| 光谱学与光谱分析 |
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| Study on the Spectroscopy of 5-(4-Pyridyl)-1,3,4-Oxadiazole-2-Thiol |
| WANG Ying,YAN Lian-he |
| Chemical Engineering School, Nanjing University of Science and Technology, Nanjing 210094, China |
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Abstract The title compound (5-(4-pyridyl)-1,3,4-oxadiazole-2-thiol) was synthesized by the ring-closing reaction of isoniazide with carbon bisulfide, and the reaction course was discussed preliminarily. The mechanism of this reaction is nucleophilic addition. The compound was characterized by Fourier transform infrared(FTIR) spectrometry and nuclear magnetic resonance(NMR). The thermal analytical data indicate that the compound was decomposed completely at the temperature of 506 ℃.
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Received: 2005-09-28
Accepted: 2005-12-26
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Corresponding Authors:
WANG Ying
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