| 光谱学与光谱分析 |
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| Comparative Study on Five Pretreatment Methods for ICP-OES Determination of Mineral Elements in Rosa rugosa |
| ZHAO Ning，YANG Bin*，DUAN Yu-cen，LEI Ran |
| Key Laboratory for Forest Resources Conservation and Use in the Southwest Mountains of China of Ministry of Education, Southwest Forestry University，Kunming 650224，China |
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Abstract Five different pretreatment methods, including dry ashing and microwave digestion with four acid systems (HNO3+H2O2, HNO3+H2O2+HF, HNO3+HClO4 and HNO3+HClO4+HF), were employed for digestion of the samples of Rosa rugosa. Nine major and trace elements were determined using ICP-OES method. The addition standard recovery rates indicate that, with the system of HNO3+HClO4, better results can be obtained for most of the determined elements. With this method, except for Fe, the recovery rates are in the range of 95.4%～104.6%. For Fe, higher recovery rate (99%) was obtained with HNO3+H2O2+HF system.
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Received: 2010-10-09
Accepted: 2011-04-07
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Corresponding Authors:
YANG Bin
E-mail: yangbin48053@yahoo.com.cn
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