光谱学与光谱分析 |
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Raman Spectroscopic Study on the Iron Oxide Film Prepared by Iron Oxidation Method |
HU Tao, LU Xin, YAN Yan, FU Yun-yi, ZHANG Han, ZHANG Shu-lin |
School of Physics, Peking University, Beijing 100871, China |
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Abstract Micro-Raman spectroscopy was used to investigate the chemical composition, microstructure and crystalline phase of an iron oxide sample with three-layer macro-structure prepared by iron oxidation. Two laser lines of 514 and 633 nm with a power of 0.5 mW on the sample were employed to excite the Raman spectra. Comparing the sample spectra to that of bulk α-Fe2O3, the sample Raman peaks were assigned. And it was found for the top-layer that the Raman frequencies were down shifted and the peak widths broadened. Therefore we verified that the top-layer of the verified sample is a nano-structure α-Fe2O3, the main component of the middle-layer is Fe3O4 and the bottom-layer is most like bulk α-Fe2O3.
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Received: 2002-07-28
Accepted: 2002-10-26
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Corresponding Authors:
ZHANG Shu-lin
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Cite this article: |
HU Tao,LU Xin,YAN Yan, et al. Raman Spectroscopic Study on the Iron Oxide Film Prepared by Iron Oxidation Method [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(09): 1072-1074.
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URL: |
http://www.gpxygpfx.com/EN/Y2004/V24/I09/1072 |
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