| 光谱学与光谱分析 |
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| Study on Different Extracts of Chrysanthemum Indicum by Fourier Transform Infrared Spectroscopy |
| ZHANG Yan-ling1, XIA Yuan1, Tsogt1*, ZHOU Qun2, SUN Su-qin2 |
1. College of Chemistry and Chemical Engineering, Inner Mongolia University, Hohhot 010021, China
2. Key Laboratory of Bioorganic Phosphorus Chemistry & Chemical Biology (Ministry of Education), Department of Chemistry, Tsinghua University, Beijing 100084, China |
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Abstract According to the macro-fingerprint characteristic of infrared spectroscopy, Fourier transform infrared spectroscopy and second-derivative infrared spectroscopy were used to analyze the extracts of chrysanthemum indicum L. by different solvents. It was speculated preliminarily that the main component of petroleum ether extract was long chain fatty acids (esters) and terpenes of small molecules, ethyl acetate extract contains terpenes and flavonoids mainly, ethanol and 95% ethanol extract was mainly composed of flavonoids and flavonoid glycosides, and deionized water extract contains polysaccharides and tannins mainly. Besides, the content of flavonoids in ethanol extract is the highest by comparison of the infrared spectroscopy of different extracts with that of buddleoside. Thus, the infrared spectroscopy can analyze directly the extracts of traditional Chinese medicines, recognize the main ingredient preliminarily, and then supply directional reference for further planning the extract scheme and detection methods.
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Received: 2012-05-28
Accepted: 2012-09-18
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Corresponding Authors:
Tsogt
E-mail: hntsogt@163.com
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[1] Pharmacopoeia Committee of the Ministry of Health of the People’s Republic of China(中华人民共和国卫生部药典委员会). Pharmacopoeia of the People’s Republic of China 2010(中华人民共和国药典2010版). Beijing: China Medical Science Press(北京: 中国医药科技出版社), 2010. 295.
[2] CAI Hua-fang(蔡华芳). China Healthcare Innovation(中国医疗前沿), 2007, 2(18): 118.
[3] CHEN Chuan-qian, SHEN Yan-ping, QU Yue-dan, et al(陈传千, 沈艳平, 屈跃丹, 等). Journal of Jilin Medical College(吉林医药学院学报), 2010, 31(03): 175.
[4] FENG Zi-ming, YANG Ya-nan, JIANG Jian-shuang, et al(冯子明, 杨桠楠, 姜建双, 等). China Journal of Chinese Materia Medica(中国中药杂志), 2010, 35(24): 3302.
[5] TANG Yi, GAO Mei-hua, YAO Mei-cun(汤 毅, 高美华, 姚美村). Journal of Chinese Medicinal Materials (中药材), 2009, 32(10): 1532.
[6] Sun Suqin, Zhou Qun, Chen Jianbo. Infrared Spectroscopy for Complex Mixtrures-Applications in Food and Traditional Chinese Medicine. Beijing: Chemical Industry Press(北京：化学工业出版社), 2011. 9.
[7] SUN Su-qin, ZHOU Qun, CHEN Jian-bo(孙素琴, 周 群, 陈建波). Analysis and Identification of the Traditional Chinese Medicine by Infrared Spectroscopy(中药红外光谱分析与鉴定). Beijing: Chemical Industry Press (北京: 化学工业出版社), 2010. 4.
[8] Sun Suqin, Chen Jian-bo, Zhou Qun, et al. Planta Medica, 2010, 76(17): 1987.
[9] LI Zhi-yong, WANG Chao-lu, SUN Su-qin, et al(李志勇, 王朝鲁, 孙素琴, 等). China Journal of Chinese Materia Medica(中国中药杂志), 2011, 36(23): 3281.
[10] Zhang Y L, Chen J B, Lei Y, et al. Journal of Molecular Structure, 2010, 974: 94.
[11] XIE Jing-xi, CHANG Jun-biao, WANG Xu-ming(谢晶曦, 常俊标, 王绪明). The Infrared Spectroscopy in Organic Chemistry and Medicinal Chemistry(红外光谱在有机化学和药物化学中的应用). Beijing: Science Press(北京: 科学出版社), 2001. 41. |
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