| 光谱学与光谱分析 |
|
|
|
|
|
| Determination of Trace Sodium Ion in High Purity Water by Graphite Furnace Atomic Absorption Spectrometry |
| YUAN Xia1, 2,SHEN Shi-gang1,SUN Han-wen1 |
1. School of Chemistry and Environment Science, Hebei University, Baoding 071002, China
2. The 718th Institute of China Shipbuilding Industry Corporation, Handan 056027, China |
|
|
|
|
Abstract The present paper studied on the determination of trace Na+ in high purity water by graphite furnace atom absorption spectrometry. A method of directly on-line concentrating samples in graphite furnace, multiple charging, ashing, then determining once by directly charging into pools of graphite furnace, was set up. The goal of concentrating samples and avoiding contamination as well as raising sensitivity were finally achieved. To prevent the background of purity water and regent in experiment from covering the ion concentration of the sample, the authors prepared the high purity water and regent to meet the requirement of the experiment by electrodialysis in series with distillation and below-boiling-point quartz distillation at pure worktable. Satisfactory results of linearity and detection limit were obtained. The detection limit with this method was 0.086 μg·L-1 for Na+. The recovery was 101%-104%.
|
|
Received: 2005-12-10
Accepted: 2006-08-20
|
|
|
|
Corresponding Authors:
YUAN Xia
E-mail: hanwen@mail.hbu.edu.cn
|
|
| Cite this article: |
|
YUAN Xia,SHEN Shi-gang,SUN Han-wen. Determination of Trace Sodium Ion in High Purity Water by Graphite Furnace Atomic Absorption Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(01): 186-189.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2007/V27/I01/186 |
[1] Meng Lan-Xlang, Nanto V, Li Song-Ping. Microchemical Journal，1995, 52: 223.
[2] Radzi Bin Abas M, Ismat Ali Takrumi, Zanariah Abdullah. Talanta，2002, 58: 883.
[3] Yasuyuki Miura, Kazunobu Fukasawa, Tomozo Koh. Journal of Chromatography A, 1998, 804: 143.
[4] Jyh-Myng Zen, Chih-Chio Yang, Annamalai Senthik Kumar. Analytica Chimica Acta，2002, 464: 229.
[5] KANG Wei-jun, LIANG Shu-xuan, HA Jing(康维钧，梁淑轩，哈 婧). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2003，23(3)：572.
[6] LIU Wen-han, HU Wei, GAO Yun-fang(刘文涵, 胡 伟，高云芳). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2002，22(6)：1033.
[7] WEN Rui-mei, WANG Zai-zhong, et al(闻瑞梅，王在忠, 等). Preparation of High Purity Water and Determination Technology(高纯水的制备及检测技术). Beijing: Science Press(北京: 科学出版社)，1997.
[8] YU Hui(俞 晖). Technology of Water Treatment(水处理技术)，1993，19(2)：69.
[9] GONG Qi, LI Xiang-xin, WEI Xiao-ling, et al(龚 琦，李向欣，韦小玲，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2006，26(6)：1162.
|
| [1] |
ZHANG Han, XUE Ai-fang, CHEN Hao, LI Sheng-qing*. Low-Density Solvent Based Dispersive Liquid-Liquid Microextraction Combined with Graphite Furnace Atomic Absorption Spectrometry for the Determination of Trace Lead and Cadmium in Domestic Water[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(10): 3264-3268. |
| [2] |
SUN Bo-si, REN Ting, ZHAO Li-jiao*, ZHONG Ru-gang . Determination of Trace Lead in Environmental Water by Cloud Point Extraction-High Resolution Continuum Source Graphite Furnace Atomic Absorption Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2012, 32(10): 2847-2852. |
| [3] |
REN Ting, ZHAO Li-jiao*, CAO Jun, ZHONG Ru-gang. Determination of Pb, Cd and Cr in Food by High Resolution Continuum Source Graphite Furnace Atomic Absorption Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2012, 32(09): 2566-2571. |
| [4] |
REN Ting, ZHAO Li-jiao*, ZHONG Ru-gang . Determination of Aluminum in Wheat Flour Food by Microwave Digestion-High Resolution Continuum Source Graphite Furnace Atomic Absorption Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2011, 31(12): 3388-3391. |
| [5] |
LIU Chong-hua1, FANG Han1, LIN Xiao-yang2, ZHANG Xiao-li1, DENG Zhi-guang1, LI Yun-song2 . Determination of Trace Extractable Lead in Artificial Acid Sweat from Ecological Textiles by GFAAS [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2009, 29(11): 3150-3153. |
| [6] |
LI Sheng-qing1,HE Xiao-min1,DU Ping1,WANG Min2,CHEN Hao1*,WU Mou-cheng3. Determination of Lead in Microemulsified Rapeseed Oil and Bio-Diesel Oil by GFAAS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2008, 28(10): 2431-2435. |
| [7] |
HE Xiao-min1,WANG Min2,WANG Xiao-dong1,XUE Ai-fang1,LI Sheng-qing1,CHEN Hao1* . Determination of Lead and Cadmium in Rapeseed and Rapeseed Meal with Microwave Digestion by Graphite Furnace Atomic Absorption Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(11): 2353-2356. |
| [8] |
QIAN Sha-hua, XIANG Luo-jing*,DENG Hong-bing, XIAO Mei, LIN Han, LI Xue-qin. Preconcentration of Trace Pd(Ⅱ) on Crosslinked Chitosan and Determination by Graphite Furnace Atomic Absorption Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(03): 592-594. |
| [9] |
CHEN Shi-zhong,LU Deng-bo. Slurry Sampling for Direct Determination of Trace Cadmium in Amber by Graphite Furnace Atomic Absorption Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(10): 1928-1930. |
| [10] |
GUO Xing-jia1，2, XU Shu-kun1*,LI Xiao-zhou3,TONG Jian２, SUN Ying4, GUO Li-li4 . Determination of As, Pb, Sn, Sb and Bi in High Temperature Iron and Nickel-Based Alloy by Graphite Furnace Atomic Absorption Spectrometry Combined with Liquid-Liquid Extraction [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(06): 1167-1169. |
| [11] |
XIAO Shan-mei1, 2, CHEN Jian-rong2*, SHEN Yu-qin2 . Determination of Lead in Water Samples by Graphite Furnace Atomic Absorption Spectrometry after Cloud Point Extraction with Dithizone[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(05): 955-958. |
| [12] |
KANG Wei-jun1，2, LIANG Shu-xuan2, JIA Li-hui3, XU Li-qin1, ZHAO Yan1, SUN Han-wen2 . Determination of Trace Cadmium in Environment Water Samples by Flame Atomic Absorption Spectrometry Using Flow Injection On-Line Preconcentration with Double Microcolumns [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(05): 792-795. |
| [13] |
SONG Guang-sen. Direct Determination of Trace Lead in Chestnut by Graphite Furnace Atomic Absorption Spectrometry with Slurry Sampling [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(04): 570-572. |
| [14] |
CHEN Shi-zhong. Direct Determination of Trace Arsenic in Coal by Slurry-Sampling Graphite-Furnace Atomic Absorption Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(10): 1267-1269. |
| [15] |
YE Ming-de，LIN Mei-jin . Determination of Trace Gold by Flow Injection On-Line Preconcentration Flame Atomic Absorption Spectrometry with Trioctylamine Levextrel Resin [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(10): 1270-1272. |
|
|
|
|
