光谱学与光谱分析 |
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Determination of Eleven Elements in Water-Touched Material by ICP-MS |
Lü Lin-lin1,XU Ye1*,YI Ping2,QU Ning2,GU Xin-rong1 |
1. College of Science, Northeastern University, Shenyang 110004, China 2. Liaoning Province Center for Disease Control and Prevention, Shenyang 110005,China |
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Abstract Water-touched material include water distribution equipment, protecting materials, and water treatment material. The security of the material plays an important role in everyone’s daily life. So it’s necessary to determing metal elements in the material. A method for the determination of eleven elements, including Ag, As, Ba, Cd, Cu, Sb, Sn, Mn, Ni, Pb and Hg, in the water-touched material by inductively coupled plasma-mass spectrum(ICP-MS) is described. The plasma parameters were optimized as follows: The RF input power was 1 350 W; flow rate of cooling gas was 13 L·min-1; flow rate of assistant gas was 0.70 L·min-1; flow rate of carrying gas was 0.8 L·min-1; flow rate of atomization gas was 1.02 L·min-1; rate of sampling was 1.48 mL·min-1. The detection limits of these eleven elements were 0.003-0.170 μg·L-1. The relative standard deviations(n=6) were 0.6%-6.3%. The correlation coefficients were 0.999 0-0.999 6. The recoveries of the method were 92.4%-108.2%. This method is sensitive, accurate and simple compared with other methods, and has the advantage of wide linear range. The results were satisfactory.
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Received: 2005-09-08
Accepted: 2005-11-28
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Corresponding Authors:
XU Ye
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Cite this article: |
Lü Lin-lin,XU Ye,YI Ping, et al. Determination of Eleven Elements in Water-Touched Material by ICP-MS [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(03): 548-550.
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URL: |
https://www.gpxygpfx.com/EN/Y2006/V26/I03/548 |
[1] YU Chang-xing,ZHANG Min-fang,GAO Ying-li(俞长兴,张敏芳,高英立). Chinese J. Anal. Chem.(分析化学), 1997, 25(5): 531. [2] ZHANG Qi-feng,LIU Qin,YAO Xing(张奇凤,刘 琴,姚 兴). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2004, 24(3): 366. [3] Atanassova D, Stefanova V, Russeva E. Talanta,1998, 47(5): 1237. [4] Gabler Hans-Eike, Bahr Andreas. Chemical Geology,1999, 156(1-4): 323. [5] YIN Ming,LI Bing, FU Ting-fa(尹 明,李 冰,符廷发). Journal of Analytical Science(分析科学学报), 1995, 11(1): 13. |
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