光谱学与光谱分析 |
|
|
|
|
|
Direct Determination of Nb in Titanium Oxide Using Slurry Sample Introduction by Axial Viewing Inductively Coupled Plasma Optical Emission Spectrometry |
WANG Zheng1, 2, CHEN Tian-yu1, TAO Guang-yi1,YANG Peng-yuan2* |
1. Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China 2. Chemistry Department, Fudan University, Shanghai 200433, China |
|
|
Abstract By using dispersant polyacrylate amine (NH4PAA) to disperse TiO2, effects of different dispersants, pH value and the amount of dispersant on TiO2 slurry were investigated. The pH value of the medium and the dispersant amount were optimized, and a stable and homogeneous suspension was prepared. Nb in TiO2 was determined by an axial viewing ICP-OES spectrometer. At the same time, the performance of the axial viewing ICP-OES using solid powder analysis was discussed. Under the optimum experimental conditions, the detection limit of the present method is 3.0 μg·L-1 and the RSD is 3.1%(n=3, c=0.3 mg·L-1).
|
Received: 2003-09-06
Accepted: 2004-01-26
|
|
Corresponding Authors:
YANG Peng-yuan
|
|
Cite this article: |
WANG Zheng,CHEN Tian-yu,TAO Guang-yi, et al. Direct Determination of Nb in Titanium Oxide Using Slurry Sample Introduction by Axial Viewing Inductively Coupled Plasma Optical Emission Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(04): 556-559.
|
|
|
|
URL: |
https://www.gpxygpfx.com/EN/Y2005/V25/I04/556 |
[1] Logothetis E M. Ceram. Eng. Sci. Prog.,1980, 1: 281. [2] Broekaert J A C, Graule T, Jenett H, Tolg G., Tschopel P. Fresenius J. Anam. Chem., 1989, 332: 825. [3] Peng Tianyou, Du Pingwu, Hu Bin, Jiang Zucheng. Analytica Chemica Acta, 2000, 421: 75. [4] Schwitzgebel J, G.Ekerdt J, Gerischer H, Heller A. J. Phys. Chem., 1995, 99: 5633. [5] Nishimoto S, Ohtani B, Kajiwara H, Kagiya T. J. Chem. Soc. Faraday Trans., 1985, 81: 61. [6] Zhang Z B, Wang C C, Zakaria R, Ying J Y. J. Phys. Chem., 1998, 102: 10871. [7] Karakitsou K E, Verkios X E. J. Phys. Chem., 1993, 97: 1184. [8] CHEN Tian-yu,SHAN Fang(陈天裕,单 芳). Chinese Journal of Analytical Laboratory(分析试验室), 1998, 17(2): 47. [9] PENG Tian-you, YAN Qin, HU Bin, JIANG Zu-cheng(彭天佑,颜 琴,胡 斌,江祖成). Chemical Journal of Chinese Universities(高等学校化学学报), 2000, 21(5): 694. [10] McCrindle R I, Marjanovic L. Spectroscopy and Spectral Analysis(光谱学与光谱分析),2002,22(6):996. [11] CUI Ai-li, WANG Ting-jie, HE Hong, JIN Yong(崔爱莉,王亭杰,何 红,金 涌). The Chinese Journal of Process Engineering(过程工程学报), 2001, 1(1): 99. [12] SUN Jing, GAO Lian, GUO Jing-kun(孙 静,高 濂,郭景坤). Journal of Inorganic Materials(无机材料学报), 1997, 12(1): 40. [13] Wang Jun, Gao Lian, Sun Jing. J. Colloid Interface Sci., 1999, 213: 552. [14] Sun Jing, Gao Lian, Guo Jinkun. J. Europ. Ceram. Soc., 1999, 19: 1725. [15] Brenner I B, Zander A T. Spectrochim. Acta, Part B, 2000, 55: 1230. [16] Silva C S, Blanco T, Nobrega J A. Spectrochim. Acta, Part B, 2002, 57: 29.
|
[1] |
HU Xuan1, CHENG Zi-hui1*, ZHANG Shu-chao2, SHI Lei2. Matrix Separation-Determination of Rare Earth Oxides in Bauxite by
Inductively Coupled Plasma-Atomic Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3130-3134. |
[2] |
ZHANG Peng-peng1, 2, XU Jin-li1, 2*, HU Meng-ying1, 2, ZHANG Ling-huo1, 2, BAI Jin-feng1, 2, ZHANG Qin1, 2*. Determinations of Zr, Hf and Nb Contents in Soil Samples by
Laser-Induced Breakdown Spectroscopy (LIBS)[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(07): 2163-2168. |
[3] |
ZHANG Xuan1, 2, 3, WANG Chang-hua1, 2, HU Fang-fei1, 2, MO Shu-min1, 2, LI Ji-dong1, 2, 3*. Determination of Nb and Re in High Purity Tungsten by Precipitation Separation-Inductively Coupled Plasma Mass Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(07): 2169-2174. |
[4] |
WANG Ling-ling1, 2, 3, WANG Bo1, 2, 3, XIONG Feng1, 2, 3, YANG Lu-cun1, 2, LI Jing-jing4, XIAO Yuan-ming1, 2, 3, ZHOU Guo-ying1, 2*. A Comparative Study of Inorganic Elements in Cultivativing Astragalus Membranaceus From Different Habitats[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1407-1412. |
[5] |
LI Ai-yang1, FU Liang2*, CHEN Lin3. Determination of Trace Heavy Metal Elements in Plant Essential Oils by Inductively Coupled Plasma Optical Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1162-1167. |
[6] |
DENG Ya-li1, LI Mei2, WANG Ming2*, HAO Hui1*, XIA Wei1. Surface Plasmon Resonance Gas Sensor Based on Silver/Titanium Dioxide Composite Film[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(03): 743-748. |
[7] |
ZHANG Bin-bin1, 2, LI Jing-bin1, 2, WANG Shi-ning1, 2, HE Peng-fei1, 2, ZHA Xiao-qin1, 2, 3. Determination of Lithium, Iron and Phosphorus in Carbon Composite Lithium Iron Phosphate by Perchloric Acid Digestion-Inductively Coupled Plasma Optical Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(09): 2703-2709. |
[8] |
SHAO Ming-jie1, 2, LIU Wen-ke1, 2*, ZHOU Cheng-bo1, 2, WANG Qi1, 2, LI Bao-shi1, 2. Effects of High Light Duration and Frequencies on Growth and Nutrient Element Contents of Hydroponic Lettuce Cultivated Under LED Red and Blue Light[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(09): 2853-2858. |
[9] |
ZHANG Peng-peng1, 2, HU Meng-ying1, 2, XU Jin-li1, 2*, CHEN Wei-ming1, 2, GU Xue1, 2, ZHANG Ling-huo1, 2, BAI Jin-feng1, 2, ZHANG Qin1, 2. Determination of Available Boron in Soil by ICP-OES With Boiling Water Extraction[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(06): 1925-1929. |
[10] |
HUANG Kai-sheng, XU Dong-yu, CHEN Shu-di, CHEN Xiao-yan*, ZHAO Yan. Determination of Sodium and Zinc in Ethanol Gasoline for Motor Vehicles (E10) by ICP-OES[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(03): 973-977. |
[11] |
FENG Ai-ming1, WANG Fu-qiang1, ZHANG Hong1*, AN Peng2, LI Yang-hui1, 3, WANG Le1*. Significantly Improved Luminescence Properties of YAG Phosphor via Localized Surface Plasmon Resonance of Nanotitania[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(10): 3081-3085. |
[12] |
WANG Shao-na1, JIN Xing2, LIU Biao1, ZHAO Bei-bei3, LI Lan-jie3, LI Ming4, DU Hao1, 5*, ZHANG Yi1. Study on Spectral Interference in the Determination of Vanadium by ICP-OES[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(07): 2283-2288. |
[13] |
ZHOU Xi-lin, WANG Jiao-na, MI Hai-peng, HUANG Qing-qing, LIU Zhong-ming. Determination of Indium in Flue Ash via ICP-AES Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(04): 1201-1206. |
[14] |
HAN Tao1, YU Xiao-ping1*, GUO Ya-fei1, LI Ming-li2, DUO Ji2, DENG Tian-long1. Determination of Lithium in High Salinity Samples by Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES)[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(04): 1214-1220. |
[15] |
LU Ya-rong1, Anwar Hushur1*, Mamatrishat Mamat1, Mubarak Molutjan1, Seiji Kojima2. High Pressure Raman Spectrum Study of NaNbO3[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(03): 738-743. |
|
|
|
|