Chemistry, 2002, 76(4): 542. [5] Hughes D M, Gregoire D C, Naka H, et al. Spectrochimica Acta Part B: Atomic Spectroscopy, 1998, 53(6-8): 1079. [6] Marin R C, Sarkis J E S, Nascimento M R L. Journal of Radioanalytical and Nuclear Chemistry, 2013, 295(1): 99. [7] NIE Xi-du, LIANG Yi-zeng, TANG You-gen, et al. Journal of Central South University of Technology, 2012, 19(9): 2416. [8] ZHU Qian-hua(朱乾华). Spectroscopy and Spectral Analysis (光谱学与光谱分析), 2013, 33(5): 1350. [9] Liu H T, Jiang S J. Spectrochimica Acta Part B: Atomic Spectroscopy, 2003, 58(1): 153. [10] Yang C H, Jiang S J. Spectrochimica Acta Part B: Atomic Spectroscopy, 2004, 59(9): 1390. [11] CHEN Yu-hong, LIU Zheng, WANG Hai-zhou(陈玉红, 刘 正, 王海舟). Metallurgical Analysis(冶金分析), 2007, 27(12): 17. [12] Gaboardi M, Humayun M. Journal of Analytical Atomic Spectrometry, 2009, 24(9): 1188. [13] Horn I, Rudnick R L, McDonough W F. Chemical Geology, 2000, 164(3-4): 281. [14] Kivel N, Schumann D, Gunther-Leopold I. Analytical and Bioanalytical Chemistry, 2013, 405(9): 2965. |
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