| 光谱学与光谱分析 |
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| Extraction and Analysis of Sargassum Hemiphyllum Polysaccharides |
| MENG Qing-yong, LIU Zhi-hui, XU Mei-yi, DONGYE Guang-zhi |
| Analysis Center of Guangdong Medical College, Zhanjiang 524023, China |
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Abstract Sargassum hemiphyllum polysaccharides(SHP) was extracted by thermal water method and the physical and chemical characters, the extraction rate, contents, compositions of SHP was studied. The result showed that SHP was ashen powder, water-soluble, insoluble in organic solvents. The reaction of iodide-potassium iodide was negative to evaluate that SHP was nonstarch polysaccharides. Extraction rate was 7.04% and the content of polysaccharides was 82.9%. Ultraviolet spectrum showed that there were little DNA and protein. Infrared spectroscopy showed that SHP was main pyrano polysaccharides and had β-linked glycopolysaccharides in molecule structure of SHP. Thin layer chromatography traced that SHP could be xylan. The results indicated that the extract was not only polysaccharides but also higher purify and the method was high efficiency.
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Received: 2003-10-08
Accepted: 2004-01-16
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Corresponding Authors:
MENG Qing-yong
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| Cite this article: |
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MENG Qing-yong,LIU Zhi-hui,XU Mei-yi, et al. Extraction and Analysis of Sargassum Hemiphyllum Polysaccharides [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(12): 1560-1562.
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| URL: |
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https://www.gpxygpfx.com/EN/Y2004/V24/I12/1560 |
[1] SHENG Jia-rong, ZENG Ling-hui, QＵ Chun et al(盛家荣，曾令辉，瞿 春等). Journal of Guangxi Teachers College(Natural Science Edition)(广西师范学院学报·自然科学版)，1999，16(4)：49.
[2] SUN Dong-ping, PAN Feng, SHI Xiao-li et al(孙东平，潘 锋，史小丽等). Chinese Traditional and Herbal Drugs(中草药)，2000, 31(12)：1.
[3] HUANG Zhi-qing, YAN Xing-hong(黄知清，严兴洪). Marine Technology(海洋技术)，2002, 21(3)：22.
[4] LI Liang-zhu, LI Ming-hua et al(李良铸，李明晔等著). Preparation Ｔechnology of the Ｌatest Ｂiochemical Ｐharmaceutics(最新生化药物制备技术)． Beijing: Chinese Medical and Pharmaceuticals Science Press(北京: 中国医药科技出版社)，2001.
[5] LI Jian-wu(李建武主编). Experimental Principles and Methods of Biochemics(生物化学实验原理和方法). Beijing: Peking University Press(北京: 北京大学出版社)，1994. 300.
[6] WANG Hong-mei, BAO Ｄa-peng, YANG Li-min(王红梅，鲍大鹏，杨立民). Journal of Anhui Agrotechnical Teachers College(安徽农业技术师范学院学报)，2000，14(3)：18.
[7] HU Tong-li, LIU Wen-ying, WU Chun-yong et al(胡同莉，刘文英，吴春勇等). Journal of China Pharmaceutical University(中国药科大学学报)，2002，33(1)：38.
[8] LI Dong-xia, ZHANG Shuang-quan, LIU Ping(李东霞，张双全，刘 平). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2002, 22(1)：59.
[9] LIU Cui-ping, DONG Qun, FANG Ji-nian(刘翠平，董 群，方积年). Chinese Traditional and Herbal Drugs(中草药)，2001, 32(5)：404.
[10] CHEN Yi(陈 怡). World Science and Technology—Modernization of Traditional Chinese Medicine(世界科学技术—中药现代化)，2000, 2(6)：52.
[11] LU Jin-qing, DENG Ke-zhong(芦金清，邓可众). Chinese Traditional Patent Medicine(中成药)，1998, 20(6)：9.
[12] HU Qun-bao, GUO Bao-jiang(胡群宝，郭宝江). Marine Sciences(海洋科学)，2001, 25(7)：41.
[13] HUO Guang-hua, LI Lai-sheng, GAO Yin-yu(霍光华，李来生，高荫榆). Chemistry of Life(生命化学)，2002，22(2)：194.
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