光谱学与光谱分析 |
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Determination of Germanium in A. Arborescens by Spectrophotometric Method |
HUI Rui-hua,HOU Dong-yan,GUAN Chong-xin |
Analytical and Testing Research Center, Anshan Normal University, Anshan 114005,China |
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Abstract A new spectrophotometric method for the determination of germanium in A. arborescens was developed. The method was based on the fact that germanium forms a stable complex with phenylfluorone in the acidified solution with CTMAB as solubilization agent. The maximum absorption of association complex is at 530 nm, the linear range is 0.1-0.7 μg·mL-1,the regression equation is A=0.081 7+0.867 7c530,(μg·mL-1) the correlation coefficient r=0.917 7, and the limit of detection is 0.65 μg·mL-1. The leaves and stems of A. arborescens were determined by the proposed method. The total amount of germanium is 697.0-1 219.5 ng·g-1, and the content of organic Ge is 95.45%-98.99%. The method is suitable for the analysis of samples which contain both organic Ge and inorganic Ge.
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Received: 2003-01-20
Accepted: 2003-08-28
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Corresponding Authors:
HUI Rui-hua
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Cite this article: |
HUI Rui-hua,HOU Dong-yan,GUAN Chong-xin. Determination of Germanium in A. Arborescens by Spectrophotometric Method [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(09): 1106-1109.
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URL: |
http://www.gpxygpfx.com/EN/Y2004/V24/I09/1106 |
[1] XIE Yong-quan et al(谢永泉等). Science of Guangdong Trace Elements(广东微量元素科学),1998, 5(2): 1. [2] FANG Yi-hua, YANG Yu-ai et al(方益华,杨玉爱等). Science of Guangdong Trace Elements(广东微量元素科学),1998, 5(1): 1. [3] LIU Yan, MA Ke-li, WU Yan, CUI Zhao-chun(刘 彦,马克里,巫 寅, 崔肇春). Chinese Traditional Herbal Drugs(中草药),1995, 26(6): 295. [4] YUAN Chang-qi, NI Tong-han et al (袁昌齐, 倪同汉等). China Journal of National Folk Medicine(中国民族民间医药杂志), 1999, (2):81. [5] NI Tong-han et al(倪同汉等). China Journal of National Folk Medica(中国民族民间医药杂志), 1999, (2):71. [6] LIAO Zhi-hua et al(廖志华等). Foreign Medicine Botany Fascicule(国外医药植物药分册),1999,14(4):148. [7] YE Yi-bing, ZHANG Xiao-hua, LI Han (叶伊兵, 张晓华, 李 涵). China Journal of National Folk Medicine(中国民族民间医药杂志), 1999, (2):77. [8] XIAO Zhi-yan, ZHAO Xiao-hong, CHEN Di-hua et al (肖志艳, 赵晓宏, 陈迪华等). Foreign Medicine Botany Fascicule( 国外医药植物药分册),1999,14(4):144. [9] WANG Qiang, YANG Jing-xiong et al(王 强, 杨竞雄等) . Chinese Traditional Herbal Drugs(中草药), 1990, 21(1):12. [10] ZHENG Jian-xian(郑建仙). Functional Food (first vol.)(功能性食品(第一卷)). Beijing: China Light Industry Press(北京:中国轻工业出版社),1995. 328.
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