| 光谱学与光谱分析 |
|
|
|
|
|
| Development of a High Resolution Simultaneous Microwave Plasma Torch Spectrometer |
| JIANG Jie1,HUAN Yan-fu1,JIN Wei2,FENG Guo-dong1,FEI Qiang1,CAO Yan-bo1,JIN Qin-han1,2* |
1. College of Chemistry, Jilin University, Jilin Province Research Center for Engineering and Technology of Spectral Analytical Instruments, Changchun 130023, China
2. Research Center for Analytical Instrumentation, Zhejiang University, Hangzhou 310058, China |
|
|
|
|
Abstract A unique high resolution simultaneous microwave plasma torch (MPT) atomic emission spectrometer was developed and studied preliminarily. Some advanced technologies were applied to the spectrometer, such as echelle grating, UV-intensified CCD array detector, adjustable microwave generator, and water cooling system for the generator, etc. The detection limits of the spectrometer for some elements were determined, the spectral resolution and pixel resolution of the spectrometer were calculated, and an analysis of a practical sample was carried out. The preliminary results demonstrate that such simultaneous spectrometer has advantages of saving sample and time, possessing high sensitivity and resolution, and low-cost for the purchase and maintenance. Taking analytical figures of merit into consideration, the high resolution simultaneous MPT spectrometer will have extended application areas and greater competition potential as compared with sequential MPT spectrometers.
|
|
Received: 2006-05-15
Accepted: 2006-09-30
|
|
|
|
Corresponding Authors:
JIN Qin-han
E-mail: qhjin@jlu.edu.cn
|
|
| Cite this article: |
|
JIANG Jie,HUAN Yan-fu,JIN Wei, et al. Development of a High Resolution Simultaneous Microwave Plasma Torch Spectrometer[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(11): 2375-2379.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2007/V27/I11/2375 |
[1] Evans E H, Day J A, Palmer C D, et al. J. Anal. Atom. Spectrom., 2005, 20: 562.
[2] Evans E H, Day J A, Fisher A, et al. J. Anal. Atom. Spectrom., 2004, 19: 775.
[3] GONG Zhen-bin, LIANG Feng, YANG Peng-yuan, et al(弓振斌、梁 枫、杨原，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2002, 22(1): 63.
[4] ZHANG Shao-yu, HUANG Ben-li, GONG Zhen-bin(张绍雨，黄本立，弓振斌). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2001, 21(5): 632.
[5] HUANG Ben-li(黄本立). Journal of Guangxi Normal University(Natural Science Edition)(广西师范大学学报·自然科学版), 2003, 21(z3): 1.
[6] Bacon J R, Linge K L, Vaeck L V. J. Anal. Atom. Spectrom., 2005, 20: 763.
[7] Jin Qinhan, Zhu Chu, Borer M W et al. Spectrochimica Acta, 1991, 46(B):417.
[8] Kim J H, Hong Y C, Shin D H, et al. Plasma Science, 2006, 34(6): 2600.
[9] Foltin V, Lestinska L, Machala Z. Czechoslovak Journal of Physics, 2006, 56: B712.
[10] Shin D H, Bang C U, Hong Y C, et al. Materials Chemistry and Physics, 2006, 99(2-3): 269.
[11] Yubero C, Garcia M C, Calzada M D. Spectrochimica Acta (Part B), 2006, 61(5): 540.
[12] ZHOU Jian-guang, PENG Zeng-hui, HUAN Yan-fu, et al(周建光，彭增辉，郇延富, 等). Chem. J. Chinese Universities(高等学校化学学报), 2002, 23(7): 1273. |
| [1] |
LI Yu-tang1, WANG Lin-zhu1, 2*, LI Xiang3, WANG Jun1. Characterization and Comparative Analysis of Non-Metallic Inclusions in Zirconium Deoxidized Steel[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2916-2921. |
| [2] |
DENG Xian-ze1, 2, DENG Xi-guang1, 2*, YANG Tian-bang1, 2, CAI Zhao3, REN Jiang-bo1, 2, ZHANG Li-min1, 2. To Reveal the Occurrence States and Enrichment Mechanisms of Metals in Modules From Clarion-Clipperton Zone in Eastern Pacific by High
Resolution Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(08): 2522-2527. |
| [3] |
HUANG Han1, CHEN Hong-yan2*, LI Xiao-lu1, LIU Jia-hao1, ZHAO Yong-jia2, CHEN Liang3. Calculation and Study of Methane Absorption Coefficient at Variable Pressure and Temperature Under 3 016.49 cm-1 Wave Number[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(08): 2462-2468. |
| [4] |
FANG Xue-jing1, 2, 3, LUO Hai-yan1, 3, SHI Hai-liang1, 3, LI Zhi-wei1, 3, HU Guang-xiao1, 2, 3, JIN Wei1, 2, 3, ZHANG Ji-cheng1, 2, 3, XIONG Wei1, 2, 3*. High-Resolution Scattered Radiation Measurement in Ultraviolet Band Based on Spatial Heterodyne Spectroscopy Technique[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(02): 357-362. |
| [5] |
ZHANG Rui1,2, ZHU Ji-wei1, LIU Jian-li1,2, CUI Ji-cheng1, LI Xiao-tian1, Bayanheshig1. Study on the Laser-Induced Plasma Spectroscopy Based on the Echelle Spectrometer[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(05): 1605-1609. |
| [6] |
LIU Xiang-lei1,2, LIU Yang-yang1*, FANG Yu1, PEI Lin-lin1, Lü Qun-bo1. Optical Design of Large Relief Large Relative Apertureand High Resolution Modified Dyson Imaging Spectrometer[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(12): 3908-3912. |
| [7] |
SHEN Chun-yang1, 2, CUI Ji-cheng1*, SUN Ci1, WANG Wei1, 2, CHEN Jian-jun1, 2, LI Xiao-tian1. A Detection System Design of Echelle Diffraction Efficiency and Stray Coefficient[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(08): 2603-2609. |
| [8] |
HUANG Yuan-shen1, 2, DONG Cheng-cheng1, 2*, HUANG Yun-bai1, 2, SHENG Bin1, 2, ZHOU Hong-yan1, 2, SUN Le1, 2, YANG Hai-ma1, 2, ZHANG Da-wei1, 2 . Research on Straightness Error Compensation of Grating Ruling Machine [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(03): 946-951. |
| [9] |
YIN Lu1, 2，Bayanheshig1*，YAO Xue-feng1，CUI Ji-cheng1，ZHU Ji-wei1，ZHANG Rui1, 2. Algorithm for Background Removal in Spectral Image of Echelle Spectrometer[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2016, 36(06): 1925-1929. |
| [10] |
WU Rui1, ZHANG Yin-xin1*, HUANG Zhan-hua1, YANG Huai-dong2, JIN Guo-fan2 . Detection System for High-Resolution and Broadband-2D Spectrogram [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2016, 36(04): 1249-1254. |
| [11] |
WANG Fu-tao1，3, WANG Shi-xin1, ZHOU Yi1*, WANG Li-tao1, YAN Fu-li1, LI Wen-jun1，2, LIU Xiong-fei1，2 . High Resolution Remote Sensing Monitoring and Assessment of Secondary Geological Disasters Triggered by the Lushan Earthquake [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2016, 36(01): 181-185. |
| [12] |
ZHAO Wen-zhi1, LUO Li-qun1, 2, GUO Zhou1, YUE Jun1, YU Xue-ying3, LIU Hui1, WEI Jing4 . Road Extraction in Remote Sensing Images Based on Spectral and Edge Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(10): 2814-2819. |
| [13] |
CHEN Qiang1, 2, CHEN Yun-hao1, 2*, JIANG Wei-guo1, 3 . The Change Detection of High Spatial Resolution Remotely Sensed Imagery Based on OB-HMAD Algorithm and Spectral Features[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(06): 1709-1714. |
| [14] |
YIN Lu1, 2, Bayanheshig1*, CUI Ji-cheng1, YANG Jin1, 2, ZHU Ji-wei1, YAO Xue-feng1 . An Effective Wavelength Detection Method Based on Echelle Spectra Reduction [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(03): 850-855. |
| [15] |
YAN Li, GONG Yi-long*, ZHANG Yi, DUAN Wei . Application of Optical Flow Dynamic Texture in Land Use/Cover Change Detection [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2014, 34(11): 3056-3061. |
|
|
|
|
