光谱学与光谱分析 |
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Determination of Eight Metal Elements in Cichorium glandulosum Boiss et Huet by Microwave Digestion-FAAS |
PEI Ling-peng1,ZHOU Xiao-ying2,CUI Jian1,PANG Zong-ran1,LIU Hong-bing3,GE Liang3 |
1. Institute of Chinese Minority Traditional Medicine, Minzu University of China, Beijing 100081, China 2. College of Pharmacy, Xinjiang Medical University, Urumqi 830054, China 3. College of Traditional Chinese Medicine, Xinjiang Medical University, Urumqi 830054, China |
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Abstract The Cichorium glandulosum Boiss et Huet is a traditional Uighur natural herbal medicine, but has not been analyzed and studied in terms of its metal elements. In the experiment, the Cichorium glandulosum Boiss et Huet powder was digested with HNO3 by microwave digestion before determination. The eight metal elements, potassium, nickel, calcium, magnesium, iron, manganese, copper and zinc, in Cichorium glandulosum Boiss et Huet were determined by FAAS. The working conditions, accuracy and precision of the method were studied. The linear correlations of standard curves are good (r=0.999 1-0.999 9). The recovery (n=6) is 92.25%-110.5%, and the RSD (n=6) is 0.7%-3.88%. The results showed that there were comparatively rich metal elements, among which are comparatively high calcium (65.84 mg·g-1), iron (24.38 mg·g-1), magnesium (278.17 mg·g-1) and potassium (18.50 mg·g-1), in Cichorium glandulosum Boiss et Huet, and the contents of other elements are nickel of 0.004 38 mg·g-1, manganese of 0.52 mg·g-1, copper of 0.016 5 mg·g-1 and zinc of 0.18 mg·g-1. This provided useful data for discussing the relationship between the content of the metal elements in Cichorium glandulosum Boiss et Huet and its clinical application in cardiovascular and osteoporosis disease.
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Received: 2008-12-20
Accepted: 2009-03-26
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Corresponding Authors:
PEI Ling-peng
E-mail: lppei@hotmail.com
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