光谱学与光谱分析 |
|
|
|
|
|
Determination of Rare Earth and Microelements in Chinese Herbal Medicine by Inductively Coupled Plasma Mass Spectrometry |
WANG Song-jun1,2, CAO Lin3, CHANG Ping4, HOU Tian-ping5, HOU Yue6 |
1. Center of Basic Experiment University of Science and Technology of Suzhou, Suzhou 215011, China 2. College of Earth Science, Jilin University, Changchun 130061, China 3. Department of Material Physics, University of Science and Technology of Beijing, Beijing 100083 , China 4. College of Geo-Exploration Science and Technology, Jilin University, Changchun 130026, China 5. Jilin Teachers Institute of Engineeing and Technology, Changchun 130052, China 6. College of Material and Chemical Engineering, Zhejiang University, Hangzhou 310027, China |
|
|
Abstract In this article, through the condition experiment of simultaneous determination of rare earth and trace elements in wolfsbane by inductively coupled plasma mass spectrometry(ICP-MS),the methods of low temperature ashing and nitric acid-overoxidation hydrogen(HNO3-H2O2) were compared. It was proved that the sample disposed with low temperature ashing for microelements and the sample disposed with acid digestion for rare earth satisfied the request for the method of determination. The accuracy is between 1.21% and 15.15%, and the precision is between 0.38% and 8.54%. The data of the experiment proved that the method completely satisfied the request for the determination of rare earth and microelements in the sample of Chinese herbal medicine.
|
Received: 2005-05-08
Accepted: 2005-07-26
|
|
Corresponding Authors:
WANG Song-jun
|
|
Cite this article: |
WANG Song-jun,CAO Lin,CHANG Ping, et al. Determination of Rare Earth and Microelements in Chinese Herbal Medicine by Inductively Coupled Plasma Mass Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(07): 1330-1333.
|
|
|
|
URL: |
https://www.gpxygpfx.com/EN/Y2006/V26/I07/1330 |
[1] CHEN Hao, LIU Han-lan, DONG Yuan-yan(陈 浩,刘汉兰,董元彦). Guangdong Trace Elements Science(广东微量元素科学),2001,8(3):1. [2] QI Jun-sheng(祁俊生). Computers and Applied Chemistry(计算机与应用化学),2000,17(2):181. [3] CHEN Hao(陈 浩). Journal of Analytical Science(分析科学学报),2002,18(4):333. [4] CHEN Hang-ting, CAO Shu-qin, ZENG Xian-jin(陈杭亭,曹淑琴,曾宪津). Analytical Chemistry(分析化学),1999,27(6):621. [5] LIANG Pie, CHEN Hao, HU Bin(梁 沛,陈 浩,胡 斌). Journal of Analytical Science(分析科学学报),2002,18(3):233. [6] CHANG Ping,WANG Song-jun,WANG Fei, et al(常 平,王松君,王 飞, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2003,23(3):556. [7] WANG Song-jun,CHANG Ping,SU Wei-na, et al(王松君,常 平,苏维娜, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2004,24(9):1113. [8] LIU Gui-fang, FU Yu-qin, HOU Feng-fei, et al(刘桂芳,付玉芹,侯风飞, 等). Chinese Traditional and Herbal Drugs(中草药),1996,27(2):67. [9] FENG Bao-min, PIE Yue-hu, HAN Bing(冯宝民,裴月湖,韩 冰). Journal of Shenyang Pharmaceutical University(沈阳药科大学学报),2000,17(4):258,288. [10] WANG Wen-xiang, DING Xing-bao(王文祥,丁杏苞). World Phytomedicines(国外医药·植物药分册),1996,11(6):252.
|
[1] |
ZHANG Yu-hui1, 2, DING Yong-kang3, PEI Jing-cheng1, 2*, GU Yi-lu1, 2, YU Min-da1, 2. Chemical Constituents and Spectra Characterization of Monocrystal
Rhodonite From Brazil[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3504-3508. |
[2] |
SUN Da-wei1, 2, 3, DENG Jun1, 2*, JI Bing-bing4. Study on the Preparation Mechanism of Steel Slag-Based Biomass Activated Carbon by Special Steel Slag-Discard Walnut Shells Based on ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2308-2312. |
[3] |
BI Yan-qi1, 2 , YANG Ying-dong3, DU Jing4, TANG Xiang5, LUO Wu-gan1, 2*. A Study on Mineral Material Sources of Multi-Style Bronzes Collected by Cultural Relic Administration Center of Huili County, Sichuan Province With MC-ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1140-1146. |
[4] |
WANG Zi-min1, MAO Xiao-tian1, YIN Zuo-wei1*, CHEN Chang2, CHENG Tian-jia1. Study on the Spectral Characteristics and the Color-Change Effect of Spinel[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(11): 3541-3545. |
[5] |
JUMAHONG Yilizhati1, 2, TAN Xi-juan1, 2*, LIANG Ting1, 2, ZHOU Yi1, 2. Determination of Heavy Metals and Rare Earth Elements in Bottom Ash of Waste Incineration by ICP-MS With High-Pressure Closed
Digestion Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3168-3173. |
[6] |
LUO Heng, Andy Hsitien Shen*. Based on Color Calculation and In-Situ Element Analyze to Study the Color Origin of Purple Chalcedony[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1891-1898. |
[7] |
YANG Yan-ling1, Andy Hsitien Shen1, FAN Yu-rong2, HUANG Wei-zhi1, PEI Jing-cheng1*. UV-Vis-NIR Spectroscopic Characteristics of Vanadium-Rich
Hydrothermal Synthetic Emeralds From Russia[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1199-1203. |
[8] |
ZHONG Yuan, QU Meng-wen, Andy Hsitien Shen*. Comparison of Chemical Composition and Spectroscopy of Purple- Brownish Red Garnet From Zambia, Tanzania and Australia[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(01): 184-190. |
[9] |
DU Jing1,JIN Tao2, HU Feng-dan1, ZHANG Chi1, ZHU Tie-quan3, ZHAN Chang-fa3, LI Nai-sheng1, JIA Zheng1, CHEN Yue1*. Desalination Monitoring of Wooden Shipwreck Components of the Qing Dynasty Marine Shipwreck,Xiaobaijiao No.1[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(10): 3294-3298. |
[10] |
ZHAO Ting1,2,3, CHI Hai-tao1,2,3*, LIU Yi-ren1,2,3, GAO Xia1,2,3, HUANG Zhao1,2,3, ZHANG Mei1,2,3, LI Qin-mei1,2,3. Determination of Elements in Health Food by X-Ray Fluorescence Microanalysis Combined With Inductively Coupled Plasma Mass Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(03): 750-754. |
[11] |
LIU Zhe1, LIU Liu2, YANG Yi-bing3, LI Xin4, SHI Jian-ping5, WANG Qin1*, XU Dong-qun1*. Characteristics and Sources Analysis of Element in Ambient PM2.5 in Taiyuan City[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(05): 1593-1598. |
[12] |
SUN Chuan-qiang, GONG Zi-shan, WANG Xiao-jun, YANG Ru, JIANG Xue-hui, WANG Yan*. Characterization and Determination of Gold Nanoparticles by SP-ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(07): 2267-2273. |
[13] |
YANG Fen1, 2, 3, XIE Shao-wen 1, 2, 3, WEI Chao-yang1, 2*, LIU Jin-xin1, 2, 3. Effects of Methanol Addition on Arsenic Speciation Analysis with HPLC-ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(06): 1884-1888. |
[14] |
FANG Fang1, JI Yu-shan1, BAI Na1, LI Xiang1, LIU Ying1, 2*. Study on Adsorption and Desorption Characteristics of Cd2+ and Zn2+ on the Surface Sediments of Taihu Lake by Using ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(06): 1889-1895. |
[15] |
YE Ting1, QIAO Hai-xia1, HUANG Yong1,2*, GUO Jia-chi1, MA Meng-chu1, RU Ping1, CHEN Fang-fang1, YUAN Cui-fang1, LIU Huan1, SU Zhuo-bin3, ZHANG Xue-jiao1*, GAO Yuan4. Preparation and Characterization of Silicon, Silver, Fluorine Co-Modified Hydroxyapatite Nano-Biofilms[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(04): 1198-1202. |
|
|
|
|