光谱学与光谱分析 |
|
|
|
|
|
Study on Properties and Resonance Rayleigh Scattering Spectra of Nanometer Selenium(0) Particles in Liquid Phase |
BAI Yan1,LI Wei-jia1,WU Ya-qin1, 2,ZHENG Wen-jie1,YANG Fang1 |
1. Department of Chemistry,Jinan University,Guangzhou 510632,China 2. Department of Chemistry,Shanxi Normal University,Linfen 041004,China |
|
|
Abstract In the HCl solution, selenium(Ⅳ) and excessive ascorbic acid(Vc) formed selenium(0), which homogeneously and steadily existed in liquid phase system. The Se(0) particles were aggregating spheres and their sizes were 26-243 nm from transmission electron microscope(TEM) and laser light scattering image. The nanometer Se(0) solution produced strongest resonance rayleigh scattering(RRS) at 470 nm. The intensity of RRS at 470 nm was linear with the concentration of Se(Ⅳ) in the range of 2.82×10-9-5.64×10-6 g·mL-1 (r=0.997). Moreover, obvious Second-order scattering(SOS) and multiple frequence scattering(MFS) appeared at the same time.
|
Received: 2004-11-16
Accepted: 2005-02-16
|
|
Corresponding Authors:
BAI Yan
|
|
Cite this article: |
BAI Yan,LI Wei-jia,WU Ya-qin, et al. Study on Properties and Resonance Rayleigh Scattering Spectra of Nanometer Selenium(0) Particles in Liquid Phase[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(02): 313-316.
|
|
|
|
URL: |
https://www.gpxygpfx.com/EN/Y2006/V26/I02/313 |
[1] ZHEN Wen-jie, OUYANG Zhen(郑文杰,欧阳政). The Application of Chemistry and Medicine for Plants Selenium(植物有机硒的化学及其医学应用). Guangzhou:Jinan University Press(广州: 暨南大学出版社),2001. [2] LIU Jin-guo,YU Jian-ning(刘进国,于建宁). Feed of Guangdong(广东饲料),2003,12(4):20. [3] YANG She-hua,ZHU Mao-xiang(杨陟华,朱茂祥). Trace Element and Health Research(微量元素与健康研究),1999,16(1):4. [4] GAO Xue-yun,ZHANG Jin-song,ZHANG Li-de, et al(高学云,张劲松,张立德, 等). Public Health of China(中国公共卫生),2003,19(3):309. [5] ZHANG Jin-song,GAO Xue-yun,ZHANG Li-de, et al(张劲松,高学云,张立德, 等). Journal of Nutrition(营养学报),2000,22(3):219. [6] HUANG Zhi,ZHENG Wen-jie,LI Le-nong, et al(黄 峙,郑文杰,李乐农, 等). Chinese bioengineering Journal(中国生物工程杂志),2003,23(7):76. [7] LIU Shao-pu,LIU Zhong-fang,LI Ming(刘绍璞,刘忠芳,李 明). Acta Chimica Sinica(化学学报),1995,53:1178. [8] LIU Shao-pu,LIU Zhong-fang,LUO Hong-qun(刘绍璞,刘忠芳,罗红群). Journal of Southwest China Normal University. Natural Science(西南师范大学学报,自然科学版),2000,25(4):408. [9] LING Shao-ming,JIANG Zhi-liang, BI Xian-shu, YI Xiang-hui(凌绍明,蒋治良, 闭献树, 义祥辉). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2001,21(6):819. [10] YANG Ming-mei,JIANG Zhi-liang(杨明媚,蒋治良). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2002,22(2):204. [11] JIANG Zhi-liang,MENG Mian-wu,LIU Shao-pu(蒋治良,蒙冕武,刘绍璞). Chinese J. of Analytical Chemistry(分析化学),2003,31(3):315. [12] JIANG Zhi-liang,LIU Shao-pu,ZHAO Bao-gang, et al(蒋治良,刘绍璞,赵宝刚, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2002,22(4):615.
|
[1] |
LI Yu-tang1, WANG Lin-zhu1, 2*, LI Xiang3, WANG Jun1. Characterization and Comparative Analysis of Non-Metallic Inclusions in Zirconium Deoxidized Steel[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2916-2921. |
[2] |
YAO Dong-mei1, 2, LU Shan-shan1, WEN Gui-qing1, LIANG Ai-hui1, JIANG Zhi-liang1*. Determination of Trace Urea by Resonance Rayleigh Scattering-Energy Transfer Spectroscopy Coupled With Polystyrene Nanoprobe and Dimethylglyoxime Reaction[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(11): 3590-3593. |
[3] |
LI Yuan, LI Kai, ZHAO Dong-e. Rapid Detection System for HSA Based on RRS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(06): 1925-1929. |
[4] |
ZHAO Yan-mei, WU Huan, ZENG Xiao-qing, GUO Yuan, YUAN Hai-yan, HUANG Yun-mei, TAN Xuan-ping, ZHANG Lei, YANG Ji-dong*. A Selective Resonance Rayleigh Scattering Method for Chiral Recognition of Carnitine Enantiomers Based on Cu2+ Functionalized Gold Nanoparticles[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(06): 1965-1972. |
[5] |
LIANG Ai-hui, YANG Duo, WEN Gui-qing, LIU Qing-ye, JIANG Zhi-liang* . A Hydride Generation-Catalytic Resonance Rayleigh Scattering Method for Detection of Trace Arsenic [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2016, 36(11): 3689-3692. |
[6] |
TIAN Bing-mei1, XIE Xiao-mei1,2*, SHEN Pan-pan1, YANG Mo1, ZHANG Sheng-long1, TANG Qing-jiu3 . Preliminary Investigation of the Amount,the Molecular Weight and the Activity of Polysaccharides from Chaenomeles Speciosa Fruits in Ethanol Fractional Precipitation [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(05): 1331-1334. |
[7] |
DING Liang1, YANG Hui1, XI Ya-nan2, ZHANG Jin-chao2, SHEN Shi-gang2* . Synthesis and Characterization of Non Fluorescent ZnS Nano Clusters [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(01): 146-150. |
[8] |
FENG Shi-qi1, SONG Wei1, WANG Yan2, MIAO Xin-hui1, XU Li-jun1, LIU Yu1, LI Cheng1, LI Wen-long1, WANG Yi-ran1, CAI Hong-xing1*. Scattering Properties of Core-Shell Structure of Mist Wrapped Dust Particles[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2014, 34(12): 3218-3223. |
[9] |
MA Lu, WEN Gui-qing, LIU Qing-ye, LIANG Ai-hui*, JIANG Zhi-liang* . Resonance Rayleigh Scattering Determination of Trace Tobramycin Using Aptamer-Modified Nanogold as Probe [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2014, 34(09): 2481-2484. |
[10] |
LIU Gao-san, LIANG Ai-hui*, WEN Gui-qing, JIANG Zhi-liang* . Resonance Rayleigh Scattering Determination of Trace Ozone Based on the Cationic Surfactant Association Particles [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2014, 34(03): 725-728. |
[11] |
WANG Gao, FENG Qiao-ling, XUE Zhong-jin, LI Yang-jun, ZHOU Han-chang . Research on Detecting Concentration of Serum Protein Based on Resonance Rayleigh Scattering[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2013, 33(03): 752-755. |
[12] |
WANG Sheng-mian1, 2, WU Meng1, LIANG Ai-hui1*, JIANG Zhi-liang1* . DNAzyme Cracking-Nanogold Resonance Rayleigh Scattering Spectral Method for the Determination of Trace Cu2+ [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2013, 33(01): 147-150. |
[13] |
WU Li-ping1, LENG Xiao-jing1, SUN Yan1, REN Fa-zheng1*,Nakai Shuryo2 . Analysis of the Effects of pH and Salt on the Conformation of the Sericin Particles by DLS and TEM Measurements [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2010, 30(05): 1391-1395. |
[14] |
YANG Pei-hui, WEI Wei, CAI Huai-hong, FENG Jing, CAI Ji-ye . Immobilization of Anti-Transferrin On Nano-Gold and Its Immune Recognition of Transferrin[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2009, 29(05): 1398-1401. |
[15] |
WAN Mu-hua, ZHAO Mei-xia, OUYANG Jian-ming*. Research on Particle Size and Size Distribution of Nanocrystals in Urines by Laser Light Scattering Method [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2009, 29(01): 217-221. |
|
|
|
|