| 光谱学与光谱分析 |
|
|
|
|
|
| Similarity Analysis of FTIR of Lapis Micae Aureum |
| WANG Dong, WANG Yong-lu, GUO Xiao, WANG Yi-qun, WANG Bo-tao* |
| School of Pharmaceutical Science, Nanjing University of Technology, Nanjing 211816, China |
|
|
|
|
Abstract Similarity analysis of FTIR of Lapis Micae Aureum was carried out to find out the relationship between similarity of infrared spectra and the quality of medicine samples, and try to provide a new method for its quality assessment. FTIR was used to analyze Lapis Micae Aureum samples. Then 6 samples with good quality were picked up to establish a reference infrared spectra by their infrared spectra. Correlation coefficient method and the included angle cosine method were used to calculate the similarity between sample’s infrared spectra and the reference infrared spectra. For all those 19 samples with characters in accordance with Ch.P, the similarity is above 0.94, and for the others the similarity is less than 0.94. Although some samples’ source meets the requirement of Ch.P, but with poor quality by traditional experience, the similarity is lower than those of good quality. It was concluded that the similarity of infrared spectra of Lapis Micae Aureum is closely related to the quality of medicines. As a result, similarity analysis of FTIR of Lapis Micae Aureum is reliable, and can be used for its quality assessment.
|
|
Received: 2010-12-11
Accepted: 2011-04-05
|
|
|
|
Corresponding Authors:
WANG Bo-tao
E-mail: hywbt@sina.com
|
|
[1] The Pharmacopoeia Commission of the People’s Republic of China(国家药典委员会). Chinese Pharmacopoeia of the People’s Republic of China Part 1(中华人民共和国药典一部). Beijing: Chemical Industry Press(北京: 化学工业出版社), 2010. 207.
[2] ZHAO Shi-min, HU Yue-hua, XU Jing, et al(赵世民, 胡岳华, 徐 竞，等). Chinese Journal of Analytical Chemistry(分析化学), 2004, 32(4)：555.
[3] SUN Su-qin, ZHOU Qun, QIN Zhu, et al(孙素琴, 周 群, 秦 竹, 等). China Patent: CN 1447109A. 2003.
[4] XIE Pei-shan(谢培山). Atlas of Chromatogram of Chinese Medicines(中药色谱指纹图谱). Beijing: People’s Medical Press(北京: 人民卫生出版社), 2005.
[5] HONG Xiao-kun, WANG Zhi-hua(洪筱坤, 王智华). Digitized Chromatographic Spectrum of Chinese Medicines(中药数字化色谱指纹). Shanghai: Shanghai Scientific and Technical Press(上海: 上海科学技术出版社), 2003.
[6] ZHAN Xue-yan, SHI Xin-yuan, ZHAN Xiao-ri, et al(詹雪艳, 史新元, 展晓日，等). Chinese Journal of Analytical Chemistry(分析化学研究简报), 2010, 38(2)：253.
[7] NIE Lei, HU Zhen, LUO Guo-an, et al(聂 磊, 胡 震, 罗国安，等). Chinese Journal of Analytical Chemistry(分析化学), 2005, 33(6)：898.
[8] NIE Li-xing, WANG Gang-li, LI Zhi-meng, et al(聂黎行, 王钢力, 李志猛，等). J. Infrared Millim. Waves(红外与毫米波学报), 2008, 27(3)：205.
[9] ZENG Zhi, YANG Dong-hui, TAO Jing-qi, et al(曾 志, 杨东晖, 陶敬奇, 等). Chinese Journal of Analytical Chemistry(分析化学), 2004, 32(8)：1035.
[10] ZHANG Yian-qiu, HONG Jin-bo(张艳秋, 洪金波). Chinese Traditional and Herbal Drugs(中草药), 2007, 38(7)：1084.
[11] JIANG Yong, ZHANG Na, CUI Zhen, et al(姜 勇, 张 娜, 崔 振, 等). Acta Pharmaceutica Sinica(药学学报), 2006, 41(2)：179.
[12] WANG Meng-yue, WEI Jing-fei, SHI Hai, et al(王梦月, 韦静斐, 史 海, 等). Chinese Pharmaceutical Journal(中国药学杂志), 2009, 44(24)：1847.
[13] ZOU Hua-bin, YUAN Jiu-yong, DU Ai-qin, et al(邹华彬, 袁久荣, 杜爱琴, 等). China Journal of Chinese Materia Medica(中国中药杂志), 2005, 30(1)：16.
|
| [1] |
LI Yang1, LI Xiao-qi1, YANG Jia-ying1, SUN Li-juan2, CHEN Yuan-yuan1, YU Le1, WU Jing-zhu1*. Visualisation of Starch Distribution in Corn Seeds Based on Terahertz Time-Domain Spectral Reflection Imaging Technology[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2722-2728. |
| [2] |
JIN Chun-bai1, YANG Guang1*, LU Shan2*, CHEN Qiang1, 3, ZHENG Nan1. Research on Band Selection Method Based on Subspace Division and Visual Recognition[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(05): 1582-1588. |
| [3] |
CHENG Jie-hong1, CHEN Zheng-guang1, 2*, YI Shu-juan2. Wavelength Selection Algorithm Based on Minimum Correlation Coefficient for Multivariate Calibration[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(03): 719-725. |
| [4] |
AIBIBAIHAN Maturzi1, XU Rong2, LI Xiao-jin1, 3*, FAN Cong-zhao3, QI Zhi-yong3, ZHU Jun3, WANG Guo-ping3, ZHAO Ya-qin3. Study on Infrared Spectrum Fingerprint of Apocynumvenetum L. in Xinjiang Based on Double Index Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(03): 757-763. |
| [5] |
ZHOU Bing, LI Bing-xuan*, HE Xuan, LIU He-xiong，WANG Fa-zhen. Classification of Camouflages Using Hyperspectral Images Combined With Fusing Adaptive Sparse Representation and Correlation Coefficient[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(12): 3851-3856. |
| [6] |
WU Xian-xue1, 2, LI Ming2, LI Liang-xing2, DENG Xiu-juan1, MA Xian-ying3, LI Ya-li1, ZHOU Hong-jie1*. Study on the Homogeneity of Tea Powder by Infrared Spectral Similarity Evaluation[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(05): 1417-1423. |
| [7] |
LIU Shi-jie1, 2, LI Chun-lai1,3*, XU Rui1, TANG Guo-liang1, 2, XU Yan1, 2, 4, WU Bing1, 2, WANG Jian-yu1, 2, 3*. Method for Evaluating Spectral Similarity Based on First-Order Gradient Information[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(03): 776-781. |
| [8] |
HUANG Guan-ming1, GUO Xiang2, QI Jian-fei2, NING Yue2, WU Qi-sheng2, WANG Xiao-qing1*, ZENG Zhi-nan2*, ZHU Li-yan3. Establishment of Quantitative Model for Six Chemical Compositions in Crassostrea Angulata by Near Infrared Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(05): 1509-1513. |
| [9] |
CHENG Feng, YANG Ke-ming*, CUI Ying, LU Tian-yu, CHEN Li-fan, RONG Kun-peng. A Model on Detecting the Polluted Degree of Maize Leaves by Cu Pollution Vegetation Index[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(01): 209-214. |
| [10] |
YANG Chang-bao1, LIU Na2*, KUAI Kai-fu3. Research on Relationship between Spectral Characteristics, Physical Parameters and Metal Elements of Rocks in Xingcheng Area[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(09): 2953-2965. |
| [11] |
WANG Hong-peng, WAN Xiong*. Distinguishing Extra Virgin Olive Oil Based on the Correlation Coefficient of Visible Absorption Spectrum of Vegetable Oil[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(09): 2814-2819. |
| [12] |
ZHU Hong-qiu, GONG Juan, LI Yong-gang*, CHEN Jun-ming. A Spectrophotometric Detecting Method of Trace Cobalt under High Concentrated Zinc Solution[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(12): 3882-3888. |
| [13] |
ZHANG Zheng-yong1, 3, SHA Min1, 3, GUI Dong-dong1, YE Xiao-jing4, WANG Hai-yan2, 3*. Research on the Rapid Discrimination Technology of the Chinese Liquor Brands Based on the Moving Window Correlation Coefficient Spectral Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(10): 3122-3126. |
| [14] |
YANG Chang-bao1, LIU Na1*, ZHOU Zhen-chao1, LI Shang-nan1，2, ZHANG Chen-xi3, SONG Jiang-tao1. Research on the Relationship between Main Rock Metal Elements Content，Physical Parameters and Spectral Features in Tahe Area[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(08): 2569-2574. |
| [15] |
TIAN Guang-jun, LÜ Pan-jie, GU Li-na. Reflectance Spectroscopy Model for Lubricant Pollution Concentration Detection[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(07): 2152-2157. |
|
|
|
|
