光谱学与光谱分析 |
|
|
|
|
|
Synthesis and Characterization of Chitosan-Imine-Palladacycle |
LIU Pu, LI San-hua, WANG Xiang-yu, LI Li-min |
Department of Chemistry, Zhengzhou University, Zhengzhou 450052, China |
|
|
Abstract Chitosan was grafted with salicylaldehyde to obtain Schiff base. The Schiff base reacted with Li2PdCl4 in methanol to synthesize chitosan-imine-palladacycle. The structure of chitosan, schiffbase and chitosan-imine-palladacycle was characterized by IR, XRD, DTA-TG, fluorescence and XPS. According to the results of analysis, the structure of Schiff base and chitosan-imine-palladacycle can be inferred.
|
Received: 2004-12-28
Accepted: 2005-06-15
|
|
Corresponding Authors:
LIU Pu
|
|
Cite this article: |
LIU Pu,LI San-hua,WANG Xiang-yu, et al. Synthesis and Characterization of Chitosan-Imine-Palladacycle[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(04): 666-669.
|
|
|
|
URL: |
https://www.gpxygpfx.com/EN/Y2006/V26/I04/666 |
[1] Bose A, Saha C H. J. Mol. Catal., 1989, 49(2): 271. [2] King K A, Watts R J. J .Am. Chem. Soc., 1987, 109(5): 1589. [3] Cope A C, Friedrich E C. J. Am. Chem. Soc., 1968, 90(4): 909. [4] Ohff M, Ohff A, Milstein D. Chem. Commun., 1999, (4): 357. [5] Nowotny M, Hanefeld U, Koningsveld H, et al. Chem. Commun., 2000, (19): 1877. [6] Onoue H, Moritani I. J. Organomet. Chem., 1972, 43(2): 431. [7] WANG Ai-qin, ZHAO Pei-qing, GAO Xiao-jun, YU Xian-da(王爱勤,赵培庆,高小军,俞贤达). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 1999, 19(6): 817. [8] Hughes J. Biotechnology Techniques, 1990, 4(1): 55. [9] SUN Wei, XIA Chun-gu, WANG Ai-qin(孙 伟, 夏春谷, 王爱勤). Acta Chim. Sin.(化学学报), 2002, 60(1): 162. [10] WEI Dan-yi, LI Dong-cheng, YAO Ke-min(魏丹毅, 李冬成, 姚克敏). Chin. J. of Inorganic Chemistry(无机化学学报), 1998, 14(2): 209. [11] Natalia V K, Alecander Y S, Olga P T, et al. Journal of Molecular Catalysts A: Chemical., 2004, 209(1-2): 97. [12] HUANG Xiao-jia, WANG Ai-qin, YUAN Guang-pu(黄小佳,王爱勤,袁光谱). Chin. J. of Applied Chemistry(应用化学), 2000, 17(1): 66. [13] Fahd A, Tirkostani A. Polymer Degradation and Stability, 1998, 60(1): 67. [14] MA Hui-xuan, HU Dao-dao, FANG Yu(马会宣,胡道道,房 喻). Chin. J. of Applied. Chemistry(应用化学), 2001, 18(4): 290. [15] LANG Hui-yun, ZHANG Xiu-jun, SHEN Ye-hua, et al(朗惠云,张秀军,申烨华,等). Chemical Journal of Chinese Universities(高等学校化学学报),2003, 24(11): 1937. [16] CAI Ming-zhong, ZHAO Hong, HUANG Yi-zheng(蔡明中, 赵 红, 黄义争). Chin. J. Organic Chemistry(有机化学), 2003, 23(6): 555. [17] Blackburn J B. Inorg Chem., 1970, 9(10): 2374. |
[1] |
LEI Hong-jun1, YANG Guang1, PAN Hong-wei1*, WANG Yi-fei1, YI Jun2, WANG Ke-ke2, WANG Guo-hao2, TONG Wen-bin1, SHI Li-li1. Influence of Hydrochemical Ions on Three-Dimensional Fluorescence
Spectrum of Dissolved Organic Matter in the Water Environment
and the Proposed Classification Pretreatment Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 134-140. |
[2] |
GU Yi-lu1, 2,PEI Jing-cheng1, 2*,ZHANG Yu-hui1, 2,YIN Xi-yan1, 2,YU Min-da1, 2, LAI Xiao-jing1, 2. Gemological and Spectral Characterization of Yellowish Green Apatite From Mexico[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 181-187. |
[3] |
HAN Xue1, 2, LIU Hai1, 2, LIU Jia-wei3, WU Ming-kai1, 2*. Rapid Identification of Inorganic Elements in Understory Soils in
Different Regions of Guizhou Province by X-Ray
Fluorescence Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 225-229. |
[4] |
WANG Hong-jian1, YU Hai-ye1, GAO Shan-yun1, LI Jin-quan1, LIU Guo-hong1, YU Yue1, LI Xiao-kai1, ZHANG Lei1, ZHANG Xin1, LU Ri-feng2, SUI Yuan-yuan1*. A Model for Predicting Early Spot Disease of Maize Based on Fluorescence Spectral Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3710-3718. |
[5] |
CHENG Hui-zhu1, 2, YANG Wan-qi1, 2, LI Fu-sheng1, 2*, MA Qian1, 2, ZHAO Yan-chun1, 2. Genetic Algorithm Optimized BP Neural Network for Quantitative
Analysis of Soil Heavy Metals in XRF[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3742-3746. |
[6] |
SONG Yi-ming1, 2, SHEN Jian1, 2, LIU Chuan-yang1, 2, XIONG Qiu-ran1, 2, CHENG Cheng1, 2, CHAI Yi-di2, WANG Shi-feng2,WU Jing1, 2*. Fluorescence Quantum Yield and Fluorescence Lifetime of Indole, 3-Methylindole and L-Tryptophan[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3758-3762. |
[7] |
YANG Ke-li1, 2, PENG Jiao-yu1, 2, DONG Ya-ping1, 2*, LIU Xin1, 2, LI Wu1, 3, LIU Hai-ning1, 3. Spectroscopic Characterization of Dissolved Organic Matter Isolated From Solar Pond[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3775-3780. |
[8] |
LI Xiao-li1, WANG Yi-min2*, DENG Sai-wen2, WANG Yi-ya2, LI Song2, BAI Jin-feng1. Application of X-Ray Fluorescence Spectrometry in Geological and
Mineral Analysis for 60 Years[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 2989-2998. |
[9] |
XUE Fang-jia, YU Jie*, YIN Hang, XIA Qi-yu, SHI Jie-gen, HOU Di-bo, HUANG Ping-jie, ZHANG Guang-xin. A Time Series Double Threshold Method for Pollution Events Detection in Drinking Water Using Three-Dimensional Fluorescence Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3081-3088. |
[10] |
MA Qian1, 2, YANG Wan-qi1, 2, LI Fu-sheng1, 2*, CHENG Hui-zhu1, 2, ZHAO Yan-chun1, 2. Research on Classification of Heavy Metal Pb in Honeysuckle Based on XRF and Transfer Learning[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2729-2733. |
[11] |
JIA Yu-ge1, YANG Ming-xing1, 2*, YOU Bo-ya1, YU Ke-ye1. Gemological and Spectroscopic Identification Characteristics of Frozen Jelly-Filled Turquoise and Its Raw Material[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2974-2982. |
[12] |
YANG Xin1, 2, XIA Min1, 2, YE Yin1, 2*, WANG Jing1, 2. Spatiotemporal Distribution Characteristics of Dissolved Organic Matter Spectrum in the Agricultural Watershed of Dianbu River[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2983-2988. |
[13] |
CHEN Wen-jing, XU Nuo, JIAO Zhao-hang, YOU Jia-hua, WANG He, QI Dong-li, FENG Yu*. Study on the Diagnosis of Breast Cancer by Fluorescence Spectrometry Based on Machine Learning[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2407-2412. |
[14] |
ZHU Yan-ping1, CUI Chuan-jin1*, CHENG Peng-fei1, 2, PAN Jin-yan1, SU Hao1, 2, ZHANG Yi1. Measurement of Oil Pollutants by Three-Dimensional Fluorescence
Spectroscopy Combined With BP Neural Network and SWATLD[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2467-2475. |
[15] |
LIU Xian-yu1, YANG Jiu-chang1, 2, TU Cai1, XU Ya-fen1, XU Chang3, CHEN Quan-li2*. Study on Spectral Characteristics of Scheelite From Xuebaoding, Pingwu County, Sichuan Province, China[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2550-2556. |
|
|
|
|