光谱学与光谱分析 |
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Simultaneous Determination of Trace Arsenic and Antimony in Textile by Intermittent Flow-Hydride Generation-Atomic Fluorescence Spectrometry with L-Cysteine as a Prereducer |
Lü Shui-yuan, DAI Jin-lan, ZHONG Mao-sheng |
Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou 350001, China |
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Abstract A method for the simultaneous determination of trace arsenic and antimony in textile by intermittent flow-hydride generation-atomic fluorescence spectrometry with L-cysteine as a prereducer was developed. The optimal instrument condition was established. The influence factors such as the acidity of sample solution and carrier liquid, the concentrations of KBH4 and L- cysteine, the flow rate of carrier, and the interference of coexistent elements were investigated. The method was convenient and rapid. Under the optimal condition, the detection limits were 0.35 and 0.22 μg·L-1, the relative standard deviations were 1.3% and 2.8%, and the recoveries were in the ranges of 93.6%-98.4% and 92.2%-103.6% for As and Sb respectively.
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Received: 2005-05-08
Accepted: 2005-08-26
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Corresponding Authors:
Lü Shui-yuan
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Cite this article: |
Lü Shui-yuan,DAI Jin-lan,ZHONG Mao-sheng. Simultaneous Determination of Trace Arsenic and Antimony in Textile by Intermittent Flow-Hydride Generation-Atomic Fluorescence Spectrometry with L-Cysteine as a Prereducer [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(07): 1352-1355.
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URL: |
https://www.gpxygpfx.com/EN/Y2006/V26/I07/1352 |
[1] GB/T 17593—1998. [2] HOU H B,Narasaki H. Analytical Sciences, 1998, 14(6): 1161. [3] LI Zhong-xi,TONG Kai-yuan,GUO Xiao-wei(李中玺,童开源,郭小伟). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2001,21(5):655. [4] GUO Xiao-wei,GUO Xu-ming(郭小伟,郭旭明). Spectroscopy and Spectral Analysis(光谱学与光谱分析),1995,15(3):97. [5] ZHOU Gen-lin(周根林). Mining and Metallurgy(矿冶), 1998,7(3):92. [6] ZHANG Chun-mei(张春美). Chinese Journal of Health Laboratory Technology(中国卫生检验杂志), 2004,14(2):213. [7] CHEN Xiao-mei(陈晓妹). Physical Testing and Chemical AnalysisPart B:Chemical Analysis Section(理化检验:化学分册), 2003,39(2): 83. [8] CHEN Heng-wu, HE Qiao-hong(陈恒武,何巧红). Chinese Journal of Analytical Chemistry(分析化学), 2000,28(3):368. [9] ISO 105-E04.1994. [10] LI Zhong-xi(李中玺). Spectral Instrument and Analysis(光谱仪器与分析), 2003, 3:13.
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