| 光谱学与光谱分析 |
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| Effect of High Performance Liquid Chromatographic Instrument System on the Analysis of Erythromycin A Oxime |
| SUN Jing-guo1, 2，YAO Guo-wei1，OU Yu-xiang3 |
1. School of Life Science and Technology, Beijing Institute of Technology, Beijing 100081, China
2. Chemistry College of Hebei Normal University, Shijiazhuang 050091, China
3. School of Material Science and Engineering，Beijing Institute of Technology, Beijing 100081, China |
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Abstract A HPLC chromatography for the determination of erythromycin A oxime and relative compounds was studied, amd the effect of chromatography systems including a HITACHI L-7100, a Shimadzu LC-6A, a WatersTM 474 and relative columns was analyzed. It was revealed that different HPLC apparatus and columns have obvious impact on the peak separation and retention time under the general chromatographic condition. The suitable chromatographic conditions for several different chromatography systems were summarized with good linear relationship，which is very significant to the quality control of erythromycin A oxime and relative compounds.
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Received: 2003-03-28
Accepted: 2003-08-06
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Corresponding Authors:
SUN Jing-guo
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| Cite this article: |
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SUN Jing-guo,YAO Guo-wei,OU Yu-xiang. Effect of High Performance Liquid Chromatographic Instrument System on the Analysis of Erythromycin A Oxime [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(09): 1148-1150.
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http://www.gpxygpfx.com/EN/Y2004/V24/I09/1148 |
[1] Clark Ｒ F, Ma Z Ｋ, Wang S Y, Griesgraber G, Tufano M, Yong H, Li L P, Zhang X L, Nilius A M, Chu D T W. Bioorg. Medi.1 Chem. Lett.，2000, 10: 815.
[2] SUN Jing-guo, LIANG Jian-hua, DENG Zhi-hua, YAO Guo-wei(孙京国, 梁建华，邓志华，姚国伟). Chin. J. Org. Chem.(有机化学), 2002, 22(12)：951.
[3] Morimoto S, Adachi T, Matsunaga T, Kashimura M, Watanabe Y, Sota K. U. S. Patent, 6342590 B1，2002.
[4] SHI Yan, QIAN Guo-hua, LIANG Jian-hua, YAO Guo-wei(石 岩, 钱国华, 梁建华, 姚国伟). Chinese J. of Chem.(合成化学), 2001, 9(2): 172.
[5] Robert Ｒ. Willkening. USP 5912331，1999.
[6] Harang Ｖ, Westerlund D. Chromatographia，1999，50(9-10): 525.
[7] Moheb M N, Terry J T. J. Liq. Chrom. rel. Technal., 1997 20(4): 553.
[8] Chieko T, Hisakazu O, Erika H, Hajime K, Hitoshi S, Tatsuji I. J. Chrom. B，2000，783: 405.
[9] SUN Jing-guo(孙京国). Acad. Conf. Chin. Asso. Sci. and Tech. in 2001，Chanｇ Chｕn(2001中国科技年会, 长春)，2001. 1524.
[10] SUN Jing-guo，YAO Guo-wei(孙京国, 姚国伟). Chinese J. of Anal. Chem.(分析化学)，2003，31(9): 1089.
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