| 光谱学与光谱分析 |
|
|
|
|
|
| Determination of Trace Arsenic and Selenium in Jellyfish by Microwave Digestion-Hydride Generation-Atomic Fluorescence Spectrometry |
| LIU Xi-guang1，2,YU Hua-hua1, ZHAO Zeng-qin1, LI Zhi-en1, XU Zu-hong1,LI Peng-cheng1* |
1. Institute of Oceanology, Chinese Academy of Sciences, Qingdao 266071, China
2. Laiyang College of Agriculture, Qingdao 266109, China |
|
|
|
|
Abstract A method of hydride generation-atomic fluorescence spectrometry was proposed in the present paper for the determination of trace arsenic and selenium in jellyfish. The samples were treated by the combination of microwave digestion and lyophilization. The optimal conditions for treating and analyzing samples were established. The problem of the effect of the superfluous acid in the digesting solution on the results was solved, and the influence of coexisting foreign ions on the determination of arsenic and selenium was investigated. The accuracy of the method was confirmed by the method of standard additions. This method proved to be simple, rapid and repeatable, and is suitable for the analysis of biologic samples containing water.
|
|
Received: 2003-11-10
Accepted: 2004-04-09
|
|
|
|
Corresponding Authors:
LI Peng-cheng1
|
|
| Cite this article: |
|
LIU Xi-guang,YU Hua-hua,ZHAO Zeng-qin, et al. Determination of Trace Arsenic and Selenium in Jellyfish by Microwave Digestion-Hydride Generation-Atomic Fluorescence Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(06): 964-967.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2005/V25/I06/964 |
[1] Hsieh Yun-hwa, Leong Fui-ming, Barnes K W. J. Agric. Food Chem., 1996, 44: 3117.
[2] SUO You-rui, LI Tian-cai，et al(索有瑞, 李天才，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2002, 22(5): 850.
[3] Semenova N V, Leal L O, Forteza R，et al. Analytica Chimica Acta, 2003, 486: 217.
[4] PENG Kun，et al(彭 琨，等). Physical Testing and Chemical Analysis Part B: Chemical Analysis(理化检验-化学分册)，2000, 36(12): 557.
[5] WU Yun-qing，et al(伍云卿，等). Chin. J. Public Health(中国公共卫生)，2003，19(5)：614.
[6] WANG Ning-sheng，et al(王宁生，等). Traditional Chinese Drug Research and Clinical Pharmacology(中药新药与临床药理)，2002，13(4)：244.
[7] Cava-Montesinos P, Cervera M L, Pastor A. Analytica Chimica Acta, 2003, 481: 291.
[8] WANG Peng，et al(王 鹏，等). Journal of Environment and Health(环境与健康杂志), 1998, 15(1): 27.
[9] YANG Li-li, ZHANG De-qiang, GAO Ying，YUAN Chun-gang, ZHANG Yan-xin，et al(杨莉丽, 张德强, 高 英，苑春刚，张艳欣，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2003, 23(2): 368.
|
| [1] |
GUO Wei1, CHANG Hao2*, XU Can3, ZHOU Wei-jing2, YU Cheng-hao1, JI Gang2. Effect of Continuous Laser Irradiation on Scattering Spectrum
Characteristics of GaAs Cells[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3674-3681. |
| [2] |
LI Hui-ji1, LI Yan-wen1, YU Wei-wei2, HUANG Ru-meng1, SUN Hai-jie1*, PENG Zhi-kun3*. Theoretical Study on the Structures and IR Spectra of Hydration of Arsenates and Iron Arsenates[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2090-2094. |
| [3] |
WANG Xue-mei1, 2, YUMITI Maiming1, HUANG Xiao-yu1, 2, LI Rui1, 2, LIU Dong1, 2. Estimation of Arsenic Content in Soil Based on Continuous Wavelet
Transform[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(01): 206-212. |
| [4] |
WANG Lu1, SUN Feng1, 2*, WANG Ruo-su1, LIANG Ya-xin1, YAO Xue3, ZHAO Fan4. Analysis and Research on Color Paints for Cliff Statues in Qionglai Caves[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3198-3202. |
| [5] |
WAN Xiao-ming1, 2, ZENG Wei-bin1, 2, LEI Mei1, 2, CHEN Tong-bin1, 2. Micro-Distribution of Elements and Speciation of Arsenic in the Sporangium of Pteris Vittata[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(02): 478-482. |
| [6] |
WEI Yi-hua1, HUANG Qing-qing2, ZHANG Jin-yan1*, QIU Su-yan1, 3, TU Tian-hua1, YUAN Lin-feng1, DAI Ting-can1, ZHANG Biao-jin1, LI Wei-hong1, YAN Han1. Determination of 5 Kinds of Selenium Species in Livestock and Poultry Meat With Ion Pair Reversed Phase Liquid Chromatography-Atomic Fluorescence Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(12): 3822-3827. |
| [7] |
LI Zhi-yuan1,2, DENG Fan1*, HE Jun-liang2, WEI Wei1. Hyperspectral Estimation Model of Heavy Metal Arsenic in Soil[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(09): 2872-2878. |
| [8] |
LI Hui-ji1, SUN Hai-jie1, LIU Na1, PENG Zhi-kun2*, LI Yong-yu1, YAN Dan3. Theoretical Study on the Structures and IR Spectra of Hydration of Arsenates and Iron Arsenates[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(07): 2071-2076. |
| [9] |
KU Ya-lun1, YANG Ming-xing1, 2*, LIU Jia1, XU Xing1. Spectral Study on Natural Seleniumin Turquoise From Shiyan, Hubei Province[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(07): 2251-2257. |
| [10] |
CHEN Hai-jie1, 2, MA Na1, 2, BO Wei1, 2, ZHANG Ling-huo1, 2, BAI Jin-feng1,2, SUN Bin-bin1, 2, ZHANG Qin1, 2, YU Zhao-shui1, 2*. Research on the Valence State Analysis Method of Selenium in Soil and Stream Sediment[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(03): 871-874. |
| [11] |
ZHANG Xin-bo1, CONG Long-zhuang1, YANG Lan-lan1, DU Zhong-lin1, WANG Yao1, WANG Yan-xin1, HUANG Lin-jun1, GAO Fan1, Laurence A. Belfiore2, TANG Jian-guo1*. Optimal Fluorescence Property of CdSe Quantum Dots and Electrospinning Polyvinylpyrrolidone Hybrid Microfibers[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(03): 990-996. |
| [12] |
LIU Yan-yan1, TAO Ning-ping1, 2, 3, WANG Xi-chang1, 2, 3, LU Ying1, 2, 3*，XU Chang-hua1, 2, 3*. Integrated Detection of Foodborne Pathogens by In-Situ Infrared Spectroscopy Based on ZnSe Film Transmission Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(02): 419-424. |
| [13] |
LI Peng1, LI Zhi2, XU Can2, FANG Yu-qiang2. Research on the Scattering Spectrum of GaAs-Based Triple-Junction Solar Cell Based on Thin-Film Interference Theory[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(10): 3092-3097. |
| [14] |
ZHANG Hai-yang1, GAO Bai1, 2*, FAN Hua3 , SHEN Wei1, LIN Cong-ye1. Mechanism of Fluoride and Arsenic Removal by Ce/γ-Al2O3 Based on XRD and FTIR[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(09): 2869-2874. |
| [15] |
CHEN Hai-jie1, 2, MA Na1, 2, BAI Jin-feng1, 2, CHEN Da-lei3, GU Xue1, 2, YU Zhao-shui1, 2, SUN Bin-bin1, 2, ZHANG Qin1, 2*. Study on Determination of Se in Geochemical Samples by External Supply H2-Hydride Generation Atomic Fluorescence Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(09): 2896-2900. |
|
|
|
|
