光谱学与光谱分析 |
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Determination of Contents of Many Kinds of Metal Elements in Phellodendron by ICP-AES |
ZHANG Yun-liang1,2, LIU Yan-cheng1, SHI Shao-ming1, CHEN Zhen-feng1*, LIANG Hong1 |
1. The Key Laboratory for the Chemistry and Molecular Engineering of Medicinal Resources (Ministry of Education),School of Chemistry & Chemical Engineering of Guangxi Normal University, Guilin 541004, China 2. Department of Pharmacy, Shaoyang Medical College, Shaoyang 422000, China |
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Abstract Dry and wet methods were used to digest Phellodendron grown in Jinxiu Dayaoshan of Guangxi with a high-pressure jar and to prepare the samples. The contents of microelements Cu, Fe, Zn, Mn and Ni and macroelements K, Ca, Mg, Sr and Na in Phellodendron were determined by using ICP-AES. Meanwhile, the optimal digestion conditions were found: 7 mL of HNO3+HClO4+H2O2 (volume ratio 5∶1∶1) for 4 h. The work condition and the optical wavelength were selected. The RSD was found to be less than 5% and the recovery rates of all elements were within the range of 89.4%-113.1%. The determined results agree with the analytical demand, and also indicate that Phellodendron contains high contents of Cu, Fe, Zn and Mn microelements. It is important to assess the medicinal value and understand pharmacological action of Phellodendron by the determination of microelements in the Chinese medicine with ICP-AES.
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Received: 2008-06-26
Accepted: 2008-10-28
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Corresponding Authors:
CHEN Zhen-feng
E-mail: chenzfgxnu@yahoo.com
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[1] GUAN Jing-huan, LI En-kuan, XUE Sha, et al(管竞环,李恩宽,薛 莎,等). Acta Medica Sinica(中国医药学报), 1990, 5: 40. [2] Huang Ru-Jin, Zhuang Zhi-Xia, Tai Yi, et al. Talanta, 2006, 68: 728. [3] KOU Xing-ming, GU Yong-zuo, GU Xing-ping(寇兴明,顾永祚,顾兴平). Sichuan Environment(四川环境), 1999, 18(1): 28. [4] PANG Jiang-lin, CHEN Jie, LI Shang-de (庞江琳,陈 杰,李尚德). Science of Guangdong Trace Elements(广东微量元素科学), 2004, 11: 46. [5] Sun Han-wen, Qiao Feng-xia, Suo Ran, et al. Analytica Chimica Acta, 2004, 505: 255. [6] WU Qi-xun, JI Lan, KU Jin-liang, et al(吴启勋, 冀 兰, 库进良, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2008,28(8):1938. [7] YUAN Zhi-qing, QIAN Gao-feng(原志庆,千高峰). Journal of Xinxiang Medical College(新乡医学院学报), 1995, 12(4): 304. [8] CHEN Ti-qiang, LI Kai-ben, HE Xiu-jin(陈体强,李开本,何修金). China Journal of Chinese Materia Medica(中国中药杂志), 1994, 19(4): 34. [9] HOU Xiao-tao, DAI Hang, ZHOU Jiang(侯小涛,戴 航,周 江). Lishizhen Medicine and Material Medica Research(时珍国医国药), 2007, 18: 498.
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