Abstract:A developing technique, laser ablation and fast pulse discharge plasma spectroscopy technique (LA-FPDPS), was used for the first time to analyze the Sn concentration in soil. The peak intensity of Sn (284.0 nm) line from soil plasma emission was greatly enhanced in comparison with using the traditional single pulse (SP) LIBS system. Using the technique, calibration curve of Sn in soil was derived. The limit of detection (LOD) for Sn in soil was reduced to be 0.16 μg·g-1. The value is significantly improved compared with the results reported in literature when using LIBS technique, which usually was between 8.2 to 54 μg·g-1 depending on the experimental condition, indicating that this technique possibly will be useful for rapid quantitative elemental analysis in soil.
李科学,周卫东*,沈沁梅,郑 毅,李霞芬,钱惠国,邵 杰 . 激光烧蚀-快脉冲放电等离子体光谱技术分析土壤中的Sn[J]. 光谱学与光谱分析, 2011, 31(08): 2249-2252.
LI Ke-xue, ZHOU Wei-dong*, SHEN Qin-mei, ZHEN Yi, LI Xia-fen, QIAN Hui-guo, SHAO Jie . Laser Ablation and Fast Pulse Discharge Plasma Spectroscopy Analysis of Sn in Soil . SPECTROSCOPY AND SPECTRAL ANALYSIS, 2011, 31(08): 2249-2252.
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