光谱学与光谱分析 |
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Fluorometric Determination of Fructose in the Presence of Glucose Using Zirconyl Chloride-Ammonium Chloride |
TONG Lei1,WANG Yan-xin1,ZHAO Zhong-yi2,JIN Ji-hong2,GUO Xiao-hui2 |
1. School of Environmental Studies and Key Laboratory of Biogeology and Environmental Geology of Chinese Ministry of Education, China University of Geosciences, Wuhan 430074, China 2. School of Material Science and Chemistry Engineering, China University of Geosciences, Wuhan 430074, China |
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Abstract According to the principle that Zn(OH)+ produced by ZrOCl2 upon hydrolysis in water can react to form a fluorescent derivative with fructose, a method for the quantitative determination of fructose has been proposed. The fluorescence of the derivative enhanced at 408 nm in NH4Cl medium has a direct ratio with fructose in the linear range of 0.5-25 μg·mL-1. When reaction conditions such as a temperature of 70 ℃ and a time of 15 min are used, the detection limits is 0.071 mg·mL-1. The proposed method was also applied successfully to the determination of fruit, satisfaction with high accuracy and good reproduction.
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Received: 2006-05-10
Accepted: 2006-08-20
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Corresponding Authors:
TONG Lei
E-mail: tonglei0710@163.com
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Cite this article: |
TONG Lei,WANG Yan-xin,ZHAO Zhong-yi, et al. Fluorometric Determination of Fructose in the Presence of Glucose Using Zirconyl Chloride-Ammonium Chloride[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(11): 2313-2316.
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URL: |
https://www.gpxygpfx.com/EN/Y2007/V27/I11/2313 |
[1] Hirotaka Kakita, Hiroshi Kamishima, Katsuo Komiya, et al. Journal of Chromatography A, 2002, 961: 77. [2] GENG Yue, ZHAO Xiang-xuan, HUA Yi-shan, et al(耿 越, 赵相轩, 花义山, 等). Journal of Food Science(食品科学), 2002, 23(1): 114. [3] HASEN Qimuge, HE Feng-ga(哈森其木格, 贺锋嘎). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2002, 22(3): 446. [4] HU Bin, CHEN Da, SU Qing-de(胡 斌 ,陈 达, 苏庆德). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2005, 25(7): 1049. [5] Danielson N D,Heenan C A,Haddadian F, et al. Microchemical Journal, 1999, 63(3): 405. [6] WANG Xi-cheng(王希成编著). Biochemistry(生物化学). Beijing: Tsinghua University Press(北京:清华大学出版社), 2001. [7] GUO Zhen-chu, HAN Liang, HU Bo, et al(郭振楚, 韩 亮, 胡 博,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2002, 22(6): 963. [8] JIANG Yu-cheng, WANG Jian-ji, ZHUO Ke-lei, et al(蒋育澄, 王键吉, 卓克垒, 等). Chemical Journal of Chinese Universities(高等学校化学学报), 2003, 24(10): 1842. [9] Valerie Ralsimba, Jose Manuel Garcia Fernandez, Jacquce Defaye, et al. Journal of Chromatography A, 1999, 844: 283. [10] Eduardo A, Borges da Silva, Antonio A, et al. Chemical Engineering Journal, 2006, 118: 168. |
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