| 光谱学与光谱分析 |
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| The Qualitative Analysis Method of the Dissolved Organic Matter (DOM) for ABS Wastewater |
| LAI Bo1, 2, ZHOU Yue-xi2*, SONG Yu-dong2, XI Hong-bo2, SUN Li-dong3, CHEN Jia-yun3 |
1. College of Water Sciences, Beijing Normal University, Beijing 100875, China
2. Research Center of Water Pollution Control Technology, Chinese Research Academy of Environment Sciences, Beijing 100012, China
3. Department of Environment Protection and Safety of Jilin Petrochemical Company, Ltd., PetroChina, Jilin 132021, China |
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Abstract The dissolved organic matter (DOM) of acrylonitrile-butadiene-styrene (ABS) resin wastewater was qualitatively analysed by gas chromatography with mass spectrometry(GC-MS), Fourier transform infrared spectrometer(FTIR) and three-dimensional excitation–emission matrix (EEM) fluorescence spectroscopy. The detected results shows that the GC-MS qualitatively analysed 21 dissolved organic pollutants, such as acetophenone, styrene, alpha, alpha-dimethyl-benzenemethanol, 3,3′-oxybis-propanenitrile, 3,3′-iminobis-propanenitrile, 3,3′-thiobis-propanenitrile, 3-(dimethylamino)-propanenitrile and 2-propenenitrile. The results of Fourier transform infrared spectrometer (FTIR) and three-dimensional excitation-emission matrix (EEM) fluorescence spectroscopy could examine and certify the accuracy and integrity for the qualitative analysis of GC-MS. The results of this study provides an important guiding role for the development of wastewater treatment process.
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Received: 2010-05-02
Accepted: 2010-08-09
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Corresponding Authors:
ZHOU Yue-xi
E-mail: zhouyuexi@263.net
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[1] WANG Bin(王 彬). Refining and Chemical Industry(炼油与化工), 2008, 19(2): 11.
[2] LU Shu-lai, LUO Li-hong, HE Lin (陆书来, 罗丽宏, 何 琳). Science & Technology in Chemical Industry (化工科技), 2003, 11(5): 55.
[3] SU Hong, ZHANG Xiao-jie, WANG De-yi(苏 宏, 张晓杰, 王德义). Environmental Engineering(环境工程), 2004, 22(4): 91.
[4] ZHAO Dong-feng, LIU Fa-qiang, JIANG Wen-qing(赵东风, 刘发强, 蒋文庆). Environmental Protection of Oil & Gas Fields (油气田环境保护), 2003, 13(2): 8.
[5] Oxana Botalova, Jan Schwarzbauer, Tom Frauenrath, et al. Water Research, 2009, 43: 3797.
[6] Wang Xiao-yi, Wei Shi, Jiang Wu, et al. Journal of Environmental Sciences, 2010, 22(2): 297.
[7] Longbottom J E, Lichtenberg J J. Methods for Organic Chemical Analysis of Municipal and Industrial Wastewater. EPA-600/4-82-057, 1982.
[8] An Ying, Wang Zhiwei, Zhichao Wu，et al. Chemical Engineering Journal, 2009, 155: 709.
[9] Champagne Pascale, Li Caijian. Bioresource Technology, 2009, 100: 5700.
[10] Zainab D, Valeria D, Provenzano MR, et al. Journal of Hazardous Materials, 2009, 164: 1281.
[11] Li WH, Sheng GP, Liu X W, et al. Water Research 2009, 42: 3173.
[12] WU Hao, ZHU Tuo, KONG Yan, et al(武 浩, 朱 拓, 孔 艳，等). Acta Optica Sinica(光学学报), 2010, 30(1): 262.
[13] HAO Rui-xia, CAO Ke-xin, DENG Yi-wen, et al(郝瑞霞, 曹可心，邓亦文, 等). Journal of Instrumental Analysis(分析测试学报), 2007, 26(6): 789.
[14] ZHAO Nan-jing, LIU Wen-qing, CUI Zhi-cheng, et al(赵南京, 刘文清, 崔志成，等). Acta Optica Sinica(光学学报), 2005, 25(5): 687.
[15] Sheng G P, Yu H Q. Water Research, 2006, 40: 1233.
[16] Huo Shouliang, XI Beidou, YU Haichan, et al. Journal of Environmental Sciences, 2008, 20(4): 492.
[17] Wang Z W, Wu Z C, Tang S J. Water Research, 2009, 43: 1533.
[18] CUI Xiang, GUO You-jing, CHANG Min(崔 香, 郭幼敬, 常 敏). Journal of Anhui Agricultural Sciences(安徽农业科学). 2009, 37(24): 11351.
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