| 光谱学与光谱分析 |
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| Pretreatment of Lead-Antimony Alloy and Determination of Antimony and Selenium Using ICP-AES |
| FANG Yi-wen, SONG Yi-bing, SUN Chang-yong, XUE Liang, YU Lin |
| Department of Chemistry, Shantou University, Shantou 515063, China |
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Abstract The sample was obtained from original sample using “sawing method” and was dissolved with a mixed solvent of nitric acid and tartaric acid. After the sample solution was pretreated with a series of methods, Sb and Se were determined by inductively coupled plasma atomic emission spectrometry (ICP-AES). The results show that the recovery of standard addition of Sb was 96.2% and that of Se was 92.1%, and that the relative standard deviations(n=11)were smaller than 3.56%. The method is efficient, accurate and easy to operate, and has been applied to the determination of Sb and Se in Pb-Sb alloy products with satisfactory results.
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Received: 2005-01-06
Accepted: 2005-04-25
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Corresponding Authors:
FANG Yi-wen
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| Cite this article: |
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FANG Yi-wen,SONG Yi-bing,SUN Chang-yong, et al. Pretreatment of Lead-Antimony Alloy and Determination of Antimony and Selenium Using ICP-AES [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(03): 561-563.
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https://www.gpxygpfx.com/EN/Y2006/V26/I03/561 |
[1] DONG Bao-guang, ZHANG Qiu-dao, MU Jun-jiang，et al(董保光，张秋道，穆俊江, 等). Material Science and Technology(材料科学与工艺), 1995, 3(1): 67.
[2] Matucha K H, DING Dao-yun, et al(马图哈 K H，丁道云, 等). Structure and Properties of Nonferrous Alloys(非铁合金的结构与性能). Beijing: Science Press(北京: 科学出版社), 1998. 69.
[3] China’s National Standard, GB-4103-83(中国国家标准, GB-4103-83). Beijing: China’s National Standard Press(北京: 中国标准出版社), 1998.
[4] LI Song-rui(李松瑞). Pb and Pb Alloy(铅及铅合金). Changsha: Central South University of Technoloyg Press(长沙: 中南工业大学出版社). 1996. 499.
[5] LI Ai-ling, ZHENG Gui-lin, JIANG Wan-chao(李爱玲，郑桂林，蒋万超). Battery(电池), 1994, 19(1): 37.
[6] HE Hai-cheng, ZHANG Guang-xia, HUANG Zhi-rong, HE Xi-wen, HUANG Xin-ping, YANG Ti-shao(何海成，张光霞，黄志荣, 何锡文, 黄新平, 杨体绍). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2004, 24(7): 887.
[7] ZHONG Zhi-guang, BIAN Qun-zhou, ZHENG Jian-guo, CHEN Pei-ling, LIU Chong-hua(钟志光，卞群洲，郑建国, 陈佩玲, 刘崇华). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2002，22(1)：83.
[8] ZHAO Ai-dong, CHEN Hong-li(赵爱东，陈洪利). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2001, 21(5): 647.
[9] WANG Qing-ming, HE Hong-xi(王清明，贺鸿喜). Battery(电池), 1995, 20(1): 26.
[10] GU Yi-dong(顾翼东). Chemical Dictionary(化学词典). Shanghai: Shanghai Dictionary Press(上海: 上海辞书出版社), 1989.
[11] FANG Yi-wen, JIA Li, YU Lin, SONG Yi-bing, SUN Chang-yong(方奕文，贾 丽，余 林, 宋一兵, 孙长勇). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2003, 23(1): 73.
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