光谱学与光谱分析 |
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Determination of the Content of Wear Metal in Lubrication Oil by ICP-AES |
ZHAO Jin-wei1, 2,CHENG Wei2,FENG Ya-hui2 |
1. Department of Materials Science & Engineering, Nanjing University of Science and Technology, Nanjing 210094,China 2. Jiangsu Entry-Exit Inspection and Quarantine Bureau, Nanjing 210001,China |
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Abstract An analytical method for determining wear metal elements directly by ICP-AES was proposed in this paper. The optimum condition was selected. The Conostan S-21 and Conostan 75 (oil-base standard samples) prepared by multi-element oil-base reserved standard samples were applied to make calibration curve. Oil samples were diluted 5 times by kerosene. The contents of wear metals in lubrication oil were determined by ICP-AES. The relative standard deviation (RSD) of all elements was less than 1%. In addition, the authors represented the analytical efficacy of Leeman labs multi-track profile ICP, and its rapid and accurate characters of simultaneous multi-element measurement.
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Received: 2004-01-06
Accepted: 2004-03-28
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Corresponding Authors:
ZHAO Jin-wei
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Cite this article: |
ZHAO Jin-wei,CHENG Wei,FENG Ya-hui. Determination of the Content of Wear Metal in Lubrication Oil by ICP-AES [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(06): 733-736.
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http://www.gpxygpfx.com/EN/Y2004/V24/I06/733 |
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