光谱学与光谱分析 |
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Determination of Trace Beryllium in Geological Samples by Oxygen Doped Air-Acetylene Flame Atomic Absorption Spectrometry |
WU Shao-wei1, 2, YANG Xiao-qiu1,CHEN Wen-wu1, YANG Ming1, TANG Zhi-yong1, JIN Ze-xiang1* |
1. Faculty of Materials Science and Chemical Engineering, China University of Geosciences, Wuhan 430074,China 2. Faculty of Chemistry and Environmental Engineering, Hubei Institute for Nationalities, Enshi 445000, China |
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Abstract A new method for the determination of trace beryllium in geological samples by oxygen-air-acetylene flame atomic absorption spectrometry is reported in the present paper. The optimum determination conditions were selected. When suitable amounts of 8-hydroxyquinoline are added, the interference effect from the coexisting elements can be minimized and the sensitivity for the determination of beryllium can be increased. The detection limit(k=3) is 0.006 μg·mL-1 for beryllium. The method has been applied to the determination of trace beryllium in geological standard samples, and the results are in good agreement with the certified values with a precision of 4.69% RSD(n=8).
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Received: 2003-12-19
Accepted: 2004-05-08
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Corresponding Authors:
JIN Ze-xiang
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Cite this article: |
WU Shao-wei,YANG Xiao-qiu,CHEN Wen-wu, et al. Determination of Trace Beryllium in Geological Samples by Oxygen Doped Air-Acetylene Flame Atomic Absorption Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(05): 785-787.
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URL: |
https://www.gpxygpfx.com/EN/Y2005/V25/I05/785 |
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