| 光谱学与光谱分析 |
|
|
|
|
|
| Study on the TLC-SERS of Sulfamethoxazole |
| ZHANG Jin-zhi1, WANG Yuan2, CHEN Xiang-ming1 |
1. Department of Physics, North China University of Technology, Beijing 100041, China
2. Department of Chemistry, Capital Normal University, Beijing 100037, China |
|
|
|
|
Abstract The spectra of sulfamethoxazole, the efficient ingredient of sulfanilamide-like medicine, were investigated by combining the TLC and FT-Raman spectroscopy using the surface enhanced Raman spectroscopy technique. The result indicates that the main vibrant characteristic spectral band can be obtained by TLC in a samples of just about 1 μg. The difference between the compound sulfamethoxazole and the corresponding spectra picture is analyzed. The analysis shows that the method of combining TLC and FT-Raman spectroscopy by the SERS is practical and advantageous in the highly sensitive measurement of the chemical ingredient in medicine.
|
|
Received: 2005-06-06
Accepted: 2005-09-28
|
|
|
|
Corresponding Authors:
ZHANG Jin-zhi
|
|
[1] Canzera M, Sturm S, Stuppner H, et al. Chromatographia, 1997, 46(3/4): 197.
[2] Herderich M, Richling E, Roscher R, et al. Chromatographia, 1997, 45: 127.
[3] LI Zhong-hong, SHEN Wen-bin, et al(李忠红，沈文斌, 等). Foreign Medical Sciences Section on Pharmacy(国外医学药学分册)，2001，28(1)：47.
[4] Zhao Y, Nookandeh A, Schneider B, et al. J. Chromatography, A, 1999, 837(1/2): 83.
[5] Moskovits M. Rev. Mod. Phys., 1985, 57: 783.
[6] Hildebrant P, et al. J. Phys. Chem., 1984, 88: 5935.
[7] WANG Yuan, GUO Zhan-sheng, WANG Ying-feng, et al(汪 瑗，国占生, 王英锋，等).Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2002，22(5)：745.
[8] ZHANG Jin-zhi, WANG Yuan(张进治，汪 瑗). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2003，23(1)：67.
[9] WANG Yuan, ZHANG Jin-zhi, MA Xin-yong(汪 瑗，张进治，马新勇). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2004，24(11)：1373.
|
| [1] |
XING Hai-bo1, ZHENG Bo-wen1, LI Xin-yue1, HUANG Bo-tao2, XIANG Xiao2, HU Xiao-jun1*. Colorimetric and SERS Dual-Channel Sensing Detection of Pyrene in
Water[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 95-102. |
| [2] |
LU Wen-jing, FANG Ya-ping, LIN Tai-feng, WANG Hui-qin, ZHENG Da-wei, ZHANG Ping*. Rapid Identification of the Raman Phenotypes of Breast Cancer Cell
Derived Exosomes and the Relationship With Maternal Cells[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3840-3846. |
| [3] |
GUO He-yuanxi1, LI Li-jun1*, FENG Jun1, 2*, LIN Xin1, LI Rui1. A SERS-Aptsensor for Detection of Chloramphenicol Based on DNA Hybridization Indicator and Silver Nanorod Array Chip[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3445-3451. |
| [4] |
LI Wen-wen1, 2, LONG Chang-jiang1, 2, 4*, LI Shan-jun1, 2, 3, 4, CHEN Hong1, 2, 4. Detection of Mixed Pesticide Residues of Prochloraz and Imazalil in
Citrus Epidermis by Surface Enhanced Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3052-3058. |
| [5] |
ZHAO Ling-yi1, 2, YANG Xi3, WEI Yi4, YANG Rui-qin1, 2*, ZHAO Qian4, ZHANG Hong-wen4, CAI Wei-ping4. SERS Detection and Efficient Identification of Heroin and Its Metabolites Based on Au/SiO2 Composite Nanosphere Array[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3150-3157. |
| [6] |
SU Xin-yue1, MA Yan-li2, ZHAI Chen3, LI Yan-lei4, MA Qian-yun1, SUN Jian-feng1, WANG Wen-xiu1*. Research Progress of Surface Enhanced Raman Spectroscopy in Quality and Safety Detection of Liquid Food[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2657-2666. |
| [7] |
ZHAO Yu-wen1, ZHANG Ze-shuai1, ZHU Xiao-ying1, WANG Hai-xia1, 2*, LI Zheng1, 2, LU Hong-wei3, XI Meng3. Application Strategies of Surface-Enhanced Raman Spectroscopy in Simultaneous Detection of Multiple Pathogens[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2012-2018. |
| [8] |
CHENG Chang-hong1, XUE Chang-guo1*, XIA De-bin2, TENG Yan-hua1, XIE A-tian1. Preparation of Organic Semiconductor-Silver Nanoparticles Composite Substrate and Its Application in Surface Enhanced Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2158-2165. |
| [9] |
LI Chun-ying1, WANG Hong-yi1, LI Yong-chun1, LI Jing1, CHEN Gao-le2, FAN Yu-xia2*. Application Progress of Surface-Enhanced Raman Spectroscopy for
Detection Veterinary Drug Residues in Animal-Derived Food[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(06): 1667-1675. |
| [10] |
HUANG Xiao-wei1, ZHANG Ning1, LI Zhi-hua1, SHI Ji-yong1, SUN Yue1, ZHANG Xin-ai1, ZOU Xiao-bo1, 2*. Detection of Carbendazim Residue in Apple Using Surface-Enhanced Raman Scattering Labeling Immunoassay[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(05): 1478-1484. |
| [11] |
LU Yan-hua, XU Min-min, YAO Jian-lin*. Preparation and Photoelectrocatalytic Properties Study of TiO2-Ag
Nanocomposites[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1112-1116. |
| [12] |
WANG Yi-tao1, WU Cheng-zhao1, HU Dong1, SUN Tong1, 2*. Research Progress of Plasticizer Detection Based on Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1298-1305. |
| [13] |
LI Wei1, 2, HE Yao1, 2, LIN Dong-yue2, DONG Rong-lu2*, YANG Liang-bao2*. Remove Background Peak of Substrate From SERS Signals of Hair Based on Gaussian Mixture Model[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 854-860. |
| [14] |
YIN Xiong-yi1, SHI Yuan-bo1*, WANG Sheng-jun2, JIAO Xian-he2, KONG Xian-ming2. Quantitative Analysis of Polycyclic Aromatic Hydrocarbons by Raman Spectroscopy Based on ML-PCA-BP Model[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 861-866. |
| [15] |
HAN Xiao-long1, LIN Jia-sheng2, LI Jian-feng2*. SERS Analysis of Urine for Rapid Estimation of Human Energy Intake[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(02): 489-494. |
|
|
|
|
