光谱学与光谱分析 |
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Study of Reference Material for Excitation Spectrum Wavelength Calibration of Fluorescence Spectrophotometer |
CHEN Xiao-bo, KANG Dong-guo, ZHAO Cheng-yi, LI Song, WU Zheng-long, MA Hui, LIU Zhong-min, ZHENG Zhe |
Applied Optics Beijing Area Major Laboratory,Analytical and Testing Center,Beijing Normal University,Beijing 100875,China |
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Abstract A reference material used for wavelength calibration of fluorescence spectrophotometer was found.The holmium doped oxide reference material GBW(E)130112 is a kind of standard reference material for absorption spectrophotometer.It can emit 547.7 nm fluorescence when excited by xenon lamp light.The excitation spectrum of 547.7 nm fluorescence was measured.It was found that the measured peaks of excitation spectrum are positioned at 333.56, 360.43 and 418.39 nm, respectively, which are coincident with the true values 333.8, 360.9 and 418.5 nm of reference material certification.It was illustrated that the holmium doped oxide reference material GBW(E)130112 could be used as reference material for the excitation wavelength calibration of the fluorescence spectrophotometer.Its property could be enhanced very much if high luminescent efficiency material is selected as rare earth ion doped matrix, and the purity is enhanced to reduce the cross relaxation.
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Received: 2004-03-16
Accepted: 2004-07-16
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Corresponding Authors:
CHEN Xiao-bo
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Cite this article: |
CHEN Xiao-bo,KANG Dong-guo,ZHAO Cheng-yi, et al. Study of Reference Material for Excitation Spectrum Wavelength Calibration of Fluorescence Spectrophotometer [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(07): 1165-1167.
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URL: |
https://www.gpxygpfx.com/EN/Y2005/V25/I07/1165 |
[1] SONG Zeng-fu(宋增福).The Principle and Application of Atom and Crystal Spectroscopy(原子光谱及晶体光谱原理与应用).Beijing: Science Press(北京: 科学出版社),1997. [2] WANG Guo-wen(王国文).Introduction of Atomic and Molecular Spectroscopy(原子分子光谱导论).Beijing: Peking University Press(北京: 北京大学出版社),1997. [3] LIU Zhong-min(刘忠敏).General Rule of Modern Instrument Analytical Method and Metrology Examine Regulation(现代分析仪器分析方法通则及计量检定规程).Beijing: Science Technology Reference Press(北京: 科学技术文献出版社),1997.797. [4] HAN Yong-zhi(韩永志).Handbook of Reference Material(标准物质手册).Beijing: Chinese Metrology Press(北京: 中国计量出版社),1999. [5] HUANG Ben-li(黄本立).Spectroscopy and Spectral Analysis(光谱学与光谱分析),2000, 20(2): 129. [6] CHEN Xiao-bo, SONG Zeng-fu(陈晓波,宋增福).Spectroscopy and Spectral Analysis(光谱学与光谱分析),2003, 23(3): 426.
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