光谱学与光谱分析 |
|
|
|
|
|
Determination of Trace Lead and Iron in Nickel Chloride and Manganese Sulfate by Flame Atomic Absorption Spectrometry after Coprecipitation with Yttrium Phosphate |
SU Yao-dong, ZHU Wen-ying, MA Hong-mei, CHEN Long-wu |
Department of Chemistry, Tongji University, Shanghai 200092, China |
|
|
Abstract Using yttrium phosphate as the coprecipitation collector for the separation and preconcentration of trace lead and iron in nickel chloride and manganese sulfate, flame atomic absorption spectrometric (FAAS) determination was described in the present paper. Coprecipitation parameters including the pH of the solution, and the amounts of YCl3 and H3PO4 were discussed. It was found that lead and iron in nickel chloride could be coprecipitated quantitatively in the range of pH 3.0~4.0, and so could be lead in manganese sulfate. The detection limits (3σ) of lead and iron in 20 mL solution were 1.63×10-2 mg·L-1 and 4.58×10-2 mg·L-1 respectively. In NiCl2 solution the standard addition recoveries for lead and iron were 100.91% and 99.73% respectively, and in MnSO4 solution the standard addition recoveries were 99.45% and 98.98% respectively. The method has eliminated the interference of matrix, and the result is satisfied.
|
Received: 2005-06-18
Accepted: 2005-10-06
|
|
Corresponding Authors:
SU Yao-dong
|
|
Cite this article: |
SU Yao-dong,ZHU Wen-ying,MA Hong-mei, et al. Determination of Trace Lead and Iron in Nickel Chloride and Manganese Sulfate by Flame Atomic Absorption Spectrometry after Coprecipitation with Yttrium Phosphate [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(09): 1732-1734.
|
|
|
|
URL: |
https://www.gpxygpfx.com/EN/Y2006/V26/I09/1732 |
[1] YAO Jin-yu, HU Qing-lan, XIE Wen-bing(姚金玉, 胡庆兰, 谢文兵). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 1994, 14(5): 69. [2] SUN Xin(孙 昕). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 1995, 15(5): 97. [3] LI Lin, FENG Yi-jun, HUANG Gan-quan(李 琳, 冯易君, 黄淦泉). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 1998, 18(3): 354. [4] SU Yao-dong, CHENG Xiang-sheng, XIAO Hong-xi(苏耀东, 程祥圣, 肖红玺). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2003, 23(5): 984. [5] DONG Li-ping, FANG Zhao-lun(董立平, 方肇伦). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 1994, 14(1): 85. [6] Kagaya S, Araki Y, Hasegawa K. Chemistry Letters, 2000, 339(通卷)(3): 208. [7] Elci Latif, Arslan Zikri, Tyson Julian F. Spectrochimica Acta Part B, 2000, 55: 1109. [8] CHEN Shu-yu, SUN Mei(陈树瑜, 孙 梅). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2001, 21(3): 377. [9] Wang Zhao-Hui, et al. Analytica Chimica Acta, 2004, 514: 151. [10] FAN Hua-jun, LI Gong-ke, LUAN Wei, et al(范华均,李攻科,栾 伟,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2005,25(9):1503. [11] Rubinson K A, Rubinson J F. Contemporary Instrumental Analysis(English Reprint Edition). Beijing: Pearson Education North Asia Limited and Science Press, 2002. 18.
|
[1] |
ZHOU Ao1, 2, YUE Zheng-bo1, 2, LIU A-zuan1, 2, GAO Yi-jun3, WANG Shao-ping3, CHUAI Xin3, DENG Rui1, WANG Jin1, 2*. Spectral Analysis of Extracellular Polymers During Iron Dissimilar
Reduction by Salt-Tolerant Shewanella Aquimarina[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1320-1328. |
[2] |
XIANG Song-yang1, 3, XU Zhang-hua1, 2, 4, 5, 6*, ZHANG Yi-wei1, 2, ZHANG Qi1, 3, ZHOU Xin1, 2, YU Hui1, 3, LI Bin1, 2, LI Yi-fan1, 2. Construction and Application of ReliefF-RFE Feature Selection Algorithm for Hyperspectral Image Classification[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3283-3290. |
[3] |
SHI Pei1, JIN Zhi-wei1, WANG Fen1*, LUO Hong-jie1, 2, ZHU Jian-feng1, YE Guo-zhen3, ZHANG Yu-feng4. Influence Mechanism of the Iron-Rich Raw Material on the Iron-Based Crystalline Glazes[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1628-1633. |
[4] |
LIU Zheng-jiang1, ZHANG Qian-cheng2, MA Hui-yan2*, LIU Ju-ming2. Spectral Characteristics of Hangjin2# Clay and Its Mechanism in Heterogeneous Fenton Reaction[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(11): 3512-3517. |
[5] |
ZHANG Zhi-qi1, ZHAO Tong1, LIU Ling1, LI Yan1,2*. Spectral Characteristics of Madagascar Agates[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(10): 3227-3232. |
[6] |
LIU Tan1, 2, XU Tong-yu1, 2*, YU Feng-hua1, 2, YUAN Qing-yun1, 2, GUO Zhong-hui1, XU Bo1. Chlorophyll Content Estimation of Northeast Japonica Rice Based on Improved Feature Band Selection and Hybrid Integrated Modeling[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(08): 2556-2564. |
[7] |
Khaled Althubeiti. Synthesis and Structural Characterizations of Ternary Iron(Ⅱ) Mixed Ligand Complex: Low Cost Materialsas a Precursor for Preparation of Nanometric Fe2O3 Oxide[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(06): 1988-1992. |
[8] |
Lamia A Albedair1*, Samar O Aljazzar1, Mohamed I Kobeasy2,3,Moamen S Refat3,4*. Complexity of Gold(Ⅲ) Ion With Cefotaxime and Cefepime Drugs: Spectroscopic, Antimicrobial and Antitumor Discussions[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(10): 3315-3320. |
[9] |
LI Ling1, 2, 3, NAI Xue-ying1, 2*, CHAI Xiao-li1, 2, 3, LIU Xin1, 2, GAO Dan-dan1, 2, DONG Ya-ping1, 2. Optimization of Determination Method of Lithium in Oil-Field Water Based on DOE[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(08): 2617-2621. |
[10] |
ZHOU Mo1, 2, ZOU Bin1, 2*, TU Yu-long1, 2, XIA Ji-pin1, 2. Hyperspectral Modeling of Pb Content in Mining Area Based on Spectral Feature Band Extracted from Near Standard Soil Samples[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(07): 2182-2187. |
[11] |
HUANG Rui1, LI Yu1, HE Wen-xuan1*, LU Xian-yong2, CHEN Wei-jian1, CHEN Ting1, ZHANG Yan-jie1. A Quick and Simple Method for Extracting Unsaponifiables of Vegetable Oil[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(06): 1852-1856. |
[12] |
LIU Rong-xiang, LI Jie*, SU Wen-rou, ZHANG Xue-feng, LI Jia-wei, MENG Liu-yang. FTIR and XPS Analysis Comparing the Activation Mechanism of Ca2+ and Fe3+ on Quartz[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(06): 1876-1882. |
[13] |
CHEN Yi-xue1, NIU Shan-shan2, LI Hong-ping2, YU Fei1, WU Yong-jun1, LIU Li-e1*. Determination of DNA Methyltransferases 1 by a Method of Fluorescence Immunoassay Based on Magnetic Particles[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(01): 162-167. |
[14] |
Ahmed. I. El-Shenawy*, Ishaq. F. E. Ahmed, Moamen. S. Refat. Fabrication of Semiconductor Polymer Membranes Combined with a Colored Charge Transfer Complexes Used in the Manufacture of Solar Cells as a Source of Alternative Energy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(07): 2307-2315. |
[15] |
ZHAO Hai-xia, WANG Xin-wei*, LI Ru-xue, WANG Deng-kui, FANG Xuan, FANG Dan, WEI Zhi-peng, WANG Xiao-hua. Effect of Passivation Substrates Surface to CsPbBr3 Quantum Dot Films Optical Stability[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(06): 1706-1710. |
|
|
|
|