光谱学与光谱分析 |
|
|
|
|
|
Spectral Analysis of Elements in Different Samples of Processed Foeniculum vulgare |
ZHANG Fan1, 2, LI Zhen2, HAMULATI Wufuer1, TIAN Shu-ge2 |
1. Pharmaceutical Post-doctoral Station, Xinjiang Medical University, Urumqi 830011, China 2. Chinese Medicine College, Xinjiang Medical University, Urumqi 830011, China |
|
|
Abstract The compositions and contents of chemical compounds in traditional Chinese medicines would be changed after being processed using different methods, and their pharmacological activity may be influenced. ICP-AES, AAS and AFS were the first methods to be used to scan and analyze macro elements, trace elements and heavy metals in Foeniculum vulgare and its nine different processed samples in the present paper, which were correlated with people’s health and lives. The experiment results showed that the three kinds of analyzing methods could be used to judge the contents and the changing trend of all elements in traditional Chinese medicine quickly and truly. Thirty two elements were found in F. vulgare, and there were noticeable changes in the contents of some elements in processed samples compared with F. vulgare without processing. These results indicated that there is great relevance between changes in the contends of elements with different processing methods, and auxiliary materials can not only change the contents of elements but also play a role in treating ills with effective constituents. Also, it was firstly found that the content of Hg rose greatly in the experiment, and these showed there was notable potential safety hazard when processed Foeniculum vulgare was used. These experiments widen the application of spectrum analyzing methods in safety evaluation of traditional Chinese medicine.
|
Received: 2009-05-10
Accepted: 2009-08-20
|
|
Corresponding Authors:
ZHANG Fan
E-mail: zhangfan596@163.com
|
|
[1] Chinese Pharmacopoeia Committee(国家药典委员会). Pharmacopoeia of the People’s Republic of China(Volume 1)(中华人民共和国药典, 一部). Beijing: Chemical Industry Press(北京: 化学工业出版社), 2005: 32. [2] RAN Mao-xiong, GUO Jian-min(冉懋雄, 郭建民). Handbook of Modern Frying Chinese Medicinal Herbs(现代中药炮制手册). Beijing: China Press of Traditional Chinese Medicine(北京: 中国中医药出版社), 2002. 464. [3] LI Zhen, ZHANG Fan, ZHANG Gang(李 臻, 张 帆, 张 刚). Xinjiang Journal of Traditional Chinese Medicine(新疆中医药), 2008, 26(4): 52. [4] YIN Jun-ya, DING Li, ZHANG Zheng-xing(尹峻雅, 丁 黎, 张正行). China Pharmacist(中国药师), 1999, 2(6): 321. [5] ZHANG Fan, HE Wen-jing, SUN Yun, et al(张 帆, 何文静, 孙 芸, 等). Chinese Journal of Analytical Chemistry(分析化学), 2008, 36(4): 541. [6] YE Ding-jiang, ZHANG Shi-chen(叶定江, 张世臣). Science of Frying Chinese Medicinal Herbs(中药炮制学). Beijing: People’s Medical Publishing House(北京: 人民卫生出版社), 2004: 520.
|
[1] |
ZHU Zhao-zhou1*, YANG Xin-xin1, LI Jun1, HE Hui-jun2, ZHANG Zi-jing1, YAN Wen-rui1. Determination of Rare Earth Elements in High-Salt Water by ICP-MS
After Pre-Concentration Using a Chelating Resin[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1862-1866. |
[2] |
YANG Lin-yu1, 2, 3, DING Yu1, 2, 3*, ZHAN Ye4, ZHU Shao-nong1, 2, 3, CHEN Yu-juan1, 2, 3, DENG Fan1, 2, 3, ZHAO Xing-qiang1, 2, 3. Quantitative Analysis of Mn and Ni Elements in Steel Based on LIBS and GA-PLS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1804-1808. |
[3] |
CHENG Can1, HEI Da-qian2*, JIA Wen-bao1, SHAN Qing1, LING Yong-sheng1, ZHAO Dong1. Study on Metallic Samples Determination Based on Prompt Gamma
Neutron Activation Analysis Technique[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1928-1933. |
[4] |
WANG Ling-ling1, 2, 3, WANG Bo1, 2, 3, XIONG Feng1, 2, 3, YANG Lu-cun1, 2, LI Jing-jing4, XIAO Yuan-ming1, 2, 3, ZHOU Guo-ying1, 2*. A Comparative Study of Inorganic Elements in Cultivativing Astragalus Membranaceus From Different Habitats[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1407-1412. |
[5] |
LI Xiao-li1, GAO Xin-hua2, WANG Yi-min3*, DENG Sai-wen3, WANG Yi-ya3, LI Song3. Review on the Application of X-Ray Fluorescence Spectrometry in Halogen Elements Analysis in Geological Materials[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 997-1009. |
[6] |
ZHENG Pei-chao, LIU Ran-ning, WANG Jin-mei, FENG Chu-hui, HE Yu-tong, WU Mei-ni, HE Yu-xin. Solution Cathode Glow Discharge-Atomic Emission Spectroscopy Coupled With Hydride Generation for Detecting Trace Mercury and Tin in Water[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1139-1143. |
[7] |
LI Xue-ping1, 2, 3, ZENG Qiang1, 2, 3*. Development and Progress of Spectral Analysis in Coal Structure Research[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(02): 350-357. |
[8] |
GONG Ge-lian1, 2, YOU Li-bing3, LI Cong-ying4, FANG Xiao-dong3, SUN Wei-dong4, 5, 6. Advances in Equipment for Deep Ultra-Violet Excimer Laser Ablation Coupled Plasma Mass and Optical Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(02): 555-560. |
[9] |
LIU Qin-rong1, DU Zi-wei1, LI Jia-zhen1, WANG Yi-shuo1, 3*, GU Xuan2, CUI Xiu-mei2. Analysis and Evaluation of Inorganic Elements in Salvia miltiorrhiza and Rhizosphere Soils From Different Areas[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(11): 3618-3624. |
[10] |
LIU Hong-wei1,3, FU Liang2*. Analysis of Metal Impurity Elements in Li4Ti5O12 Through Microwave Plasma Atomic Emission Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(10): 3021-3025. |
[11] |
LIU Ming-bo1,2, LIAO Xue-liang2, CHENG Da-wei1,2, NI Zi-yue1,2, WANG Hai-zhou1,2*. An EDXRF Quantitative Algorithm Based on Fundamental Parameters and Spectrum Unfolding[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(09): 2807-2811. |
[12] |
LIU Wei, YU Qiang*, NIU Teng, YANG Lin-zhe, LIU Hong-jun, YAN Fei. Study on the Relationship Between Element As in Soil of Agricultural Land and Leaf Spectral Characteristics[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(09): 2866-2871. |
[13] |
MENG Ru2,4, DU Jin-hua1,2*, LIU Yun-hua1,2, LUO Lin-tao1,3, HE Ke1,2, LIU Min-wu1,2, LIU Bo1,3. Exploration of Digestion Method for Determination of Heavy Metal Elements in Soil by ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(07): 2122-2128. |
[14] |
GUO Mei1, 2, ZHANG Ruo-yu2, 3, ZHU Rong-guang2, 3, DUAN Hong-wei1, 2*. Quantitative Determination of Water-Soluble P in Biochar Based on NELIBS Technology and EN-SVR Model[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(07): 2301-2306. |
[15] |
REN Jiang-bo1,2, WANG Fen-lian1,2*, HE Gao-wen1, 2, ZHANG Xin3, DENG Xi-guang1,2, YU Hong-xia4. μ-XRF Analysis and Data Mining of Deep-Sea Co-Rich Ferromanganese Nodules in Western Pacific[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(06): 1834-1840. |
|
|
|
|