光谱学与光谱分析 |
|
|
|
|
|
Synthesis and Spectral Properties of Cuboid-Shaped CdS Particles |
HUANG Feng-hua |
College of Chemistry and Materials Science, Fujian Normal University, Fuzhou 350007, China |
|
|
Abstract Cuboid-shaped CdS particles were synthesized with sol-gel method by using thiourea as surface modifier and characterized by X-ray diffraction, transmission electron microscopy, infrared absorption spectrum and fluorescence spectrum. The results show that the sulfur atoms in thiourea molecules coordinate with Cd2+ ions on the surface of the nanocrystals. The thiourea-modified CdS particles have a zinc blende crystal structure and good fluorescent characteristics. The cuboid-shaped CdS particles are probably assembled by hydrogen bonding between primary CdS nanocrystals surface-capped with thiourea. The result will promote the researches into molecular self-assembly of nanocrystals and help develop novel luminescence material.
|
Received: 2006-11-02
Accepted: 2007-02-09
|
|
Corresponding Authors:
HUANG Feng-hua
E-mail: huangfenghua63@163.com
|
|
[1] Simmons B A, Li S C, John V T, et al. Nano Lett.,2002,2(4): 263. [2] YUAN Qiu-li, NIE Qiu-lin, CHEN Wei-xiang, et al(袁求理,聂秋林,陈卫祥,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2005,25(6): 971. [3] ZHANG Yu, ZHANG Jun-xiang, FU De-gang, et al(张 宇, 张俊祥, 付德刚, 等). Chinese J. Inorg. Chem.(无机化学学报), 1999, 15: 595. [4] Colvin V L, Schlamp M C, Alivisatos A P. Nature, 1994, 370: 354. [5] Zhang P, Gao L. Langmuir,2003, 19: 208. [6] Dong L F, Jiao J, Coulter M, et al. Chem. Phys. Lett.,2003, 376: 653. [7] HUANG Feng-hua, PENG Yi-ru(黄风华,彭亦如). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2006,26(6): 1102. [8] Yamaguchi A, Penland R B, Mizushima S, et al. J. Am. Chem. Soc., 1958, 80(3):527. [9] XING De-song, SHI Jian-xin, GONG Meng-lian, et al(邢德松, 石建新, 龚孟濂, 等). Chem. J. Chinese Universities(高等学校化学学报),2004,25(1): 24. [10] Premachandran R, Banerjee S, John V T, et al. Chem. Mater., 1997, 9: 1342. [11] Bagnall D M, Ullrich B, Sakai H, et al. J. Cryst. Growth,2000,214: 1015. |
[1] |
HU Shuang1, LIU Cui-mei2*, JIA Wei2, HUA Zhen-dong2. Rapid Qualitative Analysis of Synthetic Cannabinoids by Raman
Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(01): 145-150. |
[2] |
LIU Yu-ying1, 2, WANG Xi-yuan1, 2*, MEI Ao-xue1, 2. Green Preparation of Biomass Carbon Quantum Dots for Detection of Cu2+[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(01): 248-253. |
[3] |
WANG Chong1, WANG Jing-hua1, 2, LI Dong-dong1, SHE Jiang-bo2. Preparation of Gd3+-Doped LiYF4∶Yb3+/Ho3+ Micro-Crystal and the Application Research in Anti-Counterfeiting[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(11): 3581-3587. |
[4] |
WANG Yan-ru, TANG Hai-jun*, ZHANG Yao. Study on Infrared Spectral Detection of Fuel Contamination in Mobil Jet Oil II Lubricating Oil[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1541-1546. |
[5] |
YANG Yan-ling1, Andy Hsitien Shen1, FAN Yu-rong2, HUANG Wei-zhi1, PEI Jing-cheng1*. UV-Vis-NIR Spectroscopic Characteristics of Vanadium-Rich
Hydrothermal Synthetic Emeralds From Russia[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1199-1203. |
[6] |
ZHANG Jia-lin, ZHANG Qian, PEI Jing-cheng*, HUANG Wei-zhi. Gemological and Spectroscopy Characteristics of Synthetic Blue-Green Beryl by Hydrothermal Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(07): 2258-2262. |
[7] |
WANG Chong1, MO Jian-ye1,2, LI Dong-dong1, SHE Jiang-bo2, LIU Zhen2. Application and Research of NaYF4∶Yb3+/Eu3+ Upconverting Luminescent Micro-Nano Particles in Anti-Counterfeiting Identification[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(05): 1525-1529. |
[8] |
WANG Shi-xia, HU Tian-yi, YANG Meng. Study on Preparation of Ag-Doped ZnO Nanomaterials and Phase Transition at High Pressure Using Diamond Anvil Cell and Raman Spectra[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(02): 484-488. |
[9] |
WANG Zhi-wei1, 2, 3, YUE Guang-yang1*, WU Xiao-dong1, ZHANG Wen2, WANG Pu-chang2, SONG Xue-lian2, WU Jia-hai2. A Study on Ground Deformations Monitoring in Tianshan Mountain of Xinjiang on Active Microwave Spectral Imagines[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(08): 2366-2372. |
[10] |
XIONG Yang1,2, XU Jun1,2, QIU Su-yan1,2, WEI Yi-hua1,2, ZHANG Jin-yan1,2*. Study on Interaction Between Phenylethanolamine A and CdTe Nanomaterials by Fluorescence Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(05): 1402-1406. |
[11] |
WANG Meng-xin 1,2, LUO A-li1,2. Spectral Analysis of Host Galaxy from Possible Dual AGNs[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(01): 290-293. |
[12] |
TAN Guan-ni1, GAO Hong1,2*, SONG Jie3, SHANG Shi-bin1,2, SONG Zhan-qian1,2. Synthesis, Spatial Configuration and Spectral Properties of Donor-Acceptor Molecules with Dehydroabietic Acid Triarylamine as Donors[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(07): 2083-2090. |
[13] |
LIANG Rong1, LAN Yan1, 2, ZHANG Tian-yang2, LU Tai-jin3, CHEN Mu-yu1, WANG Xiao-qing1, ZHANG Xiao-hu1. Multi-Spectroscopy Studies on Large Grained HPHT Synthetic Diamonds from Shandong, China[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(06): 1840-1845. |
[14] |
DONG Xue1, QI Li-jian2, ZHOU Zheng-yu2, SUN Dui-xiong1*. Spectral Characteristics and Application of Synthetic Hydrothermal Red Beryl[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(02): 517-521. |
[15] |
SUN Yan-wen1, CHANG Yu2, JIN Yu-fen1, XIE Wen-bing2, CHANG Jing1, YU Ting1*, PAN Li-hua2. Study of Synthesis and Spectral Property of Europium Cryptate[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(07): 2189-2193. |
|
|
|
|