| 光谱学与光谱分析 |
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| Determination of Fe, Al and Ni in ZrO2 by Electrothermal Vaporization ICP-AES |
| CHEN Shi-zhong |
| Key Laboratory, Wuhan Polytechnic University, Wuhan 430023, China |
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Abstract A novel method for the analysis of ZrO2 powder via in-situ separation of the matrix from the analytes is described, based on the use of a polytetrafluorethylene (PTFE) emulsion as a chemical modifier. The main affecting factors, including the flow rate of carrier gas and auxiliary carrier gas, ashing temperature and time, matrix concentration, signal record time, and vaporization temperature and time, were investigated systematically. Under the optimum operating conditions, the detection limits (DL) of analytes vary from 4.2 ng·mL-1 (Al) to 11 ng·mL-1 (Fe). The relative standard deviations (RSDs) are 3.1%-4.9%.
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Received: 2004-12-16
Accepted: 2005-04-25
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Corresponding Authors:
CHEN Shi-zhong
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| Cite this article: |
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CHEN Shi-zhong. Determination of Fe, Al and Ni in ZrO2 by Electrothermal Vaporization ICP-AES [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(10): 1697-1699.
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| URL: |
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https://www.gpxygpfx.com/EN/Y2005/V25/I10/1697 |
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