光谱学与光谱分析 |
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Determination of Mercury and Selenium in Bone by Atomic Absorption Spectrometry after Microwave Digestion |
LI Hui1, HU Xiao-rong1, CHENG Guang-lei2 |
1. College of Chemical Engineering, Sichuan University, Chengdu 610065, China 2. Analytical Testing Centre, Sichuan University, Chengdu 610065, China |
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Abstract Mercury and selenium in the rats’ thighbone were determinated by cold atom absorbance and flow injection hydride atom absorbance after digesting by microwave. The method of sample’s making and digesting was discussed. The factors of determination of selenium were studied. The detection limits of mercury and selenium are 1.65 and 1.78 ng·mL-1 respectively. The RSD% of mercury and selenium are 4.1% and 3.6% respectively. The linearity of calibration curve of mercury and selenium are in the concentrations of 0-120 ng·mL-1 and 0-50 ng·mL-1 respectively. The recovery of mercury and selenium are 93.72%-101.8% and 95.53%-102.2% respectively.
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Received: 2003-12-16
Accepted: 2004-04-30
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Corresponding Authors:
LI Hui
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Cite this article: |
LI Hui,HU Xiao-rong,CHENG Guang-lei. Determination of Mercury and Selenium in Bone by Atomic Absorption Spectrometry after Microwave Digestion [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(10): 1264-1266.
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URL: |
http://www.gpxygpfx.com/EN/Y2004/V24/I10/1264 |
[1] Leung S Y L, Cheng V K W, Lam Y W. Analyst, 1991, 116(6):957. [2] HU Xiao-rong, LI Hui(胡晓荣,李 晖). J. Sichuan University(Engineering science edition)(四川大学学报工程科学版),2000,32(6):27. [3] XU Fang, QIU De-ren, YANG Peng-yuan, HU Ke-ji(徐 芳,邱德仁,杨芃原,胡克季). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2002,22(2):331. [4] Tinggi U, Craven G. Microchemical J, 1996, 54:168. [5] Wei Guang Lan, Ming Keong Wong, Yoke Min Sin. Talanta, 1994, 41(2):195.
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