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A Comparative Study of Infrared Fingerprint on Extracts of Three Kinds of from Onchidium struma |
SHI Yan-mei, GU Bing-ning, YAO Li-xiang, SHEN He-ding* |
National Demonstration Center for Experimental Fisheries Science Education, Shanghai Universities Key Laboratory of Marine Animal Taxonomy and Evolution, Centre for Research on Environmental Ecology and Fish Nutrion (CREEFN) of the Ministry of Agriculture, Shanghai Ocean University, Shanghai 201306, China |
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Abstract Aiming to establish a comprehensive and rapid method to discriminate Onchidium struma(O. struma) quality from different regions, this research has established it’s three extract fingerprints in absolute ethyl alcohol, chloroform and ethyl acetate adoptd the infrared spectrometry (IR),and the information of infrared spectra of O. struma samples originated from 6 regions has been collected. Automatic baseline correction and automatic optimized smoothness of Nicolet 5700 infrared spectrometer intelligence system are applied to optimize the IR fingerprint. Combining with the OPUS software. The results showed that,the three extract fingerprints function as a evaluation index to discriminate O. struma from different regions or different quality. The characteristic absorption peaks of three extracts has been contrasted, reflecting that the IR fingerprint spectra of ethyl acetate extract can reflect more abundant chemical composition information. The three extracts have different level and angle for identification of O. struma. Dual-indexes sequential analysis comparison shows that infrared spectrum of chloroform extract can reflect different habitats and different process mode O. struma differences: It has shown ShangHai(SH)and NingDe(ND), WenZhou(WZ)and XiaMen(XM)were the region closer samples with higher common peak ratio(≥63.4)and lower variant peak ratio(≤38.5);Sample SH and YueNan(YN),YanCheng(YC)and XiaMen(XM)from the farther regions,were significant disparity with lower common peak ratio(≤40.9%)and higher variant peak ratio(≥50.0%);In addition,sample XM and YN from closer region but have different process mode, which resulted in much lower common peak ratio(38.1%)and much higher variant peak ratio(125.0%), To sum up, the quality control of aquatic products is a major concern for both the health authorities and the public, considering that current commercially available O. struma are acquired in natural way, acquiring area and time leading to the vital difference of their quality. The method of chloroform extracts dual-index sequence analysis could be used exactly and conveniently in qualitative evaluation of different region samples, and clarified the similarity level among different areas, also applied the quality evaluation of O. struma.
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Received: 2017-03-20
Accepted: 2017-07-12
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Corresponding Authors:
SHEN He-ding
E-mail: hdshen@shou.edu.cn
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[1] Sun Bianna, Chen Cheng, Shen Heding, et al. Molluscan Research, 2014, 34(1): 62.
[2] HE Shi-shui, WU Xu-gan, TENG Wei-ming, et al(贺诗水, 吴旭干, 滕炜鸣, 等). Oceanologia et Limnologia Sinica(海洋与湖沼), 2012, (4): 761.
[3] SUN Bian-na, SHEN He-ding, WU Hong-xi, et al(孙变娜, 沈和定, 吴洪喜, 等). Natural Product Research and Development(天然产物研究与开发), 2014, (7): 987.
[4] Sun Bianna, Shen Heding, Wu Hongxi, et al. Tropical Journal of Pharmaceutical Research,2014, 13(12): 2071.
[5] YAO Li-xiang, YANG Tie-zhu, ZHU Min, et al(姚理想, 杨铁柱, 朱 敏, 等). Journal of Fisheries of China(水产学报), 2016, 7: 1060.
[6] Wu Xin, Wang Dongfeng, Shen Heding, et al. Conservation Genetics Resources, 2016,8(1): 43.
[7] Sun Bianna, Wei Luanluan, Shen Heding, et al. Mitochondrial DNA Part A, 2016, 27(5): 3075.
[8] HUANG Li-ping, WU Jing(黄丽萍,吴 静). China Journal of Chinese Materia Medica(中国中药杂志),2011,36(11):1441.
[9] WANG Yan, WANG Bin, XU Yin-feng, et al(王 燕, 王 斌, 徐银峰, 等). Journal of Chinese Institute of Food Science and Technology(中国食品学报),2013,13(1): 178.
[10] CHEN Yong, WEI Hou-chao, WEI Tao, et al(陈 勇, 魏后超, 韦 韬, 等). China Journal of Traditional Chinese Medicine and Pharmacy(中华中医药杂志), 2015, 30(3): 709.
[11] YUAN Tian-jun, WANG Yuan-zhong, ZHAO Yan-li, et al(袁天军, 王元忠, 赵艳丽, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2011, 31(8): 2161.
[12] CHENG Yun-qing, LIU Jian-feng, LIU Qiang, et al(程云清,刘剑锋,刘 强,等). Journal of Nanjing Agricultural University(南京农业大学学报),2011,34(5):155.
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