| 光谱学与光谱分析 |
|
|
|
|
|
| Determination of Water-Soluble Antimony (Ⅲ) and Antimony(Ⅴ) in Leigongteng Using Ultrasound-Assisted Extraction by HG-ICP-AES |
| XIE Jian-xin, DENG Bi-yang* |
| College of Chemistry and Chemical Engineering, Guangxi Normal University, Guilin 541004, China |
|
|
|
|
Abstract A method for the determination of water-soluble antimony (Ⅲ) and antimony(Ⅴ) in Leigongteng using ultrasound-assisted extraction by hydride generation inductively coupled plasma atomic emission spectrometry was developed in the present paper.Affecting parameters of ultrasound extraction, the pH of antimony species, the operation condition of hydride generation and inductively coupled plasma atomic emission spectrometry were investigated and optimized.The effect of coexisting ions on the determination of antimony was also investigated.The detection limits are 0.3 and 2.4 ng· mL-1 for antimony (Ⅲ) and antimony(Ⅴ), respectively, and with RSD 3.9% for antimony (Ⅲ) and 4.5% for antimony(Ⅴ).The recovery is in the range of 93% to 105%.
|
|
Received: 2004-03-16
Accepted: 2004-05-28
|
|
|
|
Corresponding Authors:
DENG Bi-yang
|
|
| Cite this article: |
|
XIE Jian-xin,DENG Bi-yang. Determination of Water-Soluble Antimony (Ⅲ) and Antimony(Ⅴ) in Leigongteng Using Ultrasound-Assisted Extraction by HG-ICP-AES [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(08): 1347-1350.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2005/V25/I08/1347 |
[1] YIN Xue-bo, HE Xi-wen, LI Yan, et al(尹学博, 何锡文, 李 妍, 等).Chinese J.Anal.Chem.(分析化学)，2003，31(3)： 364.
[2] Deutsche Firschungsge Meinschaft(DFG), Analyses of Hazardous Substances in Biological Materials, VCH, Weinheim, 1994，51.
[3] YAN Xian-de(冉先德).China Pharmacopoea(中华药海).Harbin: Harbin Press (哈尔滨： 哈尔滨出版社), 1998，705.
[4] LIANG Qiong-fang, LI Zeng-xi(梁琼芳,李增禧).Science of Chinese Guangdong Trace Elements(广东微量元素科学), 1997, 4(6): 59.
[5] JIANG Jian-sheng, HUANG Gan-quan, QIAN Shan-hua, et al(姜建生, 黄淦泉, 钱沙华, 等).Chinese J.of Instrumental Analysis(分析测试学报), 1998, 17(4): 1.
[6] MA Mei-ling, YANG Sheng-ke, GENG Zheng(马美玲, 杨胜科, 耿 征).Journal of Shanxi Normal University(陕西师范大学学报), 1997, 25(2): 121.
[7] GUO Hui-shi, LI Yi-heng, XIE Hong-qi(郭会时, 李益恒, 谢红旗).Journal of Analysis Laboratory(分析试验室), 2000, 19(6): 39.
[8] XING Xiao-mei, MEI Jian-ming(邢晓梅, 梅建鸣).Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2003, 23(5): 995.
[9] XIE Jian-xin, DENG Bi-yang, YANG Xiu-fang(谢建新, 邓必阳, 杨秀芳).Journal of Analytical Science(分析科学学报)，2004，20(5)： 480
|
| [1] |
ZHENG Pei-chao, LIU Ran-ning, WANG Jin-mei, FENG Chu-hui, HE Yu-tong, WU Mei-ni, HE Yu-xin. Solution Cathode Glow Discharge-Atomic Emission Spectroscopy Coupled With Hydride Generation for Detecting Trace Mercury and Tin in Water[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1139-1143. |
| [2] |
LI Ai-yang1, FU Liang2*. Study on the Analysis Total As in Bentonite With Microwave Plasma Atomic Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(12): 3671-3675. |
| [3] |
CHEN Hai-jie1, 2, MA Na1, 2, BO Wei1, 2, ZHANG Ling-huo1, 2, BAI Jin-feng1,2, SUN Bin-bin1, 2, ZHANG Qin1, 2, YU Zhao-shui1, 2*. Research on the Valence State Analysis Method of Selenium in Soil and Stream Sediment[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(03): 871-874. |
| [4] |
LIU Wei-yi, MENG Yuan, JIN Bai-chuan, JIANG Meng-yun, LIN Zu-hong, HU Li-yang, ZHANG Ting-ting*. Distribution Characteristics and Ecological Risk Assessment of Heavy Metals in Surface Sediments of the North Canal Using ICP-OES[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(12): 3912-3918. |
| [5] |
YUAN Xiao-xue, ZHOU Ding-you, LI Jie*, XU Xian-shun, YONG Li, HU Bin, LIU Tao*. Progress in the Analysis of Elements in PM2.5 by ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(08): 2373-2381. |
| [6] |
LIN Hai-lan1, 2, ZHU Ri-long1*, YU Lei2, CHENG Yong-xia3, ZHU Rui-rui2, LIU Pei2, REN Zhan-hong3. Determination of Arsenic, Mercury, Selenium, Antimony and Bismuth in Soil and Sediments by Water Bath Digestion-Atomic Fluorescence Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(05): 1528-1533. |
| [7] |
SUN Qi-xuan, WEI Xing, LIU Xun, YANG Ting, CHEN Ming-li*, WANG Jian-hua*. Atomic Spectrometry/Elemental Mass Spectrometry in Bioanalytical Chemistry: A Review[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(05): 1340-1345. |
| [8] |
ZHAO Ming-yue1, 2, 3, CHENG Jun-qi1, 2, YANG Bing-cheng3, WANG Zheng1, 2*. Highly Sensitive Determination of Selenium, Arsenic and Mercury in Seawater by Hydride Generation Coupled with Solution Cathode Glow Discharge Optical Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(05): 1359-1365. |
| [9] |
Lü Li, LI Yuan, JING Mei-jiao, MA Meng-dan, PENG Yue-han, QIN Shun-yi, LI Liu-an*. Determination of Selenium in Three Kinds of Eggs by Hydride Generation Atomic Fluorescence Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(02): 607-611. |
| [10] |
LI Yuan-ying, XU De-gang, GUI Wei-hua, YANG Chun-hua*, CAI Yao-yi. A Novel Method for Measuring Antimony Sulfide Content Based on Gaussian-Peak Fitting of Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(12): 3743-3748. |
| [11] |
DONG Zai-zheng1, 2, WANG Nan1, LI Xue-jiao3, TONG Xiao-min1, WANG Lin1, YANG Hong-ying3*. AAS Determination of Sb in Pretreated Copper Anode Slime by Alkali Fusion Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(12): 3877-3881. |
| [12] |
ZHANG Fang1, 2, 3, ZHANG Wei-jie1, 3, DING Yan-yan1, 3, ZHAO Zhong-guo1, 3, GE Hao1, 3. XRD Diffraction Characteristics and Microscopic Morphology of Carbonates in Saline-Alkaline Soil from the Shore of the Aibi Lake[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(12): 3893-3899. |
| [13] |
LING Fang, MENG Qing-long, HUANG Ren-shuai, ZHANG Bin*. The Characteristics of Thermally Tunable Multi-Bands Terahertz Modulator[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(05): 1334-1338. |
| [14] |
ZHANG Shuo1,2 . Microsecond Pulsed Hollow Cathode Lamp as Enhanced Excitation Source of Hydride Generation Atomic Fluorescence Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(09): 2412-2419. |
| [15] |
ZHOU Jing-rong1, DENG Dong-yan1, HUANG Ke1, TIAN Yun-fei2*, HOU Xian-deng1,2* . Simultaneous Determination of Se and Te in Ores by HG-AFS After Online Preconcentration with Nano-TiO2 Immobilized on Silica Gel[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(09): 2401-2406. |
|
|
|
|
