| 光谱学与光谱分析 |
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| Determination of Berberine in Phellodendron Chinese Schneid from Sichuan Using Near Infrared Diffuse Reflectance Spectroscopy |
| ZHOU Min1,WANG Tian-zhi1,YE Li-ming1*,CHEN Cong1,HUANG Guo2,WU Yan-wei2 |
1. West China School of Pharmacy,Sichuan University,Chengdu 610041,China
2. Bruker Instruments LTD.,Beijing 100081,China |
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Abstract The objective of the present study was to develop a method for the determination of berberine in phellodendron chinese schneid from Sichuan using near infrared diffuse reflectance spectroscopy. Near infrared spectra (NIR) in the range of 12 500-3 600 cm-1 were recorded for the phellodendron chinese schneid containing berberine in the content of 2.155%-8.245% of berberine. Calibration models were established using the PLS (partial least squares). Different spectra pretreatments methods were compared. The study showed that spectra information can be extracted thoroughly by second derivative pretreatments method with the correlation coefficient(r2) of 0.922 1,SEC 0.337 (standard deviation of the calibration sets) and SEP 0.251 (standard deviation of the prediction sets). Results indicated that near infrared diffuse reflectance spectroscopy method can be used to rapidly analyze the valid component in Chinese herbs.
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Received: 2006-05-28
Accepted: 2006-08-26
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Corresponding Authors:
YE Li-ming
E-mail: dryelimin@sohu.com
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| Cite this article: |
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ZHOU Min,WANG Tian-zhi,YE Li-ming, et al. Determination of Berberine in Phellodendron Chinese Schneid from Sichuan Using Near Infrared Diffuse Reflectance Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(08): 1527-1530.
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| URL: |
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https://www.gpxygpfx.com/EN/Y2007/V27/I08/1527 |
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