光谱学与光谱分析 |
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Simultaneous Determination of Phenol and Resorcinol by Dual-Wavelength Spectrophotometric Linear Regression Method |
ZHANG Qun1,ZHAN Feng2,KAI Xiao-ming1* |
1. School of Chemistry and Environmental Science, Anqing Normal College, Anqing 246011, China 2. Tongcheng Teacher’s School,Tongcheng 230003, China |
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Abstract Spectrophotometric simultaneous determination of phenol and resorcinol was studied. The absorption spectra of these two components severely overlap in ultraviolet spectral range. In the wavelength range of 250-290 nm, the absorbances of phenol and resorcinol were measured with an internal of 0.5 nm. Two wavelengths at 280.5 and 273.5 nm were chosen for the determination. Dual-wavelength linear regression method was used for the determination of phenol and resorcinol. Twenty five mixture standard solutions were prepared according to the orthogonal projection form L25(56). Two kinds of the components were linearly regressed. Meanwhile the contents of phenol and resorcinol in six synthetic mixture samples and simulation pharmaceutical preparations were measured. The measurement results showed that the relative error of phenol and resorcinol were less than 5%. The measurement system is stable and reliable. Therefore, the dual-wavelength spectrophotometric linear regression method may provide a new approach to the determintion of phenol and resorcinol in their compound preparations.
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Received: 2005-09-28
Accepted: 2006-01-08
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Corresponding Authors:
KAI Xiao-ming
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Cite this article: |
ZHANG Qun,ZHAN Feng,KAI Xiao-ming. Simultaneous Determination of Phenol and Resorcinol by Dual-Wavelength Spectrophotometric Linear Regression Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(11): 2110-2112.
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URL: |
https://www.gpxygpfx.com/EN/Y2006/V26/I11/2110 |
[1] XIANG Bing-ren(相秉仁). Computational Pharmacy(计算药学). Beijing:Chinese Medical Science and Technology Press(北京: 中国医药科技出版社), 1990. 271. [2] HU Xiao-ling,ZHANG Peng,ZHANG Gui(胡小玲,张 鹏,张 瑰). Chinese Journal of Health Laboratory Technology(中国卫生检验杂志),2004,14(1):38. [3] LIANG Yi-zeng,LU Zhi-qiang,YU Ru-qin(梁逸曾,卢志强,俞汝勤). Chemical Journal of Chinese Universities(高等学校化学学报),1989,10(7):704. [4] ZHENG Xiao-ping,MO Jin-yuan,XIE Tian-yao(郑小萍,莫金垣,谢天尧). Computers and Applied Chemsitry(计算机与应用化学),1999,16(5):371. [5] FANG Hui-sheng,XIANG Bing-ren,LI Rui, et al(方慧生,相秉仁,李 睿, 等). Chemical Journal of Chinese Universities(高等学校化学学报),1994,15(4):518. [6] KAI Xiao-ming,SHEN Yu-hua,ZHANG Gu-xin,et al(开小明,沈玉华,张谷鑫,等). Journal of Henan University of Science and Technology(Natural Science) (河南科技大学学报·自然科学版),2004,25(6):90. [7] CHEN Li-li,JIN Ji-hong,WANG Hong-mei(陈莉莉,金继红,王洪梅). Journal of Analytical Science(分析科学学报),2004,20(1):57. [8] WU Gen-hua,HE Chi-yang,CHEN Rong(吴根华,何池洋,陈 荣). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2002,22(5):813. [9] KAI Xiao-ming,SHEN Yu-hua,ZHANG Gu-xin,et al(开小明,沈玉华,张谷鑫,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2005,25(12):2070. [10] LI Zhi-liang,LIU Yi-ming,YU Ru-qin(李志良,刘一呜,俞汝勤). Chemical Journal of Chinese Universities(高等学校化学学报),1989,10(6):575.
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