| 光谱学与光谱分析 |
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| Study on Determination of Carbaryl Content in Duck Meat Based on Synchronous Fluorescence Spectroscopy |
| XIAO Hai-bin1, LIU Mu-hua1, YUAN Hai-chao1, XU Jiang1, ZHAO Jin-hui1, 2* |
1. Optics-Electrics Application of Biomaterials Lab, College of Engineering, Jiangxi Agricultural University, Nanchang 330045, China
2. Key Laboratory of Key Technology on Agricultural Machine and Equipment, Ministry of Education, South China Agricultural University, Guangzhou 510642, China |
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Abstract For the rapid detection of carbaryl residue in duck meat, synchronous fluorescence spectroscopy was used, and GA combined with SVR was used to establish regression forecasting mode for the application of forecasting carbaryl residue in duck meat . Firstly, fluorescence spectrophotometer was used to get the 3D synchronous fluorescence spectra of carbaryl hydrolysate and duck solution containing carbaryl, and 140 nm was selected as the optimum wavelength difference Δλ; Secondly, some concentration quenching was analysed. Finally, GA was used to optimize and choose the 3D synchronous fluorescence spectra. According to the root mean square error of cross-validation (RMSECV) 21 characteristic wavelengths were chosen, then the full wavelength and 21 characteristic wavelengths were used as input characteristic variables of SVR regression forecasting model respectively. At last the results showed that characteristic wavelengths chosen by GA can get better forecasting results, and the correlation coefficient of the prediction samples set and the root mean squared error (RMSEP) were 0.976 4 and 12.232 2, respectively. The results of experiments showed that the synchronous fluorescence spectroscopy could be used to detect carbaryl residue in duck meat efficiently and rapidly when combined with GA-SVR.
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Received: 2012-06-10
Accepted: 2012-08-20
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Corresponding Authors:
ZHAO Jin-hui
E-mail: zjhxiaocao@sina.com
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[1] SU Jian-feng(苏建峰). Journal of Instrumental Analysis(分析测试学报), 2008, 27(12): 1298.
[2] Islam S, Hossain M S, Nahar N. Journal of Applied Sciences, 2009, 9(5): 973.
[3] González-Curbelo M A, Hernández-Borges J, Borges-Miquel T M. Food Additives & Contaminants. Part A: Chemistry, Analysis, Control, Exposure & Risk Assessment, 2012, 29(1): 104.
[4] LI Ping, WANG Xu-qing(李 萍，王绪卿). Journal of Hygiene Research(卫生研究), 2002, 31 (6): 465.
[5] HUANG Yong-hui(黄永辉). Fujian Analysis & Testing(福建分析测试), 2009, 18(3): 10.
[6] ZHANG Guo-wen, LI Wei-bo, ZHAO Nan(张国文, 李蔚博, 赵 楠). Journal of Nanchang University(南昌大学学报), 2010, 34(4): 349.
[7] WANG Zhong-dong, WANG Yu-tian, GUAN Xiao-jing(王忠东, 王玉田, 关晓晶). Analysis and Testing Technology and Instruments(分析测试技术与仪器), 2004, 10(4): 214.
[8] XU Jin-gou, WANG Zun-ben(许金钩，王尊本). Fluorescence Analysis(荧光分析法). Beijing: Science Press(北京：科学出版社), 2007.
[9] LI Wei-bo, ZHANG Guo-wen, ZHAO Nan (李蔚博, 张国文, 赵 楠). Chinese Journal of Analysis Laboratory(分析实验室), 2010, 29(12): 059.
[10] LI Qiong, LI Shu-wei, PAN Ke-liang(李 琼, 李树伟, 潘可亮). Journal of Southwest University for Nationalities(西南民族大学学报), 2011, 37(4): 0638.
[11] SHANG Li-ping, YANG Ren-jie(尚丽平，杨仁杰). The Ssite Fluorescence Spectroscopy Technology and Application(现场荧光光谱技术及其应用). Beijing: Science Press(北京：科学出版社), 2009.
[12] SHI Ji-yong, ZOU Xiao-bo, ZHAO Jie-wen (石吉勇, 邹小波, 赵杰文). Transactions of the Chinese Society of Agricultural Engineering(农业工程学报), 2011, 27(8): 283.
[13] LI Jing, XUE Long, LIU Mu-hua(黎 静，薛 龙，刘木华). Acta Agriculturae Universitatis Jiangxiensis(江西农业大学学报), 2010, 32(4) : 0723.
[14] GAO Jue, WANG Cong-qing(高 珏, 王从庆). Computer Measurement & Contro(计算机测量与控制), 2011, 19(1): 0176.
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