光谱学与光谱分析 |
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Confocal Micro Raman Spectroscopy for the Identification of the Binder Used in Chinese Painted Cultural Relics |
HUANG Jian-hua1,2,YANG Lu3,4,5*,YU Shan-shan3 |
1. Key Scientific Research Base of Ancient Polychrome Pottery Conservation of State Administration of Culture Heritage, Xi’an 710600, China 2. The Museum of the Terracotta and Horses of Qin Shihuang, Xi’an 710600, China 3. College of Culture Heritage and History, Northwest University, Xi’an 710069, China 4. Key Scientific Research Base on the Stone and Brick Materials’ Conservation of State Administration of Cultural Heritage, Xi’an 710061, China 5. The Institute of Culture Heritage and Archaeology, Northwest University, Xi’an 710069, China |
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Abstract For identification of the binder used in Chinese painted cultural relics, the micro-Raman spectroscopy was used to test the pig skin glue, pig bone glue, egg yolk, egg white and peach glue which were commonly used as binder in the relics. The difference between proteinaceous binder and peach glue are distinctly. According to the analysis of their Raman spectrum, the vibrations located at 1 463 and 1 088 cm-1are the features of peach glue. The four kinds of proteinaceous binder also have respective features of their own, although there are many common features in their Raman spectrum. The vibration of 1 737 cm-1 is the feature of pig skin glue, and tie pig bone glue has the feature of vibration located in 962 cm-1. The vibrations of 1 535~1 555 and 759 cm-1 are the features of egg, including egg yolk and egg white. And the egg yolk has another vibration located at 1 749 cm-1 which is different from egg white. It was concluded that the binder can be identified based on the features of Raman spectrum.
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Received: 2010-04-16
Accepted: 2010-07-22
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Corresponding Authors:
YANG Lu
E-mail: yanglu@nwu.edu.cn
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[1] Ling H, Maiqian N, Chiavari G, et al. Microchemical Journal, 2007, 85: 347. [2] Bonaduce I, Blaensdorf C, Dietemann P, et al. Journal of Cultural Heritage, 2008, 9: 103. [3] HE Qiu-ju, WANG Li-qin(何秋菊, 王丽琴). China Adhesives(中国胶粘剂), 2007, 16(3): 19. [4] SU Bo-min, Tetuo Sinkei, HU Zhi-de, et al(苏伯民, 真贝哲夫, 胡之德, 等). Dunhuang Research(敦煌研究), 2005, (4): 57. [5] Checa-Moreno R, Manzanob E, Miron G. Talanta, 2008, 75(3): 697. [6] Keulen H. International Journal of Mass Spectrometry, 2009, 284(2): 162. [7] Bonaduce I, Cito M, Colombini M P. Journal of Chromatography A, 2009, 1216(32): 5931. [8] Nevin A, Melia J L, Osticioli I. Journal of Cultural Heritage, 2008, 9(2): 154. [9] Colombini M P, Modugno F. Journal of Separation Science, 2004,27: 147. [10] Domenech-Carb M T. Analytica Chimica Acta, 2008, 621: 109. [11] ZHAO Hong-xia, GAN Fu-xi(赵虹霞, 干福熹). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2009, 29(11): 2989. [12] Nevin A, Osticioli I, Anglos D, et al. Analytical Chemistry, 2007, 79(16): 6143. [13] Nevin A, Osticioli I, Anglos D,et al. Journal of Raman Spectroscopy, 2008, 39(8): 993. [14] Osticioli I, Nevin A, Anglos D, et al. Journal of Raman Spectroscopy, 2008, 39(2): 307. [15] JIA Si-xie(贾思勰). Qi Min Yao Shu(齐民要术). Xi’an: San Qin Press(西安: 三秦出版社),1999. 506. [16] WANG Gui-wen, PENG Li-xin, YAO Hui-lu, et al(王桂文, 彭立新, 姚辉璐, 等). Acta Laser Biology Sinica(激光生物学报), 2008, 17(2): 186. [17] ZHANG Tao, LI Jun-ke, LIU Zhu, et al(张 涛, 李军科, 刘 柱, 等). Journal of Anhui Agriculture Science(安徽农业科学), 2007, 35(33): 10563. [18] Harada Makoto, YANG Xian-de(原田一诚, 杨先德). Journal of Medical Molecular Biology(医学分子生物学杂志), 1981, 3(2): 84. [19] SUN Su-qin, ZHOU Qun, ZHANG Xuan, et al(孙素琴, 周 群, 张 宣, 等). Chinese Journal of Analytical Chemistry(分析化学), 2000, 28(2): 211.
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