| 光谱学与光谱分析 |
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| Determination of Sb and Bi in 24 International Geological Reference
Materials by Using Pressurized Acid Digestion-ICP-MS |
| HU Zhao-chu1,2,GAO Shan1,2,LIU Xiao-ming2,YUAN Hong-lin2,LIU Ye2,DIWU Chun-rong2 |
1. State Key Laboratory of Geological Processes and Mineral Resources, China University of Geosciences, Wuhan 430074, China
2. State Key Laboratory of Continental Dynamics, Northwest University, Xi’an 710069, China |
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Abstract The authors studied in detail the memory effect of Bi, Sb, As and Te in ICP-MS. The produced memory effects of these element were in the order of Bi>Sb>Te>As. Bi was seriously adsorbed by the polypropylene sample storing bottle and the sample introduction system in the low nitric acid medium (0.01%-1% HNO3). The washout effect of 0.1% HF was found to be better than those of 6% HNO3 and 0.1% HClO4. Under the given experiment conditions, the instrumental limit of detection was 0.001 and 0.000 1 ng·mL-1 for Sb and Bi, respectively. The authors report the determination of Sb and Bi in 24 international geological reference materials by using pressurized acid digestion-ICP-MS (including AGV-2, BHVO-2, BCR-2, etc.). Most of the results were found to be in reasonable agreement with the reported values in the literature. The authors’ determined values of Sb for GSR-1(granite; 0.30 μg·g-1) and JP-1(peridotite; 0.045 μg·g-1) are obviously higher than those reported values. This is attributed to the efficient pressurized acid digestion, which is generally much more efficient than conventional wet digestions for insoluble minerals.
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Received: 2006-09-08
Accepted: 2006-12-16
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Corresponding Authors:
HU Zhao-chu
E-mail: zchu@vip.sina.com
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| Cite this article: |
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HU Zhao-chu,GAO Shan,LIU Xiao-ming, et al. Determination of Sb and Bi in 24 International Geological Reference
Materials by Using Pressurized Acid Digestion-ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(12): 2570-2574.
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| URL: |
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https://www.gpxygpfx.com/EN/Y2007/V27/I12/2570 |
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