| 光谱学与光谱分析 |
|
|
|
|
|
| The Research on Preparing CeO2 Nanocrystalline by Homogeneous Precipitation Method |
| Garidi1, LI Xia1*, LI Li2, Zhaorigetu1 |
1. College of Chemical and Environmental Science, Inner Mongolia Normal University, Huhhot 010022, China
2. Chemistry Department of Hetao University, Baiyinnaoer 015000, China |
|
|
|
|
Abstract CeO2 nanocrystallines were prepared by homogeneous complexed-precipitation method, using cerous nitrate and ammonium tartrate as raw materials. The effects of cerous tartrate complex compound and the way of producing precipitation on the particle size of samples were investigated. The samples were characterized by XRD, TEM and SEM. The SEM micrograph shows that the foam exhibits a perforated porousness stereostructure in shape, and the HRTEM picture of the particles reveals the clear crystal lattice. All the results indicate that the samples were CeO2 nanocrystalline.
|
|
Received: 2005-05-28
Accepted: 2005-08-26
|
|
|
|
Corresponding Authors:
LI Xia
|
|
| Cite this article: |
|
Garidi,LI Xia,LI Li, et al. The Research on Preparing CeO2 Nanocrystalline by Homogeneous Precipitation Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(09): 1746-1748.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2006/V26/I09/1746 |
[1] WANG Shi-min，XU Zu-xun, FU Jing(王世敏, 许祖勋, 傅 晶). Preparation Technology of Nanocrystalline Materials(纳米材料制备技术). Beijing: Chemistry Industry Press(北京: 化学工业出版社). 2002.
[2] DONG Xiang-ting, QU Xiao-gang, et al(董相廷, 曲晓刚, 等). Chinese Science Bulletin(科学通报), 1996, 41(16): 1396.
[3] HSU W P, Ronnquist Matijevice. Langmui, 1988, 4(1): 31.
[4] SHI Shuo, LU Run-hua, WANG Han-qing(石 硕，鲁润华，王汉卿). Chinese Chemistry Bulletin(化学通报)，1998, (12)：51.
[5] DONG Xiang-ting，LI Ming，ZHANG Wei, et al(董相廷，李 明，张 伟, 等). Journal of the Chinese Rare Earth Society(中国稀土学报), 2001，19(1)：24.
[6] ZHOU Xin-mu(周新木). Journal of the Chinese Rare Earth Society(中国稀土学报)，2002，20：67.
[7] DONG Xiang-ting，MAI Shi-jian，ZHANG Wei(董相廷，麦世坚，张 伟). Journal of Material Science and Engineering(材料科学与工程学报·自然科学版)，2001，19(1)：99.
[8] CHEN Huai-xia, HU Lin-xue, SONG Gong-wu(陈怀侠，胡林学，宋功武). Journal of Hubei University (Natural Science Edition)(湖北大学学报·自然科学版)，1999，21(4)：357.
[9] TAO Dong-liang, XU Yi-zhuang, HUANG Yi, et al(陶栋梁，徐怡庄，黄 毅, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2005, 25(1): 5.
|
| [1] |
GU Yi-lu1, 2，PEI Jing-cheng1, 2*，ZHANG Yu-hui1, 2，YIN Xi-yan1, 2，YU Min-da1, 2, LAI Xiao-jing1, 2. Gemological and Spectral Characterization of Yellowish Green Apatite From Mexico[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 181-187. |
| [2] |
ZHOU Bei-bei1, LI Heng-kai1*, LONG Bei-ping2. Variation Analysis of Spectral Characteristics of Reclaimed Vegetation in an Ionic Rare Earth Mining Area[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3946-3954. |
| [3] |
ZHANG Hao-yu1, FU Biao1*, WANG Jiao1, MA Xiao-ling2, LUO Guang-qian1, YAO Hong1. Determination of Trace Rare Earth Elements in Coal Ash by Inductively Coupled Plasma Tandem Mass Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2074-2081. |
| [4] |
SUN Da-wei1, 2, 3, DENG Jun1, 2*, JI Bing-bing4. Study on the Preparation Mechanism of Steel Slag-Based Biomass Activated Carbon by Special Steel Slag-Discard Walnut Shells Based on ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2308-2312. |
| [5] |
CHEN Di, SONG Chen, SONG Shan-shan, ZHANG Zhi-jie*, ZHANG Hai-yan. The Dating of 9 Batches of Authentic Os Draconis and the Correlation
Between the Age Range and the Ingredients[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(06): 1900-1904. |
| [6] |
HE Yan1, SU Yue1, YANG Ming-xing1, 2*. Study on Spectroscopy and Locality Characteristics of the Nephrites in Yutian, Xinjiang[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(12): 3851-3857. |
| [7] |
SHI Dong-dong, CAO Zhao-bin, HUAN Yan-hua, GONG Yan-chun, WU Wen-yuan, YANG Jun*. Reflection Polarization Spectral Characteristics of High Performance Coating Material La2Zr2O7[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 2995-2999. |
| [8] |
HU Xuan1, CHENG Zi-hui1*, ZHANG Shu-chao2, SHI Lei2. Matrix Separation-Determination of Rare Earth Oxides in Bauxite by
Inductively Coupled Plasma-Atomic Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3130-3134. |
| [9] |
JUMAHONG Yilizhati1, 2, TAN Xi-juan1, 2*, LIANG Ting1, 2, ZHOU Yi1, 2. Determination of Heavy Metals and Rare Earth Elements in Bottom Ash of Waste Incineration by ICP-MS With High-Pressure Closed
Digestion Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3168-3173. |
| [10] |
ZHU Zhao-zhou1*, YANG Xin-xin1, LI Jun1, HE Hui-jun2, ZHANG Zi-jing1, YAN Wen-rui1. Determination of Rare Earth Elements in High-Salt Water by ICP-MS
After Pre-Concentration Using a Chelating Resin[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1862-1866. |
| [11] |
SHAO Ke-man, FU Gui-yu, CHEN Su-yan, HONG Cheng-yi, LIN Zheng-zhong*, HUANG Zhi-yong*. Preparation of Molecularly Imprinted Fluorescent Probe for Rare Earth Complex and Determination of Malachite Green Residue[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(03): 808-813. |
| [12] |
ZHANG Tie-zhu1, 2, ZHANG Yu-xuan2, 3, LIU Sai-yu2, 4, LI Hang-ren2, XU Wen-ce1, 2, ZHANG Jin-shan1*, OUYANG Shun-li2*, WU Nan-nan4. The Occurrence and Distribution of REE Minerals in Fluorite-Type Ores in Bayan Obo：Constraints From Raman Mapping[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(12): 3776-3781. |
| [13] |
LIU Ming-bo1,2, LIAO Xue-liang2, CHENG Da-wei1,2, NI Zi-yue1,2, WANG Hai-zhou1,2*. An EDXRF Quantitative Algorithm Based on Fundamental Parameters and Spectrum Unfolding[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(09): 2807-2811. |
| [14] |
SUN Feng1, 2, YAN Qing-qing1, WANG Lu1, SUN Zhen-fei1. Study on the Conditions of Hydrothermal Synthesis of Chinese Purple BaCuSi2O6 and the Analysis of Its Products[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(07): 2284-2287. |
| [15] |
DING Han1, WANG Meng2*. Enhanced Development of Footprints Using YVO4∶Eu Luminescent Nanomaterials[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(01): 88-93. |
|
|
|
|
