| 光谱学与光谱分析 |
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| Synthesis of N’1,N’2-Bis[(1E)-(2-Hydroxyphenyl) Methylene]- Ethanedihydrazide and Its Application to Determination of Zn(Ⅱ) |
| LIANG Zhuo-wen, MENG Jian-xin* |
| Department of Chemistry, Jinan University, Guangzhou 510632, China |
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Abstract A reagent of N’1,N’2-bis[(1E)-(2-hydroxyphenyl)methylene]ethanedihydrazide (DSOD) was synthesized, and characterized by IR spectra and element analysis. A highly sensitive fluorimetric method for the determination of trace amounts of zinc was proposed based on the reaction of Zn2+ with DSOD in ethanol at pH 7.00. The linear range of the method was 0-65.0 μg·L-1 with a detection limit of 0.30 μg·L-1. The interferences of 16 common ions were investigated and the results showed that the DSOD had a good selectivity. The analytical results of detecting trace amounts of Zn2+ in zinc rich salt and hair by this method were satisfactory.
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Received: 2005-04-12
Accepted: 2005-08-28
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Corresponding Authors:
MENG Jian-xin
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| Cite this article: |
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LIANG Zhuo-wen,MENG Jian-xin. Synthesis of N’1,N’2-Bis[(1E)-(2-Hydroxyphenyl) Methylene]- Ethanedihydrazide and Its Application to Determination of Zn(Ⅱ)[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(06): 1145-1147.
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| URL: |
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https://www.gpxygpfx.com/EN/Y2006/V26/I06/1145 |
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