光谱学与光谱分析 |
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Surfactant-Assisted Solid-Phase Synthesis and Spectral Characterization of Silver Iodide Nanowire Bundles |
LIU Ying, FENG Jin-chao, LI Jin-shu |
College of Life and Environmental Science, Minzu University of China, Beijing 100081, China |
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Abstract In the present paper, AgNO3 and KI were used as raw materials synthesize silver iodide nanowire bundles in the condition of nonionic surfactant polyethylene glycol (PEG-400) at room temperature. XRD, TEM and SEM techniques were used to characterize the silver iodide structure and morphology. The results indicated that the product was one-dimensional silver iodide nanowire bundles with diameters of 80~100 nm and lengths of 20 μm, and the length-diameter ratio was greater than 200. In the forming process of silver iodide nanowire bundles, PEG-400 surfactant was used as soft template agent, which induced the product nanocrystalline along a particular direction and directional orderly growth so as to generate nanowire bundles. This method with a simple operation and low cost eliminated the influence of water on the reaction process.
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Received: 2011-05-30
Accepted: 2011-08-16
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Corresponding Authors:
LIU Ying
E-mail: liuying430@yahoo.com.cn
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